• Bulletin of the Korean Chemical Society
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• v.32 no.2
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• pp.498-502
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• 2011

The divergent synthesis of novel phosphorus-containing dendrimer with 4,4'-sulphonyldiphenol at the core has been accomplished involving simple condensation reactions using $P(O)Cl_3$, $P(S)Cl_3$, 3-amino-phenol, 3-hydroxy-benzaldehyde, and 2-butyn 1, 4-diol. The final compound was a Schiff's base macromolecule possessing 4 imine bonds, 8 acetylenic bonds and 8 OH groups at the periphery. The structures of intermediate compounds were confirmed by IR, NMR ($^1H$, $^{13}C$ and $^{31}P$), LC-Mass and C, H, N analysis. The structure of the final dendrimer (5) was confirmed by IR, NMR ($^1H$, $^{13}C$ and $^{31}P$), MALDI-TOF-MS, and C, H, N analysis. The surface morphological characteristics of the final dendrimer were understood by Scanning Electronic Microscopic study (SEM). The thermal stability of the final dendrimer was studied by TGA/DTA analysis.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 1997.04a
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• pp.184-191
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• 1997

A method, termed as the substructural sensitivity synthesis method, which utilizes the computational merits of the component mode synthesis technique is proposed to calculate design sensitivity of modal parameters of substructurally combined structures. In this method, the sensitivity analysis is combined with component mode synthesis thchnique. thus the degrees of freedom of a combined structure can be dramatically reduced. Free-interface mode method including the residual attachment modes among the component mode synthesis methods is used to calculate the modal sensitivity of the combined structure. For the design sensitivities of modal properties of structure, the Nelson's method, which is exact solving method is used. It is shown that the modal sensitivities of the entire structure can be obtained by synthesizing the substructural modal data, and the sensitivities of the modal data about the design variables of modifiable substructure. Using the proposed method, the final degrees of freedom of entire structure can be remarkably reduced to calculate the modal parameter sensitivities. With a structure composed of beams and plates, as an example, the sensitivities of the eigenvalues and eigenvectors obtained by this proposed method were compared with the exact solutions in terms of accuracy.

• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.7 s.94
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• pp.1833-1840
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• 1993

An efficient vibration analysis method, Component Mode Synthesis(CMS), for an exhaust system with bellows is presented. Analyses are performed for two types of bellows, where characteristics of vibration modes affecting idle shake and interior noise of a vehicle are examined. Also analyzed are the contributions of an exhaust and engine mounting system to the idle shake and interios noise. Comparison between the analysis and test is in good agreement, hence the CMS method is shown to be efficient and valid.

• Journal of KSNVE
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• v.3 no.3
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• pp.253-257
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• 1993

In this study, vibration analysis of a refrigerator was carried out to reduce vibration induced noise. When the components of a machine are assembled together, the natural frequencies of each component are changed since they have influences on one another. To avoid the problem of resonance, the vibration characteristics of each component must be checked systematically after they are designed. For this purpose, vibration analysis of a refrigerator was done using a component synthesis method. The experimental and analytical results showed good agreement and are presented here.

• Transactions of the Korean Society of Automotive Engineers
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• v.11 no.3
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• pp.177-183
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• 2003

Vibration analysis using component mode synthesis method was carried out to identify that to some extent each component contributed to the whole vibration of a powertrain consisting of several components. This analysis helped decide the component to be modified to reduce the powertrain weight, without degrading its current vibration characteristics. As a result, a cylinder block was chosen as a redesign object. Topology optimization analysis was performed to design the topology of the cylinder block whose flange connected with the transmission was chosen to be the design domain. After all, a new prototype of cylinder block was manufactured based on the analysis results for the verification experiment. It was confirmed from the analytical and experimental results that u optimally designed cylinder block had an advantage over the current one in the powertrain weight, with the powertrain vibration characteristics improved slightly.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2001.04a
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• pp.501-504
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• 2001

The use of error compensation techniques has been recognized as an effective way in the improvement of the accuracy of a machine tool. The laser measurement method for identifying position errors of machine tool has the disadvantages such as high cost, long calibration time and usage of volumetric error synthesis model. Accordingly, this paper deals with analysis of the position errors of a machine tool using ball bar test without using complicated error synthesis model. Statistical analysis method was adopted in this paper for deriving position errors using hemispherical helix ball bar test.

• Journal of the Korean Society for Precision Engineering
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• v.19 no.9
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• pp.34-40
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• 2002

Machining accuracy is affected by quasi-static errors of machining center. Since machine errors have a direct influence upon both the surface finish and geometric shape of the finished workpiece, it is very important to measure the machine errors and to compensate these errors. The laser measurement method for identifying geometric errors of machine tool has the disadvantages such as high cost, long calibration time and usage of volumetric error synthesis model. Accordingly, this paper deals with analysis of the geometric errors of a machine tool using ball bar test without using complicated error synthesis model. Statistical analysis method was adopted in this paper for deriving geometric errors using hemispherical helix ball bar test. As a result of experiment, geometric errors of the vertical machining center are compensated by 88%.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.11
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• pp.2672-2679
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• 2000

In synthesizing and RSSS-SC mechanism that is the kinematic model of the McPherson strut suspension system in automobiles, the design equations for R-S, S-S and S-C dyads should be solved separately for a given set of prescribed positions. The number of prescribed positions that the RSSS-SC mechanism can be synthesized is up to three because of the S-C dyad. This limitation may cause unsatisfactory results in synthesized joint positions. This paper presents a kinematic synthesis method to place the joints of an RSSS-SC mechanism in desired boundaries by varying the prescribed positions of the mechanism within acceptable tolerances. The sensitivity analysis of the joint positions is used determine which displacement parameter should be altered to fulfill this task.

• Proceedings of the Korean Institute of Intelligent Systems Conference
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• 1993.06a
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• pp.1321-1325
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• 1993

This paper investigates the use of Fuzzy vector quantizer(FVQ) in speech synthesis. To compress speech data, we employ K-means algorithm to design codebook and then FVQ technique is used to analysize input speech vectors based on the codebook in an analysis part. In FVQ synthesis part, analysis data vectors generated in FVQ analysis is used to synthesize the speech. We have fined that synthesized speech quality depends on Fuzziness values in FVQ, and the optimum fuzziness values maximized synthesized speech SQNR are related with variance values of input speech vectors. This approach is tested on a sentence, and we compare synthesized speech by a convensional VQ with synthesized speech by a FVQ with optimum Fuzziness values.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2000.11a
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• pp.287-290
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• 2000

An efficient dynamic response analysis method of structures supported by nonlinear resilient mounts when subjected to the transient base excitations is presented by using the structural synthesis method in time domain. Through a numerical example, the validity of the presented method is verified by comparison of the results with those of the 'traditional' analysis method.