• 제목/요약/키워드: boiling-in-oil process

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High-Temperature Drying Characteristics of Wood during Boiling-In-Oil Process

  • Lee, Hyoung Woo;Choi, Nak Ju
    • Journal of the Korean Wood Science and Technology
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    • 제35권5호
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    • pp.1-6
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    • 2007
  • Boiling-in-oil process was performed to investigate the high-temperature drying characteristics of 25, 50, and 70 mm-thick flat-sawn Douglas-fir lumber. Drying rates, moisture profiles and temperature profiles were monitored. Fully refined paraffin wax was used as drying agent and heated to $130^{\circ}C$. Average drying rates of 25, 50, and 70 mm-thick specimen were 11.6, 6.7, 5.0%/h, respectively. The moisture content differences between cores and ends were 1~2% in 25 mm-thick and 200 mm-long sample and over 10% in 50 mm-thick and 600 mm-long sample.

Enhancement of Antioxidant Quality of Green Leafy Vegetables upon Different Cooking Method

  • Hossain, Afzal;Khatun, Mst. Afifa;Islam, Mahfuza;Huque, Roksana
    • Preventive Nutrition and Food Science
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    • 제22권3호
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    • pp.216-222
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    • 2017
  • Antioxidant rich green leafy vegetables including garden spinach leaf, water spinach leaf, Indian spinach leaf, and green leaved amaranth were selected to evaluate the effects of water boiling and oil frying on their total phenolic content (TPC), total flavonoid content (TFC), reducing power (RP), and antioxidant capacity. The results revealed that there was a significant increase in TPC, TFC, and RP in all the selected vegetables indicating the effectiveness of the cooking process on the antioxidant potential of leafy vegetables. Both cooking processes enhanced significantly (P<0.05) the radical scavenging ability, especially the oil fried samples showed the highest values. There is a significant reduction in the vitamin C content in all the vegetables due to boiling and frying except in the Indian spinach leaf. However, the present findings suggest that boiling and frying can be used to enhance the antioxidant ability, by increasing the bioaccessibility of health-promoting constituents from the four vegetables investigated in this study.

Compositional Characterization of Petroleum Heavy Oils Generated from Vacuum Distillation and Catalytic Cracking by Positive-mode APPI FT-ICR Mass Spectrometry

  • Kim, Eun-Kyoung;No, Myoung-Han;Koh, Jae-Suk;Kim, Sung-Whan
    • Mass Spectrometry Letters
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    • 제2권2호
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    • pp.41-44
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    • 2011
  • Molecular compositions of two types of heavy oil were studied using positive atmospheric pressure photoionization (APPI) Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS). Vacuum gas oil (VGO) was generated from vacuum distillation of atmospheric residual oil (AR), and slurry oil (SLO) was generated from catalytic cracking of AR. These heavy oils have similar boiling point ranges in the range of 210-$650^{\circ}C$, but they showed different mass ranges and double-bond equivalent (DBE) distributions. Using DBE and carbon number distributions, aromatic ring distributions, and the extent of alkyl side chains were estimated. In addition to the main aromatic hydrocarbon compounds, those containing sulfur, nitrogen, and oxygen heteroatoms were identified using simple sample preparation and ultra-high mass resolution FT-ICR MS analysis. VGO is primarily composed of mono- and di-aromatic hydrocarbons as well as sulfur-containing hydrocarbons, whereas SLO contained mainly polyaromatic hydrocarbons and sulfur-containing hydrocarbons. Both heavy oils contain polyaromatic nitrogen components. SLO inludes shorter aromatic alkyl side chains than VGO. This study demonstrates that APPI FT-ICR MS is useful for molecular composition characterization of petroleum heavy oils obtained from different refining processes.

폐플라스틱의 열분해 유화기술 개발 (Process Development of Pyrolysis Liquefaction for Waste Plastics)

  • 노남선;신대현;박소원;이경환;김광호;전상구;조봉규
    • 신재생에너지
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    • 제2권2호
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    • pp.118-125
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    • 2006
  • The target of this work was the process development of demonstration plant to produce the high quality alternative fuel oil by the pyrolysis of mixed plastic waste. In the first step of research, the bench-scale units of 70 t/y and the pilot plant of 360 t/y had been developed. Main research contents in this step were the process performance test of pilot plant of 360 ton/year and the development of demonstration plant of 3,000 t/y, which was constructed at Korea R & D Company in Kimjae City. The process performance of pilot plant of 360 t/y showed about 80% yield of liquid product, which was obtained by both light gas oil(LGO) and heavy gas oil(HGO), The boiling point range distribution of LO product that was mainly consisting of olefin components in PONA group appeared at between that of commercial gasoline and kerosene. On the other hand, HO product was mainly paraffin and olefin components and also appeared at upper temperature distribution range than commercial diesel. Gas product showed a high fraction of $C_3\;and\;C_4$ product like LPG composition, but also a high fraction of $CO_2$ and CO by probably a little leak of process.

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조리과정에서 생성된 미세먼지의 크기분포 특성 (Size Distribution Characteristics of Particulate Matter Emitted from Cooking)

  • 주상우;지준호
    • 한국입자에어로졸학회지
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    • 제16권1호
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    • pp.9-17
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    • 2020
  • The characteristics of particulate matter made from daily cooking at a Korean residential apartment house with three dwellers had been investigated for about 3 months. All data were recorded by an optical particle counter every minute at the kitchen. Types of cooking such as boiling, frying, and grilling that performed in the house were listed. Boiling only was used in 32% cases among total 234 meals. Frying and grilling were 14% and 11%, respectively. From an initial indoor particulate matter smaller than 10 ㎛ in diameter, the increases due to cooking are reported by size. In case of boiling, PM at 1-10 ㎛ size and under 1 ㎛ size little increased. Normally, particles from oil or combustion in a process of frying or grilling increased indoor PM. In a case of grilling, particle mass concentration in a region of 1-10 ㎛ in diameter increased as much as 295 ㎍/㎥. Mass concentration of particles smaller than 1 ㎛ increased as much as 33 ㎍/㎥.

우리나라 사슴고기와 노루고기 조리법(調理法)의 역사적(歷史的) 고료(考寮) (The Historycnl Study of Deer and Roe Deer Cooking in Korea)

  • 김태홍
    • 한국식생활문화학회지
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    • 제12권3호
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    • pp.275-287
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    • 1997
  • The purpose of this paper is to examine the various kinds of recipes of deer and roe deer through classical cookbooks written from 1670 to 1943. The recipes of deer and roe deer are found 31 times in the literature written in classical Chinese from 1715 to the mid-l8th century, which can be classified six groups. Their records are less than other recipes such as beef, chicken, pork, lamb, and dog, but the deer recipe is recorded frequently as four times as the roe deer one The deer were cooked and preserved by the following six ways like large-size drying, drying, boiling, soup, roasting, and gruel, while three ones such as boiling, roasting, and drying were applied to the roe deer. However, there is little difference in recipes between deer and roe deer. In case of deer, boiling and drying were the most popular ones with the frequency of 28%. But the recipes of the roe deer, boiling, roasting, and drying are recorded with the same frequency of 33.3%. The recipes were introduced from China, and had many characteristics different from other kinds of meat, of which most process reflected the mordern cooking scientific aspect. The main ingredients were flesh meat, tail, and tongue and horn was used with uniqueness. Salt, vinegar, oil soy sauce, and the white part of the green onion were used as main seasonings. Alcohol, chuncho, sesame flower powder, and cinnamon powder are frequently added.

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감압비등을 이용한 혼합연료의 분무제어에 관한 연구 (Study on the Spray Control of Mixed Fuel Using Flash Boiling)

  • 명광재;윤준규
    • 대한기계학회논문집B
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    • 제34권11호
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    • pp.1005-1013
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    • 2010
  • 본 연구는 HCCI 엔진의 운전조건을 고려한 혼합연료의 감압비등 분무제어방법을 평가하기 위하여 수행하였다. 2상영역이 존재하는 혼합연료는 고비점성분의 증발촉진과 함께 연료분무의 급격한 증발을 유도할 수 있는 감압비등분무를 이용함으로써 저온 및 저밀도장에서 혼합기형성과정의 제어가 가능하다. HCCI 엔진은 이러한 분위기조건에서 연료를 조기분사하기 때문에 착화성이 높은 경유와 휘발성이 높은 가솔린성분으로 함유한 혼합연료의 감압비등현상을 이용함으로써 액체연료의 분열, 미립화와 같은 물리적 제어 및 착화연소에 의한 화학적 제어를 실현할 수 있다. 본 연구는 혼합연료의 성분과 몰분율을 주요변수로 설정하여 정적용기 내에 분사된 연료분무의 감압비등현상을 슐리렌 화상 및 Mie 산란광을 촬영한 후, 화상처리과정을 통하여 이루어졌다. 그 결과로 감압비등현상은 비교적 저온 및 저밀도장에서 분무구조가 크게 변화함을 알 수 있었으며, 조기 연료분사시기에서 감압비등분무를 이용한 혼합기형성을 제어함으로써 HCCI 연소에 적용이 가능할 것으로 분석하였다.

UNS N08810 합금의 입계부식손상과 원인 분석 (Elucidation of Intergranular Corrosion of UNS N08810 alloys)

  • 김영식;황보덕
    • Corrosion Science and Technology
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    • 제11권5호
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    • pp.196-204
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    • 2012
  • Corrosion failure of petrochemical facilities is one of the difficulties in maintenance, since operating conditions of crude oil production, storage, and refinement are very aggressive. UNS N08810, which has been used for crude oil transportation pipes and storage tanks in petrochemical industries, shows good resistance to general corrosion and localized corrosion in several environments. Among its environments, UNS N08810 showed better corrosion resistance in fuel gas containing sulfuric acid and phosphoric acid and sulfur. However, ductility and toughness at high temperature over about $500^{\circ}C$ were greatly reduced due to microstructural change. In general, welding process is the representative method to join the parts in industrial components. Because the alloy by welding can be sensitized and corroded, the manufacturing process should be controlled. In this work, UNS N08810 was used and heat treatment conditions including solution and stabilization treatments were controlled. Oxalic acid etch test by ASTM A262 Practice A was done to evaluate the qualitative sensitization in room temperature. Huey test by ASTM A262 Practice C was done to evaluate the intergranular corrosion rate in boiling 65% $HNO_3$ solution. Also, the microstructure by thermal history was analyzed. Experimental alloy showed high intergranular corrosion rate and its corrosion mechanism was elucidated.

Display 제조공정 배출가스 처리를 위한 휘발성 유기화합물 전처리 장치 개발 (Development of Volatile Organic Compound Pretreatment Device for Removing Exhaust Gas from Display Manufacturing Process)

  • 문기학;김재용
    • 공업화학
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    • 제30권5호
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    • pp.523-529
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    • 2019
  • 본 연구에서는 최근 반도체 및 display 산업이 발달함에 따라 문제가 되고 있는 휘발성 유기화합물의 전처리에 관해 조사하였다. 일반적인 VOCs 처리 설비인 직접연소장치에 사용되는 농축기는 display 제조 공정 내 배출가스에 의해 쉽게 오염되어 성능저하를 일으키며 결과적으로 VOCs의 처리 효율을 떨어뜨린다. 배출가스 성분 분석 결과 고비점, 고점도, 고분자량의 Alcohol류 및 Oil 성분이 다량 검출되었다. 이에 전처리 설비 내 열교환기를 이용하여 농축기 성능저하 물질을 응축시켜 처리하고자 하였고, 대부분의 물질을 90% 이상 처리하였다. 또한 열교환기에서 재 비산되는 고분자 Oil 등은 후처리 설비로 Grease Filter를 장착하여 대부분 처리할 수 있는 것으로 확인되었다.

비재내형(非在來型) 원유(原油) 자원(資源)으로서의 오일셰일 특성(特性) 고찰(考察) (Characteristics of Oil Shale as Unconventional Oil Resources)

  • 나정걸;정수현
    • 자원리싸이클링
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    • 제17권6호
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    • pp.62-67
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    • 2008
  • 오일셰일은 유기물질인 케로젠을 함유한 암석으로 레토르팅을 통하여 암석 내부의 케로젠을 오일로 회수할 수 있다. 본 연구에서는 미국과 러시아산 오일셰일 시료에 대한 물성을 분석하고 레토르팅 실험을 수행함으로써 대체 원유로서의 활용가능성을 평가하였다. 열중량 분석 결과, 오일셰일은 케로젠 분해로 인한 유기물 배출과 $CaCO_3$ 분해로 인한 $CO_2$ 배출의 두 단계 열분해 과정을 거치는 것으로 조사되었다. 오일셰일 내 유기물은 수소/탄소비가 높아 레토르팅을 통하여 액체연료로 쉽게 회수할 수 있으며 Fischer assay 레토르팅에 의한 오일 회수율은 미국산이 12.7%, 러시아산이 18.5% 정도였다. 미국 및 러시아산 오일셰일로부터 회수한 셰일오일은 비중 및 비점이 재래형 원유보다 높아 정유시설 투입을 위해서 추가 업그레이딩 공정이 필요하지만 유황분 함량이 낮을뿐 아니라 바나듐과 니켈 등의 촉매독 성분이 미량이어서 후속 정제공정에 드는 비용은 적을 것으로 예상된다. 회수된 오일에 대하여 GC/MS 분석을 수행한 결과 미국산 세일오일은 파라핀 성분이 다량 존재하였고, 러시아산 세일오일은 주로 산소가 포함된 유기화합물이 많이 함유되어 있음을 알 수 있었다.