• Title/Summary/Keyword: aging treatment

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Effect of long-term thermal aging on the microstructural and mechanical characteristics of nickel-based alloy weldment (니켈계 합금 용접부의 미세조직 및 기계적 특성에 대한 장기 열적 시효의 영향)

  • Yoo, Seung Chang;Ham, Junhyuk;Kim, Ji Hyun
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.12 no.1
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    • pp.41-48
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    • 2016
  • To investigate the effect of long-term thermal aging on the microstructural and mechanical characteristics of weldment made of nickel base alloy and its weld metal, an accelerated heat treatment was applied to simulate the process of long-term thermal aging in the operating condition of nuclear power plant. A representative nickel-based weldment with Alloy 600 and Alloy 182 was fabricated and heat-treated at $400^{\circ}C$ for 1,713 h and 3,427 h to simulate the thermal aging for the period equivalent to 15 and 30 years in operating pressurized water reactors, respectively. The microstructural and mechanical characteristics were analyzed by using optical microscopy, scanning electron microscopy and Vickers microhardness measurement. Changes were observed in precipitation behavior and microhardness of each specimen, and these changes were mainly attributed to the change in precipitated morphology and residual stress across the weld during the thermal aging process.

Effect of Dewaxing Ratio of Beeswax-treated Hanji by Heat and Pressure Method on Aging Behavior of Dewaxed Hanji (가온 가압법에 의한 밀랍도포한지의 탈랍율이 탈랍지의 열화 거동에 미치는 영향)

  • Cho, Byoung-Uk;Choi, Do-Chim;Jo, Byoung-Muk
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.3
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    • pp.15-21
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    • 2012
  • The optimum dewaxing ratio in dewaxing treatment by the heat and pressure method was investigated by considering aging stability of dewaxed Hanji. Commercial Hanji was coated with beeswax and thermally aged at $150^{\circ}C$ for 24 hours. Then it was dewaxed using the laboratory sheet press equipped with hot plates on both top and bottom sides. Dewaxing ratio was controlled by pressing temperature and time. Four type of dewaxed Hanji samples with different dewaxing ratio were prepared and thermally aged at $150^{\circ}C$. Then the aging stability of dewaxed Hanji samples was evaluated in terms of optical and strength properties. It was found that the aging stability of dewaxed Hanji was superior with higher dewaxing ratio. The result concluded that, in the aspect of aging stability, the coated beeswax in beeswax-treated Hanji shall be completely removed if the coated wax would be dewaxed.

Physicochemical Characteristics and Antioxidant Activities of Deoduck (Codonopsis lanceolata) with Different Aging Temperatures and Periods

  • Jang, Gwi Yeong;Lee, Youn Ri;Song, Eun Mi;Jeong, Heon Sang
    • The Korean Journal of Food And Nutrition
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    • v.31 no.2
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    • pp.258-263
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    • 2018
  • To assess a potential possibility of Deoduck as functional food resources, this study was performed to determine the changes in chemical components and antioxidant activities on Deoduck with various aging conditions; aging temperatures were 60, 70, and $80^{\circ}C$, and aging periods were 5, 10, 15, 30, and 50 days. We determined pH, total acidity, browning index, 5-hydroxymethyl-furfural, total phenolic contents, DPPH and ABTS radical scavenging activities of aged Deoduck. Total acidity of aged samples increased during aging treatment, at higher temperature and longer time. The pH value of aged Deoduck ranged from 4.97 to 3.76. Aged Deoduck at $60^{\circ}C$ decreased slowly than 70 and $80^{\circ}C$, and these results were similar in total acidity. 5-HMF and total phenolic contents increased when increased aging temperature and periods. The DPPH and ABTS radical scavenging activities of Deoduck were ranged from 0.374 to 1.560 mg TEAC eq/g and from 0.302 to 1.745 mg trolox eq/g, respectively.

Effect of R Phase Formation on the Mechanical Properties of 25Cr-7Ni-2Mo-4W Super Duplex Stainless Steel (25Cr-7Ni-2Mo-4W 슈퍼 2상 스테인리스강의 기계적 성질에 미치는 R상의 영향)

  • Lee, Byung-Chan;Kang, Chang-Yong
    • Korean Journal of Materials Research
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    • v.24 no.8
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    • pp.401-406
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    • 2014
  • In this study, we investigated the precipitation behavior of the R-phase precipitated at the initial stage of aging and its effects on the mechanical properties of 25%Cr-7%Ni-2%Mo-4%W super duplex stainless steel. The R-phase was mainly precipitated at the interface of ferrite/austenite phases and inside of the ferrite phase during the initial stage of aging. It was transformed into the ${\sigma}$-phase with an increase of the aging time. The ferrite phase was decomposed into a new austenite(${\gamma}_2$)phase and the ${\sigma}$-phase by an aging treatment. The R phase was an intermetallic compound showing higher molybdenum and tungsten concentrations than the matrix and also showed higher molybdenum and tungsten concentrations than the ${\sigma}$ phase. In the initial stage of aging, precipitation of the R-phase did not change the hardness, the strength and the elongation. The hardness and the strength increased upon a longer aging time, but the elongation rapidly decreased. These results show that the R-phase did not significantly affect the hardness and the strength, though it did influence the elongation.

How we should approach and manage older patients with cancer (노인 암 환자의 접근과 관리 원칙)

  • Kim, Jee Hyun
    • Korean Journal of Head & Neck Oncology
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    • v.33 no.2
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    • pp.1-8
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    • 2017
  • Cancer is the disease of aging and Korea is one of the fastest aging country in the world. Older patients have decreased organ function and stress tolerance, therefore are at high risk of functional decline and developing complication from cancer and cancer treatment. Before beginning cancer treatment, it is important to assess patients' life expectancy, whether the patient is likely to die of cancer or of other comorbidity, and also the risks with cancer treatment. In order to estimate patient's physiologic age, it is recommended to perform geriatric assessment and implement appropriate geriatric intervention together with meticulous supportive care, when planning cancer treatment for older patients. In a resource limited country such as Korea, two step approach of applying screening tool followed by geriatric assessment can be more efficient. Geriatric assessment is used to predict toxicity from cancer treatment such as surgery, radiotherapy, and chemotherapy, predict survival, and also to aid treatment decision. Number of randomized trials are ongoing to compare usual care versus oncogeriatric care, and with these results we expect to improve outcome of older patients with cancer.

Effect of Heat Treatment on the Martensitic Transformation and Tensile Deformation Behavior in Ti-Ni-B shape Memory Alloy (Ti-Ni-B 형상기억합금의 마르텐사이트변태 및 인장변형거동에 미치는 열처리의 영향)

  • Lee, O.Y.;Park, Y.K.;Ahn, H.K.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.1
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    • pp.75-83
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    • 1995
  • The purpose of this study is to investigate the effect of heat treatments on the martensite transformation and tensile deformation behavior in Ti-Ni-B alloys with various boron concentration. Three types of heat treatment are given to the specimens; i) solution treatment ii) aging iii) thermo-mechanical treatment. In solution treated specimens. R-phase transition which is related to abnormal increase of electrical resistance prior to martensitic transformation has been formed at a boron content of 0.2at % and the $M_s$ temperature has been decreased with the increasing of boron content. However. It has not been affected by aging, while that of thermo-mechanically treated specimens has been remarkably increased in the vicinity of recrystallization temperature. The thermo-mechanically treated specimen has showed a good thermal fatigue characteristics, shape memory effect and superelasticity in comparison with the solution treated specimen.

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The Effect of Thermomechanical Treatment on the Microstructural Changes and Fatigue Properties in 7050 Al Alloy (7050 AI 합금의 가공열처리가 미세조직변화와 피로성질에 미치는 영향)

  • Kim, M.H.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.4
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    • pp.24-33
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    • 1991
  • The effects of thermomechanical treatments on microstructure and fatigue properties of 7050 Al alloy were investigated. The precipitation kinetics changed to a faster rate due to cold deformation employed in this special TAHA thermomechanical treatments including pre-aging, plastic deformation and two step final-aging. The G.P. zones in the under-aged condition were cut by dislocations and dissolved during the plastic deformation. During the low cycle fatigue, the T6' condition showed cyclic hardening behavior whereas the TMT5, TMT27 and T76 conditions showed cyclic softening at above 0.7% total strain amplitudes. The ${\Delta}K_{th}$ value of TMT27 was improved more than two times, compared with that of T76 condition. The T6' with small shearable precipitates resulted in the markedly high ${\Delta}K_{th}$ value. This is thought to be resulted from dislocation reversibility and roughness-induced crack closure due to planarity of slip.

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Wire electrical discharge machining of titanium alloy according to the heat treatment conditions (열처리 조건에 따른 티타늄합금의 와이어 방전가공)

  • 김종업;왕덕현;김원일
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2001.04a
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    • pp.930-933
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    • 2001
  • Titanium Alloys used in this experiment has an good corrosion resistance and specific strength, and is the new material developed for medical supplies living goods. In this study the rolled titanium alloy is done by annealing, solution heat-treatment and aging and then is worked by wire EDM. With changing the process conditions, the process properties of surface hardness, surface roughness, shape of process surface and the analysis of ingredients are measured through experiment repeating main cut and finish cut. It is confirmed to gain good measure values as increasing the number of processing of wire EDM. In this experiment the phenomena of processing is studied and the appropriate process condition is proposed.

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Microstructure and Fracture Path of Cr-Mn-N Steel upon Aging Treatment

  • Lee, Se-Jong;Sung, Jang-Hyun;Ralls, K.M.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.3
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    • pp.21-30
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    • 1991
  • Microstructural analysis was conducted to observe the effect of aging treatments in a Cr-Mn austenitic stainless steel containing nitrogen, and the amount, size, shape and distribution of precipitates were investigated. It was found that on water quenching from $1000^{\circ}C$ after holding 3 h at that temperature, the steel contained no precipitates observable by optical microscopy. Precipitation of phases begins at places most favorable for the formation of nuclei-in the boundaries of grains and twins. Precipitates were studied in detail by means of scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Chemical compositions of precipitates were examined by the use of scanning transmission electron microscopy (STEM) together with an energy dispersive X-ray (EDX) microanalysis. Also chromium depletion adjacent to grain boundary precipitates was investigated by the use of Auger electron spectroscopy (AES) for a direct examination of the fracture surface chemistry.

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The Effect of Ausforming Process on Mechanical Properties of Ultrahigh Strength Secondary Hardening Martensitic Steels (극초고강도 이차경화형 마르텐사이트강의 기계적성질에 미치는 오스포밍 공정의 영향)

  • Kim, S.B.;Won, Y.J.;Song, Y.B.;Cho, K.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.4
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    • pp.179-184
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    • 2021
  • Two types of secondary hardening martensitic steels, 10Co-14Ni and 6Co-5Ni, were produced by vacuum induction melting to investigate the effect of ausforming process on mechanical properties. According to the results of present study, the alloy samples ausformed at low temperature indicated a rather low hardness level in overall aging time despite the refinement of martensite lath width. As the result can closely be related with the presence of primary carbides precipitated within the initial austenite matrix, we confirmed that, in ultrahigh strength secondary hardening martensitic alloy steels, the ausforming process can rather limit the degree of secondary hardening during the subsequent aging treatment.