• Bulletin of the Korean Chemical Society
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• v.30 no.11
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• pp.2680-2686
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• 2009

The synthesis of a novel superabsorbent hydrogel with natural hybrid backbone via graft copolymerization of acrylamide (AAm) onto kappa-carrageenan (kC, as a polysaccharide) and gelatin (as a protein) under classic thermal conditions is described. The Taguchi method as a strong experimental design tool was used for synthesis optimization. A series of hydrogels were synthesized by proposed conditions of Qualitek-4 Software. Considering the results of 9 trials according to analysis of variance (ANOVA), optimum conditions were proposed. The swelling behavior of optimum hydrogel was measured in various solutions with pH values ranging from 1 to 13. In addition, swelling kinetics, swelling in various organic solvents, various salt solutions and On–Off switching behavior were investigated. The hydrogel formation was confirmed by Fourier transform infrared spectroscopy (FTIR) and thermogravimetrical analysis (TGA). Surface morphology of the synthesized hydrogels was assessed by scanning electron microscope (SEM).

• The KIPS Transactions:PartB
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• v.9B no.2
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• pp.223-230
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• 2002

In a speech coding system using excitation source of voiced and unvoiced, it would be involves a distortion of speech waveform in case coexist with a voiced and an unvoiced consonants in a frame. This paper present a new method of TSIUVC (Transition Segment Including Unvoiced Consonant) approximate-synthesis by using Least Mean Square. The TSIUVC extraction is based on a zero crossing rate and IPP (Individual Pitch Pulses) extraction algorithm using residual signal of FIR-STREAK Digital Filter. As a result, This method obtain a high Quality approximation-synthesis waveform by using Least Mean Square. The important thing is that the frequency signals in a maximum error signal can be made with low distortion approximation-synthesis waveform. This method has the capability of being applied to a new speech coding of Voiced/Silence/TSIUVC, speech analysis and speech synthesis.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2000.11a
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• pp.495-499
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• 2000

The booming noise of a vehicle is usually caused by the vibration of the vehicle's body transmitted from the engine through the mounting system. Thus the engine mounting system must be cautiously designed to reduce the noise. Vector synthesis analysis is performed to predict the booming noise when the characteristic of the engine mounting system is changed., i.e., when magnitudes and phases of vibratory forces after the mounts are altered. To effectively use the method, the concept of 'effectiveness' is introduced to identify the contributions of each vibration sources and transmission paths to interior noise. When the magnitudes and phases of the forces due to the engine vibration are changed, the synthesized interior booming noise level is predicted by the vector synthesis diagram. Thus, the optimum characteristics of the forces are obtained through the simulations of the vector synthesis analysis. It is shown that the vector synthesis method can be used to obtain the optimum design characteristic of the mounting system to control the interior booming noise of a vehicle.

• Journal of Powder Materials
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• v.30 no.3
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• pp.233-241
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• 2023

In this study, we evaluated the effects of acid leaching on the properties of Cr powder synthesized using self-propagating high-temperature synthesis (SHS). Cr powder was synthesized from a mixture of Cr2O3 and magnesium (Mg) powders using the SHS Process, and the byproducts after the reaction were removed using acid leaching. The properties of the recovered Cr powder were analyzed via X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), particle size analysis (PSA), and oxygen content analysis. The results show that perfect selective leaching of Cr is challenging because of various factors such as incomplete reaction, reaction kinetics, the presence of impurities, and incompatibility between the acid and metal mixture. Therefore, this study provides essential information on the properties under acidic conditions during the production of high-quality Cr powder using a self-propagating high-temperature synthesis method.

• Journal of Advanced Marine Engineering and Technology
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• v.24 no.3
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• pp.52-57
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• 2000

This study intends to reduce the weight of structure without changing the dynamic characteristics. At first, the Vibration analysis by the Substructure Synthesis Method and FFM using the ANSYS are performed for the engine speed converter to confirm the reliability of the analyzing tools. Weight minimization is performed by the Sensitivity Analysis and the Optimum Structural Modification. To decrease the converter weight ideally, the parts with low sensitivity are to be cut mainly, and the changing quantity of the natural frequency by the cut is to be recovered by the weight modification of the parts with high sensitivity. As the unique mathematical solution for the homogeneous problem(i.e. 0 object function problem) does not exist, the converter is redesigned with much thinner initial thickness. The goal of this study is to recover the dynamic characteristics of redesigned structure to those of the original one. To say in the other words, the modified structure has the same dynamic characteristics and the more lighter weight to compare with the original one.

• Journal of Microbiology and Biotechnology
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• v.28 no.4
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• pp.566-570
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• 2018

Because glycosylation of aesculetin and its 6-glucoside, aesculin, enhances their biological activities and physicochemical properties, whole-cell biotransformation and enzymatic synthesis methodologies using Neisseria polysaccharea amylosucrase were compared to determine the optimal production method for glycoside derivatives. High-performance liquid chromatography analysis of reaction products revealed two glycosylated products (AGG1 and AGG2) when aesculin was used as an acceptor, and three products (AG1, AG2, and AG3) when using aesculetin. The whole-cell biotransformation production yields of the major transfer products for each acceptor (AGG1 and AG1) were 85% and 25%, respectively, compared with 68% and 14% for enzymatic synthesis. These results indicate that whole-cell biotransformation is more efficient than enzymatic synthesis for the production of glycoside derivatives.

• Polymer(Korea)
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• v.25 no.5
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• pp.609-616
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• 2001

The application of microwave technology to synthesis of polymer in solvent media has been shown by the synthesis of copper phthalocyanine (CUPc). The increase of synthetic yield-was demonstrated successfully in this study. A power variable microwave synthetic system has been developed with modifying cavity of domestic microwave oven and attaching microwave power controller. The properties of the specimen synthesized at various condition under the conventional thermal processing and microwave processing has been characterized by the means of chemical analysis, X-ray diffractometry (XRD), scanning electron microscopy (SEM), and particle size analysis (PSA).

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2006.05a
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• pp.182-186
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• 2006

An efficient dynamic response analysis mettled of structures supported by resilient mounts is presented by using the structural synthesis method in frequency domain and time domain. As a numerical example, a mount-deck system is considered. Through numerical simulations, the validity of the presented method is verified by comparison of the results with those of the 'traditional' analysis method.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1325-1326
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• 2006

Tungsten-molydiside $W_xMo_{1-x}Si_2$ was synthesized by self-propagating high temperature synthesis (SHS). The SHS product with the initial composition of (0.5Mo+0.5W+2Si) contains 23.9% $MoSi_2$, 40.89% $WSi_2$ with remaining 9.11% Mo, 9.16% Si and 16.94%W. Lattice parameters of the $MoSi_2$ and $WSi_2$ determined by Rietvelt analysis were a=0.3206 nm, c=0.7841 nm and a=0.3212 nm, c=0.7822 nm, respectively.

• Journal of KSNVE
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• v.7 no.6
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• pp.993-1000
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• 1997

This paper presents a new technique of mathematical treatment using a finite element model for analyzing the vibration of the towed line array. Since the towed line array has the axisymmetricity, axisymmetric elements are used in finite element modeling for the towed array structure. The fluid-structure interaction is also considered. The array consists of a series of identical substructures which can include internal structures such as spacers, hydrophones and ropes. That periodicity of substrucutres permits the substructure synthesis technique using characteristic wave guide for analyzing the response of towed array system. This synthesis technique can reduce the cost of computing the array response. It is suggested that a response of towed array can be computed by the finite element method and substructure synthesis technique using wave guide. Several experiments for towed array were performed to verify the present computation technique. The predicted vibration for the towed array shows good agreement with the measured result.