• Advances in nano research
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• v.14 no.4
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• pp.355-362
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• 2023

Physical exercise, especially intense exercise and high intensity interval training (HIIT) by trampoline, can lead to muscle injuries. These effects can be reduced with intelligent products made of nanocomposite materials. Most of these nanocomposites are polymers reinforced with silicon dioxide, alumina, and titanium dioxide nanoparticles. This study presents a polymer nanocomposite reinforced with silica. As a result of the rapid reaction between tetraethyl orthosilicate and ammonia in the presence of citric acid and other agents, silica nanostructures were synthesized. By substituting bis (4-amino phenoxy) phenyl-triptycene in N, N-dimethylformamide with potassium carbonate, followed by catalytic reduction with hydrazine and Pd/C, the diamine monomer bis (4-amino phenoxy) phenyl-triptycene is prepared. We synthesized a new polyaromatic (imide) with triptycene unit by sol-gel method from aromatic diamines and dianhydride using pyridine as a condensation reagent in NMP. PI readily dissolves in solvents and forms robust and tough polymer films in situ. The FTIR and NMR techniques were used to determine the effects of SiO₂ on the sol-gel process and the structure of the synthesized nanocomposites. By using a simultaneous thermal analysis (DTA-TG) method, the appropriate thermal operation temperature was also determined. Through SEM analysis, the structure, shape, size, and specific surface area of pores were determined. Analysis of XRD results is used to determine how SiO₂ affects the crystallization of phases and the activation energy of crystallization.

• Journal of the Korea Institute of Military Science and Technology
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• v.5 no.3
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• pp.105-112
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• 2002

A combined process of non-thermal plasma and catalytic techniques has been investigated to treat toxic gas compounds in air. The treated gas in the present study is $CH_3$CN that has been known to be a simulant of toxic chemical agent. A planar type dielectric barrier discharge(DBD) reactor has been used to generate non-thermal plasma that produces various chemically active species, O, N, OH, $O_3$, ion, electrons, etc. Several different types of adsorbents and catalysts, which are MS 5A, MS 13X, Pt/alumina, are packed into the plasma reactor, and have been tested to save power consumption and to treat by-products. Various aspects of the present techniques, which are decomposition efficiencies along with the power consumption, by-product analysis, reaction pathways modified by the adsorbents and catalysts, have been discussed in the present study.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 1999.10a
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• pp.213-214
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• 1999

발전소, 소각시설 및 산업공정에서 다량으로 배출되는 질소산화물(NOx)을 처리하기 위하여 과잉공기 연소시 고온에서 암모니아(NH$_3$)나 요소(CO(NH$_2$)$_2$)를 환원제로 사용하는 SNCR법, 그리고 암모니아와 각종 촉매를 사용하여 NOx를 $N_2$로 환원시키는 SCR법이 주로 개발ㆍ상용화되었다. 최근 90년대 초반부터 NOx의 제거기술은 Cu-ZSM-5, Alumina 통의 경제적이고 효과적인 촉매의 개발과 암모니아 사용으로 인한 부담요소를 제거하고자 다양한 HCs를 대체사용하는 방향으로 많은 연구가 진행되었다.(중략)

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.07b
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• pp.772-775
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• 2003

The development of new improved type of dielectric materials on the conception of multiphase structure has been carried out in this paper. Metal alkoxides solutions were used for application of thin film by electrophoretic deposition technique. We succeeded in preparation of amorphous and composite dielectric films from Al alkoxides. Specific features of the preparation technique were considered. Microstructure of the films was examined as well as their dielectric properties. TEM analyses reveals that films deposited from aging sols and heat-treated at temperatures as low as $400^{\circ}C$ contain small whiskers of ${\delta}-Al_2O_3$.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2008.11a
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• pp.62-63
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• 2008

Photonic crystas were fabricated using an anodic aluminum oxide(AAO) mask on GaN diode. The Photonic crystal structure has been investigated from Atomic Force Microscope(AFM). The hole diameter and lattice constant of photonic crystal are 60nm and 105nm, respectively. Photoluminescence of photonic crystal was enhanced and optical interference was increased by photonic crystal effect.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.12 no.5
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• pp.76-85
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• 2013

This study was carried out to investigate the relation between surface roughness and heat absorption capability of materials for solar collector. For this purpose, 3 kinds of materials (copper, aluminum, iron), 5 kinds of surface roughness (scrubber, alumina sand #80, #200, #400, glass bead) and 2 kinds of surface treatment (black chrome plating, copper black coating) were used for finding optimal conditions to apply solar collector. As the results, it was confirmed that the optimal relations between surface roughness and surface treatment as well as optimal materials were necessary. Further, heat absorption capability was showed good results in cases of copper materials, glass bead and black chrome plating.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1992.10a
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• pp.166-171
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• 1992

Mechanical seals are generally used in the fields of industries as sealing devices. The failure of mechanical seals like crack, leakage, breakage fast and severe wear, excessive torque, and squeaking result in big problems. For the development of monitoring system, this study was carried out to identify abnormal phenomina on alumina(AI $\_$2/ O /sub3/) seal ring and resin bonded carbon ring, and to propose the proper parameter for monitoring failure on mechanical seals. Sliding were tests are conducted at 12 experimental conditions that contains 3 different contact pressure and 4 surface conditions. Torque, temperature, and acoustic emission are measured. Optical microstructure and scanning electron microscopy are observed for the wear processing every 10 minute sliding at rotation speed of 1750 RPM.

• Korean Journal of Pharmacognosy
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• v.2 no.1
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• pp.39-40
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• 1971

An alkaloidal component was extracted from the root of Aconitum koreanum R. $R_{AYMOND}$ of the commercial origin. Crude extract was obtained in ca. 2% yield out of dried root with ether-methanol (10:1). White amorphous compound was precipitated out from the HCl solution upon the addition of ammonia water, and crude base was obtained by extraction of its mother liquid with chloroform. This crude base was purified by the alumina-column chromatographic method. A pure alkaloidal component(500mg) was yielded from its crude base. Its pure base comes as needle crystals melting at $250{\sim}252^{\circ}C$ (decomp.), $[\alpha]^{20}_D$ D+9.82 (methanol) and Anal. calcd. for $C_{19}H_{27}O_{8}N$.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1994.11a
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• pp.206-209
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• 1994

This paper has been researched bondability of electronic devices, such as lead frame and thick film of Ag/Pd on an alumina substrate by different heat sources. To obtain the bonds with high quality, it is very important to control both the thermal distribution of the bonds and it stability, because electronics components is consist of different materials. Therefore, this paper clarifies not only heat mechanism of micro parallel gap resistance bonding method and pulse heat tip bonding method but also investigates selection of heat sources with micro-electronic materials for bonding. Finally, it is realzed fluxless bonding process with filler metal such as plating layers.

• Tribology and Lubricants
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• v.5 no.1
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• pp.28-35
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• 1989

The wear tests of ceramic materials in dry rolling contact were carried out at room temperature to investigate their macroscopic wear characteristics. Both point contact and line cootact were adapted in the wear tests of them. Ceramic materials used in these tests were silicon nitride, silicon carbide, cermet of TiN and TiC, titania, and alumina. The wear test of the bearing steel was carried out to compare to the wear test results of the ceramic materials. The results showed that the wear rate of silicon nitride was smaller than any other ceramic materials and bearing steel. In the steady wear, the wear volume of ceramic materials increases linearly with the rolling distance. It was also found from the experimental results that fracture toughness and surface roughness dominate the wear process of ceramic materials in dry rolling contact.