• 한국마린엔지니어링학회:학술대회논문집
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• 한국마린엔지니어링학회 2001년도 추계학술대회 논문집(Proceeding of the KOSME 2001 Autumn Annual Meeting)
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• pp.71-79
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• 2001

Recently the steel parts used at automobiles are required to be used under high stress more than ever before in need of the weight down. To achieve this requirement of a high strength steel, it must be necessary to decrease inclusion content and surface defect as like decarburization, surface roughness etc.. In this study, the surface conditions are measured to know the influence on fatigue properties by two cases of shot peening of two-stage shot peening and single-stage shot peening. And for this study, three kinds of spring steel(JISG4081-SUP ,SAE 9254, DIN 50CrV4, ) are made. This study shows the outstanding improvement of fatigue properties at the case of two-stage shot peening in the rotary bending fatigue test and this is assumed to be from (1) Decreasing the surface roughness (2) Unchanging the surface hardness (3) Increasing the compressive residual stress But, results also show fatigue failures originated at inclusion near surface, and this inclusion type is turned out to be a alumina of high hardness.

• 분석과학
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• 제6권1호
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• pp.21-27
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• 1993

54% 순도의 공업용 n-헥산을 HPLC급으로 분리, 정제하였다. 분별증류법으로 분리하기 어려운 methylcyclopentane, 2-methylpentane, 그리고 3-methylpentane 등은 molecular aieve 5A를 이용한 액체-고체 크로마토그래피법으로 분리하였다. HPLC 용매로서 엄격히 규제받는 UV와 형광불순물은 알루미나와 실리카겔을 이용한 흡착법으로 정제하였다. 이와 같은 방법으로 n-헥산을 정제함으로써 수분, 색도(APHA), 산도, 증발잔류물, 황 및 thiophene 등의 불순물 항목을 모두 HPLC급의 규격까지 낮출 수 있었다.

• 한국주조공학회지
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• 제17권3호
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• pp.267-275
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• 1997

Fabrication of high strength Mg-Li-Al alloys by squeeze casting was established by the stabilization of melt and mold temperatures, applied pressure and the refining method. The entrapment of inclusions during pouring was prevented using 30 ppi alumina foam filter. The as-cast microstructure consists of a mixture of ${\alpha}$ and ${\beta}$ phases including AILi and $MgLi_2$, Al particles, which are distributed in the ${\beta}$ matrix. The grain sizes of gravity and squeeze casting alloys were 288 ${\mu}m$ and 207 ${\mu}m$ respectively. The addition of Al in Mg-Li alloys promoted the formation of second phase particles, which were adjusted to optimize the properties of Mg-Li-Al alloys. The Mg-10wt%Li-5wt%Al alloy after heat treatment at $350^{\circ}C$ for 1 hour showed the maximum hardness value. This is due to the facts that the amounts of ${\alpha}$ and ${\beta}$ phases and their distributions are dependent upon the solution treatment temperature, and that the amounts of AILi and $MgLi_2Al$ particles are dependent upon the Al content.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2003년도 제5회 영호남 학술대회 논문집
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• pp.31-34
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• 2003

($Ba_{0.6-x}Sr_{0.4}Ca_x)TiO_3$ (BSCT) (x=0.10, 0.15, 0.20) powder, prepared by the sol-gel method, were mixed with organic vehicle and the BSCT thick films were fabricated by the screen-printing techniques on alumina substrates using the BSCT paste. The structural and the electrical properties were investigated for various composition ratio and sintering temperature. BSCT thick film thickness, obtained by four printings, was approximately 110 ~ 120 ${\mu}m$. The Curie temperature and dielectric constant at room temperature were decreased with increasing Ca content. The relative dielectric constant, dielectric loss and tunability of the BSCT(50/40/10) specimen, which was sintered at $1420^{\circ}C$ and measured at 1MHz, were about 910, 0.46% and 9.28% at 5kV/cm, respectively.

• 대한화학회지
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• 제15권2호
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• pp.55-63
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• 1971

In this study, several nickel catalysts for the steam-hydrocarbon reforming process were prepared from various nickel salt, magnesium oxide, alumina and kaolinite. The activity and strength of the catalysts were investigated. 1. The proper composition of the calcined catalysts are: NiO (5-15%)-MgO(10-20%)-$Al_2O_3$(10-40%)-Kaolinite(50-80%). 2. The admixed or cosedimented ingredients of the catalysts was pelletized and calcinated at 1000 or $1150^{\circ}C$. Calcination at $1150^{\circ}C$ for an hour was optimum. 3. The water to oil ratio (W/O) for reforming of hexane should be above 7 mole/mole. As the W/O increases, more carbon dioxide and hydrogen, but less carbon monoxide was produced. Also carbon deposition become lessen at higher W/O. 4. Maximum conversion had attained at about $850^{\circ}C$. As the reaction temperature increases, more carbon monoxide and hydrogen, but less carbon dioxide and lower hydrocarbon was produced. 5. The percent conversion at $850^{\circ}C$ was about 80%, using a catalyst which the nickel oxide content are 5%.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2001년도 춘계학술대회 논문집
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• pp.338-343
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• 2001

Recently the steel parts used at automobiles are required to be used under high stress more than ever before in need of the weight down. To achieve this requirement of a high strength steel, it must be necessary to decrease inclusion content and surface defect as like decarburization, surface roughness etc., In this study, the surface conditions are measured to know the influence on fatigue properties by two cases of shot peening of two-stage shot peening and single-stage shot peening. And for this study, two kinds of spring steel(SAE 9254, DIN 50CrV4) are made. This study shows the outstanding improvement of fatigue properties at the case of two-stage shot peening in the rotary bending fatigue test and this is assumed to be from (1) on low stress condition, the single stage shot peening is not affected by nonmetallic inclusion under metal. (2) it is possible that the two-stage shot peening increases the fatigue life and the high stress, but, that is affected by nonmetallic inclusion under metal. (3) so far, beeasily 50CrV4 have made high stress. But, results also show fatigue failures originated at inclusion near surface, and this inclusion type is turned out to be a alumina of high hardness.

• 한국세라믹학회지
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• 제50권6호
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• pp.460-465
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• 2013

Plate-shaped inorganic particles are coated onto a stainless steel substrate by the electrophoretic deposition of a precursor slurry which includes the inorganic particles of $Al_2O_3$ and polymer resin in mixed solvents to mimic the abalone shell structure, which is a composite of plate-shaped inorganic particles and organic interlayer binding materials with a layered orientation. The process parameters of the electrophoretic deposition include the voltage, coating time, and conductivity of the substrate. In addition, the suspension parameters are the particle size, concentration, viscosity, conductivity, and stability. We prepared an organic-inorganic composite coating with a high inorganic solid content by arraying the plate-shaped $Al_2O_3$ particles and electrophoretic resin via an electrophoretic deposition method. We analyzed the effect of the slurry composition and the electrophoretic deposition process parameters on the physical, mechanical and thermal properties of the coating layer, i.e., the thickness, density, particle orientation, Young's modulus and thermogravimetric analysis results.

• 한국전기전자재료학회논문지
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• 제16권4호
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• pp.304-310
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• 2003

(Ba$\sub$0.6-x/Sr$\sub$0.4/Ca$\sub$x/)TiO$_3$(BSCT) (x=0.10, 0.15, 0.20) powder, prepared by the sol-Bel method, were mixed with organic binder and then BSCT thick films were fabricated by the screen printing techniques on alumina substrates using the BSCT paste. The structural and the dielectric Properties were investigated for various composition ratio and sintering temperature. The second phase appeared in BSCT(40/40/20) thick film sintered at 1450$^{\circ}C$. BSCT thick film thickness, obtained by four printings, was approximately 110∼120$\mu\textrm{m}$. The Curie temperature and dielectric constant at room temperature were decreased with increasing Ca content. The relative dielectric constant, dielectric loss and tunability of the BSCT(50/40/10) specimen, which was sintered at 1420$^{\circ}C$ and measured at 1MHz, were about 910, 0.46% and 9.28% at 5㎸/cm, respectively.

• 한국자동차공학회논문집
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• 제11권1호
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• pp.185-192
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• 2003

Recently the steel parts used at automobiles are required to be used under high stress more than ever before in need of the weight down. To achieve this requirement of a high strength steel, it must be necessary to decrease inclusion content and surface defect as like decarburization, surface roughness etc.. In this study, the surface conditions are measured to Dow the influence on fatigue properties by two cases of shot peening of two-stage shot peening and single-stage shot peening. And for this study, three kinds of spring steel (JISG4081-SUP7, SAE 9254, DON 50CrV4) are made. This study shows the outstanding improvement of fatigue properties at the case of two-stage shot peening in the rotary bending fatigue test and this is assumed to be from (1) Decreasing the surface roughness (2) Unchanging the surface hardness (3) Increasing the compressive residual stress. But, results also show fatigue failures originated at inclusion near surface, and this inclusion type is turned out to be a alumina of hish hardness.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2002년도 추계학술대회 논문집
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• pp.366-372
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• 2002

Recently the steel parts used at automobiles are required to be used under high stress more than ever before in need of the weight down. To achieve this requirement of a high strength steel, it must be necessary to decrease inclusion content and surface deject as like decarburization, surface roughness etc.. In this study, the surface conditions are measured to know tile influence on fatigue properties by two cases of shot peening of two-stage shot peening and single-stage shot peening. And for this study, three kinds of spring steel (JISG4081-SUP7,SAE 9254, DIN 50CrV4, ) are made. This study shows the outstanding improvement of fatigue properties at tire case of two-stage shot peening in the rotary bending fatigue test and this is assumed to be from (1) Decreasing the surface roughness (2) Unchanging the surface hardness (3) Increasing the compressive residual stress But, results also show fatigue failures originated at inclusion near surface, and this inclusion type is turned out to be a alumina of high hardness.