• Title/Summary/Keyword: analytical testing

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Accelerated SCC Testing of Stainless Steels According to Corrosion Resistance Classes

  • Borchert, M.;Mori, G.;Bischof, M.;Tomandl, A.
    • Corrosion Science and Technology
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    • v.14 no.6
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    • pp.280-287
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    • 2015
  • The German Guidelines for stainless steel in buildings (Z.30.3-6) issued by the German Institute for Building Technology (DIBt) categorizevarious stainless steel grades into five corrosion resistance classes (CRCs). Only 21 frequently used grades are approved and assigned to these CRCs. To assign new or less commonly used materials, a large program of outdoor exposure tests and laboratory tests is required. The present paper shows theresults of stress corrosion cracking (SCC) tests that can distinguish between different CRCs. Slow strain rate tests (SSRT) were performedin various media and at different temperatures. CRC IV could be distinguished from CRC II and CRC III with a 31.3 % $Cl^-$ as $MgCl_2$ solutionat $140^{\circ}C$. CRC II and CRC III could be differentiated by testing in a 30% $Cl^-$ as $MgCl_2$ solutionat $100^{\circ}C$.

Bearing Modeling of Superconducting Magnetic Bearings-Flywheel System (초전도 자기베어링-플라이휠 시스템의 베어링 모델링)

  • 김정근;이수훈
    • Journal of KSNVE
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    • v.9 no.5
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    • pp.891-898
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    • 1999
  • The purpose of Superconducting Magnetic Bearing Flywheel Energy Storage System (SMB-FESS) is to store unused nighttime electricity until it is needed during daytime. An analytical model of the SMB-FESS is necessary to identify the system behavior. At first, we have to model the superconducting magnetic bearing. Modeling the SMB is same as estimating the bearing parameter. The theoretical modal parameter is calculated through the equation of motion and the experimental modal parameter is estimated through the impact testing (modal testing). The bearing parameter is searched by using the non-linear least square method until the theoretical result corresponds to the experimental result. The suggested modeling method is verified by comparing experimental and analytical frequency response function.

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Flexural behavior of partially-restrained semirigid steel connections

  • Campione, G.;Scibilia, N.
    • Steel and Composite Structures
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    • v.1 no.4
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    • pp.441-458
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    • 2001
  • We analyzed the experimental and theoretical behavior of a particular type of steel joint designed to connect beam to beam and able to transfer both shear forces and bending moments. This joint is characterized by the use of steel plates and bolts enclosed in the width of the beams. The experimental investigation was carried out characterizing the constituent materials and testing in flexure beams constituted by two portions of beams connected in the middle with the joint proposed. Connections having different characteristics in terms of thickness of plates, number and type of bolts were utilized. Flexure tests allow one to determine the loaddeflection curves of the beam tested and the moment-rotation diagrams of the connections, highlighting the strength and the strain capacity of the joints. The proposed analytical model allows one to determine the moment-rotation relationship of the connections, pointing out the influence of the principal geometrical and mechanic characteristics of single constituents on the full properties of the joint.

Assessment of load carrying capacity and fatigue life expectancy of a monumental Masonry Arch Bridge by field load testing: a case study of veresk

  • Ataei, Shervan;Tajalli, Mosab;Miri, Amin
    • Structural Engineering and Mechanics
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    • v.59 no.4
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    • pp.703-718
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    • 2016
  • Masonry arch bridges present a large segment of Iranian railway bridge stock. The ever increasing trend in traffic requires constant health monitoring of such structures to determine their load carrying capacity and life expectancy. In this respect, the performance of one of the oldest masonry arch bridges of Iranian railway network is assessed through field tests. Having a total of 11 sensors mounted on the bridge, dynamic tests are carried out on the bridge to study the response of bridge to test train, which is consist of two 6-axle locomotives and two 4-axle freight wagons. Finite element model of the bridge is developed and calibrated by comparing experimental and analytical mid-span deflection, and verified by comparing experimental and analytical natural frequencies. Analytical model is then used to assess the possibility of increasing the allowable axle load of the bridge to 25 tons. Fatigue life expectancy of the bridge is also assessed in permissible limit state. Results of F.E. model suggest an adequacy factor of 3.57 for an axle load of 25 tons. Remaining fatigue life of Veresk is also calculated and shown that a 0.2% decrease will be experienced, if the axle load is increased from 20 tons to 25 tons.

Isolation of Humic Acid from Water (물 중의 Humic Acid 분리)

  • Yook, Keun-Sung;Kim, Yong-Hwa
    • Analytical Science and Technology
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    • v.9 no.1
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    • pp.118-121
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    • 1996
  • 56.2% of Aldrich HA was recovered from water by XAD-8 and AGMP-50 procedure. With this method, 0.58mg/l of HA was determined in the water collected from irrigation reservoir near Tae Dok Science Town. For the removal of ash from Aldrich HA, centrifugation was simple, but as effective as dialysis. Neither centrifugation nor dialysis removed Na at all. Only with XAD-8 and AGMP-50 procedure, Na and ash were completely removed.

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A rapid assessment methodology for bridges damaged by truck strikes

  • Stull, C.J.;Earls, C.J.
    • Steel and Composite Structures
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    • v.9 no.3
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    • pp.223-237
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    • 2009
  • The present research aims to develop a methodology to rapidly assess bridges with damage to the superstructure, caused by overheight trucks or lower-than-average overhead clearance. Terrestrial laser scanning and image processing techniques are combined with the finite element method to arrive at an analytical model which is more accurate, with respect to the complex geometrical aspects of the bridge in its damaged configuration. ""Virtual load testing"" may subsequently be carried out on this analytical model to determine the reserve capacity of the structure in an objective manner.

Estimation on the application of Reference Materials for PCBs Proficiency Testing from the transformer oil (폐절연유를 이용한 숙련도 평가용 PCBs 표준물질의 적용성 평가)

  • Kim, Woo-Il;Kwon, Myung-Hee;Jeon, Tae-Wan;Kim, Dong-Hoon;Chun, Jin-Won;Sim, Ki-Tae;Yeon, Jin-Mo
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.247-254
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    • 2010
  • This study was carried out to produce Reference Materials (RMs) for Proficiency Testing (PT) of PCBs in waste analytical laboratories. Two RMs were prepared from used transformer oil samples and PCB free transformer oil by spiking PCBs standard solutions. The spiked PCB RMs were homogenized by mixing and settling up to 90 days. Homogenized concentration of PCBs with Arochlor 1254 (6 ppm), 1254:1260 (1:1) (5 ppm) were observed in 60 days stationary phase but Arochlor 1260 (3.5 mg/L) were observed in 90 days stationary phase. One-way ANOVA test were carried out and showed that the RMs were suitably homogenized, which can be used for proficiency testing. The Relative Standard Deviations (RSDs) of analytical results were 3.51~5.01% for the PCBs RMs in 10 replicates. The expanded uncertainty of PCBs analytical procedure were 0.26~0.49.

Quality Control System for Analytical Chemistry Laboratory of Pesticide Products (농약 이화학시험 분석기관 정도관리체계)

  • Chang, Hee-Ra;Lee, Joon-Yeob;Lee, Young-Ju;Kang, Hye-Rim;Kim, Chan-Sub;Kim, Kyun
    • The Korean Journal of Pesticide Science
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    • v.15 no.4
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    • pp.529-544
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    • 2011
  • Many international organizations, such as the International Organization for Standardization (ISO) and Collaborative International Pesticide Analytical Council (CIPAC), have published a guide to quality control requirements, proficiency testing and method validation for pesticide formulation. In general, proficiency testing is to determine the performance of individual laboratories from the comparison of test results and to monitor a laboratory's performance abilities. One of quality assurance (QA) scheme would be include the validation of analytical method that implies a performance characteristics, specificity, selectivity, linearity and so on. According to many international organizations, the quantification methods of active substance in formulated pesticide products are required to be reproducible, accurate and precise. This study was conducted to compare the international guidelines for the quality control, proficiency testing and method validation of analytical laboratories and to propose a general guidance for the establishment of quality control system in the analytical chemistry laboratories of pesticide formulation in domestic.

Interlaboratory Study for Proficiency Testing on the Water Toxicity Determinations by Acute Toxicity Test with Daphnia magna (국내 생태독성 분석기관에 대한 숙련도시험 결과 평가)

  • Kim, Jongmin;Shin, Kisik;Yu, Soonju;Kim, Myeong Ock;Choe, Sung Hun
    • Journal of Korean Society on Water Environment
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    • v.30 no.6
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    • pp.632-637
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    • 2014
  • Proficiency testing by interlaboratory comparisons is used to determine the performance of individual laboratories. In order to verify the quality of acute toxicity testing with Daphnia magna, National Institute of Environmental Research in South Korea is regularly organizing interlaboratory comparisons to estimate the analytical accuracy of different laboratories. Total 58 laboratories located in South Korea took part in interlaboratory proficiency testing scheme with three proficiency testing samples. TU(Toxic Unit) values of each laboratory were determined and robust z-score was calculated in order to evaluate the proficiency levels. Based on the robust z-score classification, 74% of the participant laboratories showed a satisfactory performance (43 laboratories). The main reason of 'unsatisfactory' performance seemed to be considered that the unsuitable management of test organism incubation system and the lack of experience on the identification of the test organism condition by effect of toxicity.