• 대한치과보철학회지
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• 제39권5호
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• pp.502-513
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• 2001

The purpose of this study was to evaluate the effect of dentin pretreatment with Dentin Conditioner, Ultra-Etch, conditioner of Fuji Plus cement on the shear bond strength of resin-reinforced glass ionomer cements to dentin and analyze the fractured surfaces. To evaluate the bond strength, the extracted human teeth which had uniform area of exposed dentin were cemented with conventional glass ionomer cement, 3M $RelyX^{TM}$ Luting (Vitremer luting cement), Fuji Plus cement after dentin pretreatment. The shear bond strength was measured using the Universal testing machine (Instron Co., USA) with a crosshead speed of 1mm/m. The effect of dentin pretreatment was evaluated by observing pretreated dentin surfaces under the scanning electron microscope, measuring the shear bond strength and observing the fractured surfaces under the scanning electron microscope. The results were as follows : On the SEM observation of surface morphology, the specimens treated with Dentin Conditioner. Ultra-Etch and conditioner of Fuji Plus cement were removed the smear layer and funneled dentinal tubules in dentin surfaces. In $RelyX^{TM}$ Luting cement group, shear bond strength of pretreated group was significantly higher than control group. In Fuji Plus cement group and Fuji I group, regardless of the type of pretreatment agents, there was tendency of increase in the shear bond strength. On the SEM observation of fractured surfaces, as the shear bond strength increase, it were shown thicker cement layers and were not shown dentinal tubules According to these results. it were shown that dentin pretreatment have much effect on bonding states.

• 박물관보존과학
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• 제14권
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• pp.69-79
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• 2013

손기정(1912 - 2002)이 1936년 베를린 올림픽 마라톤 우승의 부상으로 받은 보물 제904호 고대 그리스 청동제투구는 보존처리 부위가 열화되어 균열과 변색이 발생하였고, 코가리개가 상단 접합 부위의 균열에 의해 아래쪽으로 쳐지게 되어 다시 보존처리하였다. 코가리개를 본체에서 분리하고, 본체와 코가리개를 안정화 및 강화처리를 한 후 다시 접합하였다. 본체의 균열 부위와 결실 부위에는 직조 유리섬유로 보강하였으며, 코가리개는 접합 후 직조 유리섬유와 Ti판을 사용하여 보강하였다. 코가리개의 충전 부위는 주변과 같이 문양을 새기고 색맞춤을 하였다.

• Restorative Dentistry and Endodontics
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• 제38권3호
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• pp.134-140
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• 2013

Objectives: There has been a growing interest in glass ceramic systems with good esthetics, high fracture resistance and bonding durability, and simplified fabrication techniques using CAD/CAM. The aim of this study is to compare flexural strength before and after heat treatment of two lithium disilicate CAD/CAM blocks, IPS e.max CAD (Ivoclar Vivadent) and Rosetta SM (Hass), and to observe their crystalline structures. Materials and Methods: Biaxial flexural strength was tested according to ISO 6872 with 20 disc form specimens sliced from each block before and after heat treatment. Also, the crystalline structures were observed using field-emission scanning microscopy (FE-SEM, Hitachi) and x-ray diffraction (XRD, Rigaku) analysis. The mean values of the biaxial flexural strength were analyzed by the Mann-Whitney U test at a significance level of p = 0.05. Results: There were no statistically significant differences in flexural strength between IPS e.max CAD and Rosetta SM either before heat treatment or after heat treatment. For both ceramics, the initial flexural strength greatly increased after heat treatment, with significant differences (p < 0.05). The FE-SEM images presented similar patterns of crystalline structure in the two ceramics. In the XRD analysis, they also had similar patterns, presenting high peak positions corresponding to the standard lithium metasilicate and lithium disilicate at each stage of heat treatment. Conclusions: IPS e.max CAD and Rosetta SM showed no significant differences in flexural strength. They had a similar crystalline pattern and molecular composition.

• 한국세라믹학회지
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• 제39권2호
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• pp.184-189
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• 2002

본 연구는, PbO-base 유리계의 정보와의 비교 등을 통해 Bi-base 조성 PDP rib으로의 새로운 유리조성 설계를 위한 기초연구의 일환이다. PbO와 유사한 밀도값 및 작업 용이성을 갖고 있는 Bi를 도입한 $Bi_2O_3-B_2O_3-ZnO$ 조성계에 대해, 연화점, 열팽창계수, 에칭성, 유전율 등의 특성측정 및 XPS로 조성에 따른 구조변화 등을 조사하였다. $Bi_2O_3$를 50∼80 wt%까지 폭넓게 첨가된 $Bi_2O_3-B_2O_3-ZnO$계 유리들은 조성에 따라 연화점이 400∼480$^{\circ}C$, 열팽창계수가 $68{\sim}72{\times}10^{-7}/^{\circ}C$, 유전상수는 13∼25으로서 동조성의 Pb-base 조성계와 유사한 물성치를 나타내었다. 특히, Bi의 함유량이 70∼65 wt%의 조성의 경우, 성분 및 물성의 미세조정 등을 통해 rib 재료의 출발조성으로서 적용가능성이 확인되었다. $Bi_2O_3$의 양이 감소함에 따라 $O_{1s}$ peak에서의 결합에너지의 증가와 반가폭(FWHM)이 감소하였는데, 이는 비가교산소의 증가에 기인하였다.

• Restorative Dentistry and Endodontics
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• 제23권1호
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• pp.183-196
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• 1998

The purpose of this study was to determine the effect of bleaching technique on the shear bond strength of esthetic restorative materials to bovine enamel. The bleaching agent was used 35% $H_2O_2$(Hi-Lite, Shofu, U.S.A.). Experimental groups were divided into two divisions as group A and B. Experimental A groups for the effect of number of bleaching were as follows ; Group Al : no bleaching Group A2 : bleaching 1 time ( for 5 minutes ) Group A3 : bleaching 3 times ( each for 5 minutes ) Group A4 : bleaching 6 times ( each for 5 minutes ) Group A5 : bleaching 9 times ( each for 5 minutes ) Experimental B groups for the effect of storage period in artificial saliva were as follows ; Group B1 : not stored in artificial saliva after bleaching Group B2 : stored in artificial saliva for 1 day after bleaching Group B3 : stored in artificial saliva for 1 week after bleaching Group B4 : stored in artificial saliva for 2 weeks after bleaching Group B5 : stored in artificial saliva for 4 weeks after bleaching Composite resin and glass ionomer cement were bonded to all specimens, and the shear bond strength between enamel and r~storative material were measured in Instron Universal Testing Machine(Instron, 4467, U.S.A,), Additionally, the bleached enamel specimens were examed after etching with 37.4% $H_3PO_4$ for 1 min under SEM(S-2300, Hitachi Co., Japan) to observe the effect of bleaching procedure on enamel surface morphology. The result were as follows ; 1. In SEM findings, bleached bovine enamel was found to be superficially rough. 2. In bleached bovine enamel, the effect of acid etching was reduced with the increase of number of bleaching. 3. The mean shear bond strength of composite resin and glass ionomer cement to bleached enamel surface tended to be lower than those to non-bleached enamel surface. 4. With the increase of number of bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively decreased. 5. Increasing the, storage period in artificial saliva after bleaching, the shear bond strength of composite resin and glass ionomer cement to bleached enamel were progressively increased. 6. The mean shear bond strength of glass ionomer cement to bleached bovine enamel tended to be clearly lower than that of composite resin.

• Composites Research
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• 제32권2호
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• pp.90-95
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• 2019

LNG 운반선의 슬로싱 충격하중은 LNG 화물창 내 단열시스템의 파손을 야기하는 주원인이다. 단열시스템의 파손은 LNG 화물창 내 극저온을 유지시키는 데 치명적으로 작용하게 된다. 극저온을 유지하기 위해서는 단열재료의 성능 강화가 가장 전형적인 방법이다. 일반적으로 LNG 화물창 내의 단열재료는 폴리우레탄 폼과 플라이우드, 이 두 재료를 접합시키기 위한 접착제가 사용된다. 본 연구에서는 단열시스템에 채용되는 단열재료를 강화하기 위한 일환으로 글라스 버블/에폭시 복합수지를 제작하여 충격 하중이 작용할 때 재료의 흡수에너지를 향상시켰다. 실험 시나리오는 글라스버블의 첨가량, 온도의 영향성을 분석하기 위한 상온 및 극저온 환경을 고려하여 자유낙하 실험을 수행하였다. 실험 결과는 글라스 버블 첨가량이 20 wt.%에 도달할 경우 극저온 흡수에너지가 최대의 성능이 나타나는 것을 확인하였다. 반면에 상온 흡수에너지는 첨가량 0 wt.%에서 최대 성능을 보였다. 글라스버블/에폭시 수지의 혼합성능의 경우 첨가량이 20 wt.%가 되면 교반성능 저하로 인하여 응집현상이 발생하여, 접착성능이 떨어질 것으로 판단된다.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2005년도 추계종합학술대회
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• pp.793-796
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• 2005

In this paper, we propose a method which can improve uniformity of a miniaturized electron beam array for inspection of very small pattern with high speed using vertical interconnection. This method enables the individual control of columns so that it can reduce the deviation of beam current, beam size, scan range and so on. The test device that used vertical interconnection method was fabricated by multiple wafer bonding and metal reflow. Two silicon and one glass wafers were bonded and metal interconnection by melting of electroplated AuSn was performed. The contact resistance was under $10{\Omega}$.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.376-376
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• 2016

Poly(ethylene oxide) (PEO)/functionalized bacterial cellulose nanowhiskers (f-BCNW) (0.1 wt%) composite nanofibers were fabricated by electrospinning process and the thermomechanical properties were significantly enhanced more than the PEO and PEO/bacterial cellulose nanowhiskers (BCNW) (0.1 wt%) composite nanofibers. The functionalization of BCNW (f-BCNW) was performed by microwave plasma treatment for effects of nitrogen functionalization of chemically-driven BCNW. The N-containing functional groups of f-BCNW enhanced chemical bonding between the hydroxyl groups of the polymer chains in the PEO matrix and diameter size of PEO/f-BCNW (0.1 wt%) composite nanofibers were decreased more than PEO and PEO/BCNW (0.1 wt%) composite nanofibers on the same concentration. The strong interfacial interactions between the f-BCNW nanofillers and polymer matrix were improved the thermomechanical properties such as crystallization temperature, weight loss and glass transition temperature (Tg) compared to PEO and PEO/BCNW composites nanofibers. The results demonstrated that N2 plasma treatment of BCNW is very useful in improving thermal stability for bio-applications.

• 대한기계학회논문집B
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• 제30권12호
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• pp.1196-1202
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• 2006

A MEMS methanol reformer was fabricated and its performance was evaluated in the present study. Catalytic steam reforming of methanol was selected because the process had been widely applied in macro scale reformers. Conventional Cu/ZnO catalyst that was prepared by co-precipitation method to give the highest coating quality was used. The reactor structure was made by bonding three layers of glass wafers. The internal structure of the wafer was fabricated by the wet-etching process that resulted in a high aspect ratio. The internal surface of the reactor was coated by catalyst and individual wafers were fusion-bonded to form the reactor structure. The internal volume of the microfabricated reactor was $0.3cm^3$ and the reactor produced exhaust gas with hydrogen concentration at 73%. The production rate of hydrogen was 4.16 ml/hr that could generate power of 350 mW in a typical PEM fuel cell.

• E2M - 전기 전자와 첨단 소재
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• 제8권4호
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• pp.434-442
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• 1995

To improve dielectric and mechanical properties of insulating composite by plasma surface treatment, new plasma surface treatment process is designed with concentric and hemi-circle electrodes system. the plasma, which is generated between anode and cathode, is induced to the upper side of the electrode system and treats the surface of the insulators. The optimal surface treatment condition is that pressure : 0.5[torr], flux density : 100[gauss], discharge current : 500[mA] and treatment time : 3 minutes. The composite filled with glass cloth surface-treated by plasma shows the improvement in electric and mechanical properties, comparing non- and coupling agent treated samples.