• Title/Summary/Keyword: bead formation

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Fabrication and Characterization of Flurbiprofen loaded Chitosan Beads for Periodontal Regeneration (치주조직 재생용 플루르비프로펜 함유 키토산 비드의 제조 및 용출특성)

  • Rhee, Su-Jin;Park, Yoon-Jeong;Lee, Seung-Jin;Chung, Chong-Pyoung
    • Journal of Pharmaceutical Investigation
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    • v.27 no.1
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    • pp.71-77
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    • 1997
  • With the aim of improving periodontal regeneration efficacy, as a biodegradable local drug delivery device, drug releasing chitosan beads were prepared. Chitosan beads were prepared through the formation of intermolecular or intramolecular ionic interaction bewteen chitosan and sodium tripolyphosphate and were loaded with flurbiprofen. The mean diameter of the beads was $250\;{\mu}m$. Drug loading efficiency was improved by regulating the pH of tripolyphosphate solution. The drug release kinetics mainly depended upon the hydrophobic properties of the flurbiprofen, that is, the release of flurbiprofen showed initial burst with rapid release for the first day followed by a levelling off of the release rate. However, the release rate could be controlled by the formulation factor including the pH, concentration of the tripolyphosphate solution, gelation time, drug contents. From these results, flurbiprofen loaded chitosan beads were anticipated as biodegradable local drug delivery devices for periodontal regeneneration.

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The Weldability of Primer-coated Steel for Shipbuilding by $CO_2$ Laser (조선용 Primer코팅강판의 $CO_2$레이저 용접성)

  • Park, Hyun-Joon;Kim, Jong-Do;Kim, Young-Sik
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.316-321
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    • 2003
  • The spatter and porosity could be occurred during $CO_2$ CW laser welding of Primer-coated Steel for Shipbuilding. This study has suggested an alternative idea by examining of weld-defect formation mechanism. The primer-coated plate has caused the spatter, humping bead and porosity and these are main part of the welding defect, attributed to the powerful vaporizing pressure of primer attached on the base metal. The zinc of primer has a boiling point that is the lower temperature than melting point of steel. Zinc va}X)f will build up at the interface between the two sheets and this tends to deteriorate the quality of the weld by ejecting weld material from lap position or leaving porosity. Therefore introducing a small gap clearance in the lap position, the zinc vapor could escape through it and sound weld beads can be acquired. In conclusion, we suggested the occurred and prevented mechanism of weld defects with searching the factor.

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Variable Polarity Arc Welding of Aluminum Thin Plate (가변 극성을 이용한 박판 알루미늄 아크 용접)

  • Cho, Jungho
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.13 no.2
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    • pp.89-93
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    • 2014
  • Variable polarity (VP) arc welding is known as an effective solution for aluminum thanks to the cleaning effect, which means oxide removal, during the DCEP (direct current electrode positive) period. In this research, VP GTAW (gas tungsten arc welding) is adopted for lap joint fillet welding of 3mm thickness 5052 aluminum alloy. Various welding currents and DCEP duty cycles are applied as welding conditions with a fixed welding speed to investigate the influence of DCEP characteristics on weld bead formation. Results show a tendency of higher heat input for higher DCEP duty cycle, which result does not follow conventional arc theory because it is known that DCEN (DC electrode negative) polarity is more efficient for heat input than is DCEP. This phenomenonhas recently been reported by several VP-GTA researchers and is still controversial because the mechanism of oxide removal is not yet clear except for the previous, well-known idea of "ion bombardment", which cannot explain the situation. Finally, proper usage conditions for VP-GTAW are suggested; then, further, related theoretical topics in the field of cathode physics are brieflyintroduced.

Use of Chitosan-TPP microsphere as a matrix for the encapsulation of somatic embryos of Capsicum annum var. grossum

  • Senarath, Wtpsk;Stevens, W.F.;Lee, Kui-Jae;Rehman, S.;Lee, Wang-Hyu
    • Proceedings of the Plant Resources Society of Korea Conference
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    • 2002.11b
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    • pp.52-52
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    • 2002
  • Chitosan is a key compound of shrimp waste. It is a biopolymer, which is widely used in the field of medical Sciences. Chitosan-TPP (Tripolyphosphate) complex has more or less similar physical properties as Ca-alginate which can be used for the production of synthetic seeds. Possibility of the use of Chitosan-TPP complex as a matrix for encapsulation of somatic embryos was tested against the Ca-alginate complex (2.5w/v Na-alginate, 100mM CaCl2 at pH 5.5). Somatic embryos grown in the induction medium (IM) were drawn into the viscous chitosan solution (1%) and mixed well by inverting the tube carefully. Then the mixture was dropped at regular intervals into the tripolyphosphate (TPP) solution kept on a magnetic stirrer for bead formation. Synthetic seeds formed were washed and transferred into the incubation medium, then allowed either to air-dry or freeze-dry.(중략)

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A Study on the Metal Transfer and Spatter Generation in High Current $CO_2$ Welding (고전류 $CO_2$용접에서의 금속이행 및 스패터 발생 현상에 관한 연구)

  • 김남훈;유회수;김희진;고진현
    • Journal of Welding and Joining
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    • v.21 no.3
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    • pp.51-57
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    • 2003
  • The metal transfer in $CO_2$ welding shows the transition of transfer mode from short-circuiting to repelled transfer will the increase of welding current. While the short-circuiting mode in $CO_2$ welding has been studied very extensively relating with droplet formation and spatter generation, the repelled transfer has little been understood. In this study, high current $CO_2$ welding has been performed with bead-on-plate welds along with the waveform analyzer and high speed camera. The image of high speed camera was synchronized with its waveform so that the moment of spatter generation could be realized during drop detachment. As a results of this study, it was found that welding arc changes its location either once or three times and thus single or double pulse signals were developed in the voltage waveform. Whenever the arc moved its location, new arc was developed in a explosive way and thus it caused spatter generation. Specially severe spattering took place when the waveform showed a double-peak pattern. As a consequence of these results, new waveform control techniques could be suggested for suppressing the spatter generation in the high-current $CO_2$ welding.

Bead Formation and Wire Temperature Distribution during Ultra-high-speed GTA Welding Using Pulse-heated Hot-wire

  • Shinozaki, K.;Yamamoto, M.;Mitsuhata, Koichi;Nagashima, Toshiharu;Kanazawa, T.;Arashin, H.
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.226-234
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    • 2009
  • The purpose of this study was to investigate the melting phenomenon of filler wire in detail and to obtain the precise temperature distribution of filler wire during GTA welding under the ultra-high welding speed condition in order to develop the ultra-high-speed GTA welding process with the pulse-heated hot-wire system by using three kinds of materials. The melting phenomenon of filler wire was observed using a high-speed camera and the temperature distribution of filler wire was measured using a radiation thermometer. From the above result, the adequate welding conditions of each material to make the GTA welding process with the ultra-high welding speed could be obtained. The ultra-high-speed GTA welding process needed the adequate wire current in order to obtain the adequate temperature distribution and the adequate melting position of filler wire. Moreover, the temperature distributions of three kinds of filler wire could be estimated by using the proposed simple estimation method.

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Numerical Simulation of Bubble and Pore Generations by Molten Metal Flow in Laser-GMA Hybrid Welding (레이저-GMA 하이브리드 용접에서 유동에 의한 기포 및 기공 형성 해석)

  • Cho, Won-Ik;Cho, Jung-Ho;Cho, Min-Hyun;Lee, Jong-Bong;Na, Suck-Joo
    • Journal of Welding and Joining
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    • v.26 no.6
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    • pp.67-73
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    • 2008
  • Three-dimensional transient simulation of laser-GMA hybrid welding involving multiple physical phenomena is conducted neglecting the interaction effect of laser and arc heat sources. To reproduce the bubble and pore formations in welding process, a new bubble model is suggested and added to the established laser and arc welding models comprehending VOF, Gaussian laser and arc heat source, recoil pressure, arc pressure, electromagnetic force, surface tension, multiple reflection and Fresnel reflection models. Based on the models mentioned above, simulations of laser-GMA hybrid butt welding are carried out and besides the molten pool flow, top and back bead formations could be observed. In addition, the laser induced keyhole formation and bubble generation duo to keyhole collapse are investigated. The bubbles are ejected from the molten pool through its top and bottom regions. However, some of those are entrapped by solid-liquid interface and remained as pores. Those bubbles and pores are intensively generated when the absorption of laser power is largely reduced and consequently the full penetration changes to the partial penetration.

The characteristic of penetration on the 800Mpa class high-tensile steel using remote welding system by $CO_2$ laser ($CO_2$ 레이저 원격 용접시스템을 이용한 800Mpa급 고장력강의 용입특성)

  • Song, M.J.;Lee, Y.J.;Song, Y.C.;Jung, S.M.;Jung, B.H.;Lee, M.Y.
    • Proceedings of the Korean Society of Laser Processing Conference
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    • 2006.11a
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    • pp.17-20
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    • 2006
  • In the remote welding system using $CO_2$ laser, laser beam is rapidly deflected by moving mirrors of scanner system and has focusable distance over 1000mm from workpiece. From such arrangement, various advantages and disadvantages arise. Remote welding is a highly efficient laser process. As the mirrors of the scanner system allow positioning speeds exceeding 700m/s, it becomes possible to reduce the welding cycle time. On the other hand, as there no the provision of shielding gas which is normally required for beam powers exceeding 3kW, may become difficult task. Therefore, In this study, the influence of the various penetration of back bead by the different laser welding speed on the weld seam formation without shielding gas was investigated.

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A Study on Locally Drying Underwater Welding (국부건식(물커튼식)수중용접법에 관한 연구)

  • 이규복;황선효;박영조;김종열
    • Journal of Welding and Joining
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    • v.10 no.2
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    • pp.51-62
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    • 1992
  • A torch was designed and fabricated in order to develope the technology of "locally drying underwater welding" by water curtain method. The condition for the formation of the possible local cavity, the mechanical properties and the thermal cycle of welds were investigated in the developed welding equipment compared with in-air welding. The possibility of highly reliable and practical underwater welding was found. The proper local cavity was formed above the water flowrate of 30l/min and CO$_{2}$ gas flowrate of 100l/min. The bead width and penetration depth were increased with increasing welding current. The hardness of weldments is about 160Hv in air welding, but about 210Hv in underwater welding. The elongation and the impact value of underwater weldments are 15% and 6Kg/cm$^{2}$ respectively, which are only half as much as the values of in-air welding. The cooling time in the temperature range from 800.deg.C to 500.deg.C affecting the structure and the hardness of weldments is about 22sec. in air welding while about 10sec. in underwater welding.r welding.

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Improvement of Organics and Nitrogen Removal by HRT and Recycling Rate in Air Lift Reactors (공기부상반응조에서 체류시간과 반송율에 의한 유기물질 및 질소제거 향상에 관한 연구)

  • Kim, Jin-Ki;Yu, Sung-Whan;Lim, Bong-Su
    • Journal of Korean Society on Water Environment
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    • v.22 no.1
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    • pp.45-50
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    • 2006
  • This study was performed to evaluate the air lift reactors (ALR) by variations of HRT and recycling rate. Air lift reactor was composed of bioreactor and clarifier above it. To remove organic matters and nitrogen through the formation of microbic film and filtration, bio-filter reactors were filled with clay, glass, bead, waste plastic, respectively. Influent wastewater was fed to biofilter reactor, and effluent wastewater from bio-filter reactor was injected ALR again, instead of adding external carbon source. Effluent BOD concentration was satisfied with lower than 10 mg/L in recycling rate 100% regardless of the variation of HRT and the kinds of media materials. In HRT 4 hr, recycling rate 100%, BOD removal efficiency rate was from about 85 to 90%, COD removal efficiency rate was higher than 90%. Effluent TN concentration was satisfied with less than 20 mg/L, if HRT was maintained by over than 6 hr regardless of recycling rate and media materials. Over than HRT was 4 hr, microbes concentration in air lift reactor was maintained over than 2,500 mg/L constantly, not sensitive to environmental condition, and organic removal was effective as it was higher.