• Title/Summary/Keyword: aminopropylpolydimethylsiloxane

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Preparation and Properties of Silicone-Modified Epoxy Coating Materials (실리콘 변성 에폭시 코팅 액의 제조와 물성)

  • Kim, Jin Kyung;Bak, Seung Woo;Hwang, Hee Nam;Kang, Doo Whan;Kang, Ho Jong
    • Applied Chemistry for Engineering
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    • v.25 no.4
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    • pp.352-356
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    • 2014
  • PDMS modified epoxy resin with epoxy group (EMPDMS) was prepared from the reaction of ${\alpha},{\omega}$-aminopropylpolydimethylsiloxane and diglycidyl ether of bisphenol-A (DGEBA) based epoxy resin, and PDMS modified epoxy hybrid compound (EMPDMSH) was prepared by introducing alkylesteraminopropyl alkoxy silane to EMPDMS. Their structures were characterized using FT-IR, $^1H$-NMR and $^{29}Si$-NMR. Coating materials were prepared by mixing EMPDMSH base and solvent. Physical properties of the coating materials coated on epoxy/glass fiber composite film were measured according to the content of PDMS in EMPDMSH. Contact angle of coating film was increased 30 to 71 degree. Adhesive property of coating film was 5B degree better then epoxy or acrylate coating materials, and surface roughness was decreased as increasing in EMPDMSH.