• 제목/요약/키워드: analytical testing

검색결과 447건 처리시간 0.023초

한국어 퍼지 언어변수를 이용한 리스크 평가의 논리적 일관성 (Logical Consistency in Risk Assessment using the Korean Fuzzy Linguistic Variables)

  • 임현교;변상훈
    • 한국안전학회지
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    • 제31권4호
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    • pp.120-125
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    • 2016
  • Usually, a risk can be expressed as a product of likelihood and consequence of a hazard factor. Therefore, conventional risk assessment is carried out by frequency analysis and severity analysis, in turns. However, it is well known that intuitive thinking is another excellent way of thinking of human beings. This study aimed to confirm whether there exist any difference in risk assessment results derived by two different procedures - intuitive and analytical. Thus, the present study showed 10 different illustrations to 30 undergraduate students. Their responses were organized as fuzzy membership functions, and summarized as risk assessments, and compared. The results were also verified with the help of statistical hypothesis testing, which showed no significant difference. On the contrary, however, similarity measure used in fuzzy set theory was not credible as anticipated. Many cases failed to satisfy statistical hypothesis even with similarity measure higher than 0.60 so that only a trend could be accepted. In addition, a subject showed a somewhat consistent logical discrepancy in his response, which implied the necessity of sincere analysis in fuzzy formulations.

청석면 분석 정도관리용 표준시료 개발 및 평가 (Development and Validation of Crocidolite Quality Control Samples for Proficiency Analytical Testing)

  • 이지현;김은영;노수진;박용진;정지연
    • 한국환경보건학회지
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    • 제37권1호
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    • pp.57-63
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    • 2011
  • Crocidolite quality control (QC) sampling created by the wet generation method has been validated by validation tests such as the accuracy, precision, and storage tests. For this study we designed and developed a manufacturing apparatus and standard operating procedure for making these QC samples. The most important step in the procedure of making QC samples was the stage eliminating static electricity in asbestos fibers. This static electricity hampers the fibers clog functioning. In accuracy and precision tests by phase contrast microscopy analysis, the difference between the reference values and the studied values was at maximum 17.8%. This satisfies the AIHA proficiency analytical test criteria for asbestos. We could confirm the nearly even distribution of crocidolite fibers on the membrane filter. Also, there was no loss of fibers in the storage test after the one month.

산소공장 공기터보압축기(ATC)의 회전체동역학 설계특성 분석 및 진동저감 (Analysis of Rotordynamic Design Characteristics and Vibration Reduction of an Air Turbo Compressor for Oxygen Plant)

  • 김병옥;이안성
    • 한국유체기계학회 논문집
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    • 제13권3호
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    • pp.43-48
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    • 2010
  • In this study rotordynamic characteristics of an air turbo-compressor (ATC) used in oxygen plant are analyzed and its operating-speed balancing is performed to solve the vibration trouble caused by rotor unbalance. Three dimensional model of the ATC rotor is completed and then analytical FE (finite element) model, which is verified by experimental modal testing, is developed. A rotordynamic analysis includes the critical map, Campbell diagram, and unbalance response, especially considering the pedestal housings supporting tilting pad bearings. A test run of operating-speed, using tilting-pad bearing of actual use, showed that the vibration level increased very sharply as approaching the rated speed. The operating-speed balancing specified by API 684 was carried out by using influence coefficient method. The results showed that the vibrations at the bearing pedestal housings represented good levels of 0.1 mm/s. From the test run and operating-speed balancing, the analytical results, that is, critical speeds are in good agreement with the test results and unbalance responses introducing the correction masses are similar to the as-is test responses in its aspect.

Fast analytical estimation of the influence zone depth, its numerical verification and FEM accuracy testing

  • Kuklik, Pavel;Broucek, Miroslav;Kopackova, Marie
    • Structural Engineering and Mechanics
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    • 제33권5호
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    • pp.635-647
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    • 2009
  • For the calculation of foundation settlement it is recommended to take into account so called influence zone inside the subsoil bellow the foundation structure. Influence zone inside the subsoil is the region where the load has a substantial influence on the deformation of the soil skeleton. The soil skeleton is pre-consolidated or over consolidated due to the original geostatic stress state. An excavation changes the original geostatic stress state and it creates the space for the load transferred from upper structure. The theory of elastic layer in Westergard manner is selected for the vertical stress calculation. The depth of influence zone is calculated from the equality of the original geostatic stress and the new geostatic stress due to excavation combined with the vertical stress from the upper structure. Two close formulas are presented for the influence zone calculation. Using ADINA code we carried out several numerical examples to verify the proposed analytical formulas and to enhance their use in civil engineering practice. Otherwise, the FEM code accuracy can be control.

Developments of double skin composite walls using novel enhanced C-channel connectors

  • Yan, Jia-Bao;Chen, An-Zhen;Wang, Tao
    • Steel and Composite Structures
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    • 제33권6호
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    • pp.877-889
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    • 2019
  • The developments of double skin composite (DSC) walls with novel enhanced C-channel connectors (DSCW-EC) were reported. Followed axial compression tests on prototype walls were carried to evaluate structural performances of this novel DSC composite structures. The testing program consists of five specimens and focused on the layout of the novel enhanced C-channel (EC) connectors, which include the web direction of C-channels, steel-faceplate thickness, vertical and horizontal spacing of C-channels. Crushing in concrete core and buckling of steel faceplate were two main observed failed modes from the compression tests. However, elastic or plastic buckling of the steel faceplate varies with designed parameters in different specimens. The influences of those investigated parameters on axial compressive behaviors of DSCW-ECs were analyzed and discussed. Recommendations on the layout of novel EC connectors were then given based on these test results and discussions. This paper also developed analytical models for predictions on ultimate compressive resistance of DSCW-ECs. Validation against the reported test results show that the developed theoretical models predict well the ultimate compressive resistance of DSCW-ECs.

Rapid Determination of L-carnitine in Infant and Toddler Formulas by Liquid Chromatography Tandem Mass Spectrometry

  • Ahn, Jang-Hyuk;Kwak, Byung-Man;Park, Jung-Min;Kim, Na-Kyeoung;Kim, Jin-Man
    • 한국축산식품학회지
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    • 제34권6호
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    • pp.749-756
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    • 2014
  • A rapid and simple analytical method for L-carnitine was developed for infant and toddler formulas by liquid chromatography tandem mass spectrometry (LC-MS/MS). A 0.3 g of infant formula and toddler formula sample was mixed in a 50 mL conical tube with 9 mL water and 1 mL 0.1 M hydrochloric acid (HCl) to chemical extraction. Then, chloroform was used for removing a lipid fraction. After centrifuged, L-carnitine was separated and quantified using LC-MS/MS with electrospray ionization (ESI) mode. The precursor ion for L-carnitine was m/z 162, and product ions were m/z 103 (quantitative) and m/z 85 (qualitative), respectively. The results for spiked recovery test were in the range of 93.18-95.64% and the result for certified reference material (SRM 1849a) was within the range of the certificated values. This method could be implemented in many laboratories that require time and labor saving.

Characteristic analysis on train-induced vibration responses of rigid-frame RC viaducts

  • Sun, Liangming;He, Xingwen;Hayashikawa, Toshiro;Xie, Weiping
    • Structural Engineering and Mechanics
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    • 제55권5호
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    • pp.1015-1035
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    • 2015
  • A three-dimensional (3D) numerical analysis for the train-bridge interaction (TBI) system is actively developed in this study in order to investigate the vibration characteristics of rigid-frame reinforced concrete (RC) viaducts in both vertical and lateral directions respectively induced by running high-speed trains. An analytical model of the TBI system is established, in which the high-speed train is described by multi-DOFs vibration system and the rigid-frame RC viaduct is modeled with 3D beam elements. The simulated track irregularities are taken as system excitations. The numerical analytical algorithm is established based on the coupled vibration equations of the TBI system and verified through the detailed comparative study between the computation and testing. The vibration responses of the viaducts such as accelerations, displacements, reaction forces of pier bottoms as well as their amplitudes with train speeds are calculated in detail for both vertical and lateral directions, respectively. The frequency characteristics are further clarified through Fourier spectral analysis and 1/3 octave band spectral analysis. This study is intended to provide not only a simulation approach and evaluation tool for the train-induced vibrations upon the rigid-frame RC viaducts, but also instructive information on the vibration mitigation of the high-speed railway.

Flexural ductility of reinforced HSC beams strengthened with CFRP sheets

  • Hashemi, Seyed Hamid;Maghsoudi, Ali Akbar;Rahgozar, Reza
    • Structural Engineering and Mechanics
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    • 제30권4호
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    • pp.403-426
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    • 2008
  • Externally bonding fiber reinforced polymer (FRP) sheets with an epoxy resin is an effective technique for strengthening and repairing reinforced concrete (RC) beams under flexural loads. Their resistance to electro-chemical corrosion, high strength-to-weight ratio, larger creep strain, fatigue resistance, and nonmagnetic and nonmetallic properties make carbon fiber reinforced polymer (CFRP) composites a viable alternative to bonding of steel plates in repair and rehabilitation of RC structures. The objective of this investigation is to study the effectiveness of CFRP sheets on ductility and flexural strength of reinforced high strength concrete (HSC) beams. This objective is achieved by conducting the following tasks: (1) flexural four-point testing of reinforced HSC beams strengthened with different amounts of cross-ply of CFRP sheets with different amount of tensile reinforcement up to failure; (2) calculating the effect of different layouts of CFRP sheets on the flexural strength; (3) Evaluating the failure modes; (4) developing an analytical procedure based on compatibility of deformations and equilibrium of forces to calculate the flexural strength of reinforced HSC beams strengthened with CFRP composites; and (5) comparing the analytical calculations with experimental results.

필라멘트 와인딩 복합재료 연소관의 구조적 안정성 연구 (Analysis of filament Wounded Composite Rocket Motor)

  • 이윤규;권태훈;이원복
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2004년도 제23회 추계학술대회 논문집
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    • pp.278-281
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    • 2004
  • 본 논문의 목적은 KSLV-1 KM 축소형 연소관의 변형을 예측할 수 있는 효과적인 해석방법을 제시하는 것을 목적으로 하며, 내압을 받는 F/W 복합재 연소관에 대한 구조해석과 실험을 수행하였다. 효과적인 연소관의 해석을 위해 돔 무위 기하학적 비선형성을 고려한 유한요소법의 3차원 적층 축대칭요소(layered axi-symmetric solid element)에 적용하였다. 유한요소 해석은 전처리 프로그램(HC2004)을 이용 연소관 돔 부위에서의 기하학적 비선형성을 고려하여 ANSYS로 해석을 수행 하였으며, 그 결과 전처리 시간 및 계산 소요시간이 짧았으며, 수압실험 결과 값과 비교, 검토하였다.

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Amphetamine-type Stimulants in Drug Testing

  • Chung, Heesun;Choe, Sanggil
    • Mass Spectrometry Letters
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    • 제10권1호
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    • pp.1-10
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    • 2019
  • Amphetamine-type stimulants (ATS) are a group of ${\beta}$-phenethylamine derivatives that produce central nervous system stimulants effects. The representative ATS are methamphetamine and 3, 4-methylenedioxymethamphetamine (MDMA), and abuse of ATS has become a global problem. Methamphetamine is abused in North America and Asia, while amphetamine and 3, 4-methyle nedioxym ethamphetamine (Ecstasy) are abused in Europe and Australia. Methamphetamine is also the most abused drug in Korea. In addition to the conventional ATS, new psychoactive substances (NPS) including phenethylamines and synthetic cathinones, which have similar effects and chemical structure to ATS, continue to spread to the global market since 2009, and more than 739 NPS have been identified. For the analysis of ATS, two tests that have different theoretical principles have to be conducted, and screening tests by immunoassay and confirmatory tests using GC/MS or LC/MS are the global standard methods. As most ATS have a chiral center, enantiomer separation is an important point in forensic analysis, and it can be conducted using chiral derivatization reagents or chiral columns. In order to respond to the growing drug crime, it is necessary to develop a fast and efficient analytical method.