• Title/Summary/Keyword: average particle diameter

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The Model and Experiment for Heat Transfer Characteristics of Nanoporous Silica Aerogel

  • Mingliang, Zheng
    • Korean Journal of Materials Research
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    • v.30 no.4
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    • pp.155-159
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    • 2020
  • Nanoporous silica aerogel insulation material is both lightweight and efficient; it has important value in the fields of aerospace, petrochemicals, electric metallurgy, shipbuilding, precision instruments, and so on. A theoretical calculation model and experimental measurement of equivalent thermal conductivity for nanoporous silica aerogel insulation material are introduced in this paper. The heat transfer characteristics and thermal insulation principle of aerogel nano are analyzed. The methods of SiO2 aerogel production are compared. The pressure range of SiO2 aerogel is 1Pa-atmospheric pressure; the temperature range is room temperature-900K. The pore diameter range of particle SiO2 aerogel is about 5 to 100 nm, and the average pore diameter range of about 20 ~ 40 nm. These results show that experimental measurements are in good agreement with theoretical calculation values. For nanoporous silica aerogel insulation material, the heat transfer calculation method suitable for nanotechnology can precisely calculate the equivalent thermal conductivity of aerogel nano insulation materials. The network structure is the reason why the thermal conductivity of the aerogel is very low. Heat transfer of materials is mainly realized by convection, radiation, and heat transfer. Therefore, the thermal conductivity of the heat transfer path in aerogel can be reduced by nanotechnology.

Ag-Cu Powders Prepared by Electrical Wire Explosion of Cu-plated Ag Wires (동도금한 은선재의 전기선폭발에 의해 제조한 Ag-Cu분말)

  • Kim, Won-Baek;Park, Je-Shin;Suh, Chang-Youl
    • Journal of Powder Materials
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    • v.14 no.5
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    • pp.320-326
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    • 2007
  • Ag-Cu alloy nano powders were fabricated by the electrical explosion of Cu-plated Ag wires. Ag wires of 0.2mm diameter was electroplated to final diameter of 0.220 mm and 0.307 mm which correspond to Ag-27Cu and Ag-68Cu alloy. The explosion product consisted of equilibrium phases of ${\alpha}-Ag$ and ${\beta}$-Cu. The particle size of Ag-Cu nano powders were 44 nm and 70 nm for 0.220 mm and 0.307 mm wires, respectively. The Ag-Cu nano powders contained less Cu than average value due to higher sublimation energy compared to that of Ag. As a result, micron-sized spherical particles formed from liquid droplets contained higher Cu content.

Impact Resistance of Al2O3-SiC Composites Against High Velocity Copper Jet (고속 구리제트에 대한 알루미나-탄화규소 복합재료의 충돌 저항물성)

  • Kim, Chang-Wook;Lee, Hyung-Bock
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.660-665
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    • 2006
  • The mechanical properties of $Al_2O_3$-SiC composites manufactured with adding various amount and size of SiC particles have been measured and analyzed. Generally, the elastic modulus of the composites shows about 50% less than that of PL-8 (45 wt% $Al_2O_3$-51 wt% $SiO_2$-4 wt% other oxides), but the flexural strength is similar with each other. The impact resistance property of $Al_2O_3$-SiC composite against high velocity copper jet was lower than that of PL-8 when SiC particles of approximately 3 $\mu$m diameter was added to. It is caused probably due to the micro-pores made by oxidation of SiC particles. However, in the case of the less-weighted $Al_2O_3$-SiC composite adding to 10 wt% SiC with average diameter of 10 $\mu$m and sintering at 1200$^{\circ}C$, the impact resistance property was improved up to 37 percent compared with that of PL-8.

Synthesis and characterization of the ultrafine $ZnFe_2O_4$ powder by glycothermal (Glycothermal에 의한 초미립의 $ZnFe_2O_4$분말 합성 및 특성)

  • Bae, Dong-Sik;Han, Kyong-Sop;Cho, Seung-Beom;Choi, Sang-Hael
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.1
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    • pp.167-173
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    • 1997
  • The $ZnFe_2O_4$ powder was prepared under glycothermal conditions by precipitation from metal nitrates with aqueous potassium hydroxide. The fine powder was obtained at temperatures as low as 225 to $300^{\circ}C$. The microstructure and phase of the $ZnFe_2O_4$ powder were studied by SEM and XRD. The properties of the powder were studied as a function of various parameters (reaction temperature, reaction time, solid loading, etc). The average particle size of the $ZnFe_2O_4$ increased with increasing reaction temperature. After glycothermal treatment at $270^{\circ}C$ for 8 h, the average particle diameter of the $ZnFe_2O_4$ was about 50 nm.

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Characteristics of Particulate Matter Generated during the Operation of a Small Directly Fired Coffee Roaster (소형 직화식 커피 로스터 이용 시 발생하는 미세먼지 특성 연구)

  • Yu, Da Eun;Kim, Seung Won
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.30 no.2
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    • pp.236-248
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    • 2020
  • Objectives: The purpose of this study was to evaluate the concentrations of particulate matter generated during coffee roasting and to study various factors affecting the concentrations. Methods: Differences in concentration levels were investigated based on various factors to understand the emission rates of particulate matter over time and to compare the mass and number concentrations according to their size. Sampling was performed in closed laboratories without the operation of air conditioning or ventilation. Optical Particle Sizer(OPS) was used as a measuring device. An OPS measures using a light-scattering method. Sampling was performed for sixty minutes at one-minute intervals. The background concentration was measured for about 30 minutes before starting of coffee roasting. The concentrations of particulate matter generated during coffee roasting were monitored until roasted coffee beans were removed from the roaster and cooled down. Several factors affecting the concentrations of particulate matter were investigated, which includes the origins of green beans, the roasting level, and the input amount of green beans. Results: The results of this study may be summarized as follows: 1) There was no difference in particulate matter concentration levels by the origin of the green beans, but a statistically significant difference in concentration levels by roasting level and the input amount of green beans; The higher the roasting level, the higher was the particulate matter concentration. The more green beans we put in the roaster, the higher were the concentrations; 2) The PM10 mass concentrations increased over time. The average concentration after roasting was higher than the average concentration during roasting; 3) In the distribution of mass and number concentration by particle diameter, the majority of particles was below 2.5 ㎛. Conclusions: Persons who work in roastery cafes can be exposed to high concentrations of particulate matter. Therefore, personal exposure and risk assessment should be conducted for roastery cafe workers.

Dispersion Polymerization of Acrylamide in the Media of t-Butyl Alcohol/$H_2O$ Mixtures (t-Butyl Alcohol/$H_2O$ 혼합 용매에서 아크릴아미드의 분산중합)

  • 이기창;이성은;송봉근;이동주
    • Polymer(Korea)
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    • v.24 no.5
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    • pp.629-637
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    • 2000
  • Dispersion polymerization of acrylamide in the media of t-butyl alcoho1/$H_2O$ mixtures at 30~5$0^{\circ}C$ in the presence of hydroxypropyl cellulose and ammonium persulfate as steric stabilizer and initiator, respectively, was carried out. It was studied the effects of concentrations of initiator and steric stabilizer, amount of monomer, polymerization temperature, t-butyl alcohol/$H_2O$ ratio, concentration of crosslinker, purification of monomer and nitrogen purge on the particle size of the resulting acrylamide latices and molecular weight of the latex-poly(acrylamide). In this study, poly(acrylamide) latices of 0.1~0.5 ${\mu}{\textrm}{m}$ with 470000~2080000 in (equation omitted) were prepared and the resulting PAM latices were all dissolved in water in stantly.

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Preparation of Monosized Titanium Dioxide Powder from TEOT (TEOT로부터 TiO₂단분산 분말 합성에 관한 연구)

  • 안영필;최석홍
    • Journal of the Korean Ceramic Society
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    • v.25 no.5
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    • pp.50-50
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    • 1988
  • The controlled Ti(CO2H5)4 hydrolysis reactions for the synthesis of Spherical Monodispersed Titania powders are described. Increasing the concentration of TEOT and the molar ratio of water to TEOT in alcohol solution decrease the reaction time and the particle size. The reaction time is delalyed by increasing the chain length and the number of carbon branches of alcohol as a solvent. The prepared powders with an average diameter of 0.8μ and the spherical monodispersed transfer to Rutile phase at 550℃.

Continuous Processing of Monodispersed Zirconia Powders (초음파 혼합 연속공정에 의한 단분산 지르코니아 분체의 합성)

  • Rhee, Jhun;Jo, Dong-Soo
    • Journal of the Korean Ceramic Society
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    • v.29 no.12
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    • pp.919-925
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    • 1992
  • Continuous synthesis process for monodispersed zirconia powders with ultrasonic wave mixing was developed. Reactant solutions were flowed through a T-tube with small diameter and then mixed in a microscale with ultrasonification. Reaction and aging were followed during the mixed solution of reactants is in plug flowing through a narrow long teflon tubing. Zr(n-OC4H9)4 in ethanol and H2O in ethanol were used as reactants. From this process monodispersed, spherical, non-agglomerated, singlet hydrated zirconia powders with 0.6 $\mu\textrm{m}$ average size were obtained. Geometrical standard deviation of the particle size distribution was less than 1.2 with ultrasonic mixing, and the geometrical standard deviation was not affected by the flow rate of the reactants.

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HYDRAULIC ANALYSIS OF OXYGEN TRANSFER THROUGH AIR ENTRAINMENT IN RIPARIAN RIFFLES

  • Kim, Jin-Hong
    • Water Engineering Research
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    • v.4 no.3
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    • pp.127-139
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    • 2003
  • This paper presents the hydraulic analysis of the oxygen transfer through the air entrainment and the relationships between the efficiency of the oxygen transfer and the hydraulic parameters in the riparian riffles. Field survey on the pool-riffle formation of the river reach and the measurements of the oxygen transfer in the riffles were performed. Air entrainment occurred more frequently in the edged gravels rather than in the round and edgeless ones, and it was formed mainly from behind the trailing edges of the gravels. Oxygen transfer was found to be proportional to the flow velocity, the flow discharge, and the Froude number, but to be not closely related to the particle diameter. Average value of oxygen transfer in the riffles of study area was about 0.085, which shows good efficiency compared with results of smooth chute. Variation of the water level, which increases in proportion to the flow velocity and the flow discharge, seems to make the air entrainment more active, but has not been verified quantitatively. Relationships between the air entrainment and the variation of the water level must be considered in the further study.

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Characteristics of Anion Concentration Distributions in Airbone Fine Particles in Urban Atmosphere (도시대기 중에 부유하는 미세입자중 음이온의 농도분포 특성)

  • 천만영;조기철;여현구
    • Journal of Korean Society for Atmospheric Environment
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    • v.13 no.1
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    • pp.1-7
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    • 1997
  • Anion concentrations and distributions of airborne fine particles less than 2 $\mu$m in urban atmosphere were determined from Feb. 5 to 16, 1996. The sampling was carried out using 8 stages Hering's low pressure impactor (LPI, aerodynamic cutoff diameters are 0.05, 0.075, 0.11, 0.26, 0.50, 1.0, 2.0, and 4.0$\mu$m) on the top of a five-story building located at Kon-Kuk university in Seoul. Average concentrations if C $l^{[-10]}$ , N $O_3$$^{[-10]}$ and S $O_4$$^{2-}$ were 9.4, 8.4, and 14.5 $\mu\textrm{g}$/㎥, respectively. The distributions of these anion concentrations were bimodal types which showed two peaks in the range of 0.075~0.12 ${\mu}{\textrm}{m}$ and 0.5~1 ${\mu}{\textrm}{m}$ in aerodynamic diameter. These results were 2.5~4.7 times higher than anion concentrations collected by Anderson low volume air sampler.

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