• 제목/요약/키워드: ageing time

검색결과 207건 처리시간 0.028초

숙성이 제주마 등심의 육질과 관능적 특성에 미치는 영향 (Meat Quality and Sensory Characteristics in Longissimus Muscle of Jeju Horse as Influenced by Ageing)

  • 성필남;이종언;박범영;하경희;고문석
    • Journal of Animal Science and Technology
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    • 제48권2호
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    • pp.287-292
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    • 2006
  • 연도증진의 가장 일반적인 방법인 숙성을 통해 말고기의 육질과 관능적 특성이 어떻게 변화하는지를 조사하여 말고기의 적정 숙성기간을 제시하고, 국내 말고기의 냉장 유통에 대비한 기초자료를 확보하고자 제주마 24두의 등심을 4℃에서 25일간 숙성시키면서 육질과 관능적 특성을 조사하였다. 말고기 pH는 숙성기간에 따라 차이가 없었으며, 전단력은 저장 12일까지 유의적으로 감소하다가(P<0.05) 12일 이후 차이를 나타내지 않았다. 보수력, 가열감량 및 포장감량은 숙성기간이 경과할수록 증가하는 경향이였으며, 육색특성은 숙성기간이 경과할수록 명도(L*)와 적색도(a*) 값이 증가하는 경향을 보였다. 관능적 특성 중 풍미는 저장 7일에 가장 높은 수치를 나타내었고, 다즙성은 숙성 12일에 패널에 의해 가장 좋은 점수를 받았으며, 연도는 숙성 7일에 유의적인 증가를 보였으며(P<0.05) 이후 숙성기간에는 차이가 없었다. 숙성기간별 말고기에 대한 전체기호도는 숙성 7일에 유의적인 증가를 보인 후 숙성 18일까지 지속하다가 25일에 다소 감소하였다(P<0.05). 이상의 결과로 볼 때 말고기 등심의 최적숙성기간은 도축 후 9~14일로 나타났으며, 도축 후 20일 이후에는 기호성과 육질이 저하되는 결과를 보였다.

Rubber gaskets for fuel cells-Life time prediction through acid ageing

  • Kim, Mi-Suk;Kim, Jin-Kuk
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2007년도 추계학술대회 논문집
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    • pp.47-51
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    • 2007
  • The present paper reports the life time prediction of Acrylonitrile-Butadiene rubber (NBR) fuel cell gasket materials as a function of operational variables like acid concentration, ageing time and temperature. Both material and accelerated acid-heat aging tests were carried out to predict the useful life of the NBR rubber gasket for use as a fuel cell stack. The acid ageing of the gasket compounds has been investigated at 120, 140 and $160^{\circ}C$, with aging times from 3 to 600 h and increasing acid ($H_2SO_4$) concentrations of 5, 6, 7 and 10 vol%. Material characteristics the gas compound such as cross-link density, tensile strength and elongation at break were studied. The hardness of the NBR rubber was found to decrease with decreasing acid concentration at both 120 and $140^{\circ}C$, but at $160^{\circ}C$ interestingly the hardness of the NBR rubber increased abruptly in a very short time at different acid concentrations. The tensile strength and elongation at break were found to decrease with increase in both the acid concentrate ion & temperature. The life time of the compounds were evaluated using the Arrhenius equation.

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Ageing effect on compressibility, permeability and shear strength of clayey soils exposed to salt solutions

  • Cakar, Emel;Yukselen-Aksoy, Yeliz
    • Geomechanics and Engineering
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    • 제25권3호
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    • pp.245-251
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    • 2021
  • The present study investigated the ageing effect on compressibility, permeability and shear strength behavior of kaolin and bentonite samples in the presence of NaCl and CaCl2 solutions. The compressibility, permeability and shear strength parameters were determined on the 60, 190, and 250 days cured samples. The results have shown that, the kaolin sample becomes more compressible in the presence Ca2+ ions with ageing. Generally, the normalized compression index values of bentonite samples increased at the end of 60 days and 250 days curing time periods. The normalized permeability value of kaolin decreased by ageing in the presence of Na+ ions almost twofold. The permeability values of bentonite increased both in NaCl and CaCl2 solutions during ageing. In the presence of Na+ ions kaolin had higher max. shear stress value than Ca2+ ions. When the max. shear stress values of 0, 60 and 190 days samples were compared, it was seen that NaCl solution had no significant effect on the shear strength of kaolin sample. However, the shear strength of kaolin increased in the CaCl2 solution during ageing. In the presence of Ca2+ ions the max. shear stress value of bentonite was higher. The results of this study have shown that ageing has significant effects on the compressibility, permeability and shear strength of kaolinitic and bentonitic clayey soils.

숙성온도와 기간이 한우 거세우 배최장근의 육질 특성에 미치는 영향 (Effect of Ageing Temperature and Time on the Meat Quality of Longissimus Muscle from Hanwoo Steer)

  • 김진형;조수현;성필남;하경희;김학균;박범영;이종문;김동훈;안종남
    • 한국축산식품학회지
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    • 제27권2호
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    • pp.171-178
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    • 2007
  • 본 연구는 숙성온도와 숙성기간이 한우 거세우 배최장근의 육질 특성에 미치는 영향을 구명하고자 숙성온도를 0, $4^{\circ}C$로 하여 2, 7, 14, 21, 28, 49일 동안 숙성하면서 한우 거세우 배최장근의 pH, 전단력, MFI, 가열 및 육즙감량, 전자현미경 관찰, 관능검사 및 아미노산 조성을 분석하였다. pH는 숙성온도가 $0^{\circ}C$일 때 숙성 21일까지, 숙성온도가 $4^{\circ}C$일 때 숙성 14일까지 증가하다가 감소하였다(p<0.05). 전단력 값은 숙성 14일부터 28일까지 $4^{\circ}C$에서 숙성한 배최장근이 $4^{\circ}C$보다 유의적으로 낮았고, 숙성기간이 경과함에 따라 유의적으로 연도가 향상되었다(p<0.05). MFI의 경우 $4^{\circ}C$에서 숙성한 배최장근 보다 $0^{\circ}C$에서 높은 경향을 보였고, 숙성기간이 경과함에 따라 유의적으로 증가하였다(p<0.05). $0^{\circ}C$에서 숙성한 배최장근의 가열 및 육즙감량이 $4^{\circ}C$보다 적은 경향이었고, 숙성기간이 경과함에 따라 유의적으로 증가하였다(p<0.05). 관능검사에서 연도와 다즙성은 $0^{\circ}C$에서 숙성한 배최장근이 $4^{\circ}C$ 보다 좋은 평가를 보였고, 숙성기간이 경과하면서 유의적으로 높은 평가를 얻었다(p<0.05). 전자현미경에 의한 미세구조 변화는 $4^{\circ}C$에서 숙성한 배최장근이 $0^{\circ}C$보다 1주일 빠르게 Z-disk의 붕괴가 확실하게 관찰되었고, 숙성기간이 경과하면서 Z-disk의 붕괴정도가 많아졌다. 아미노산 함량 변화는 $4^{\circ}C$에서 숙성한 배최장근이 $0^{\circ}C$보다 높은 경향이었고, 숙성기간이 경과하면서 각 아미노산 조성의 함량이 유의적으로 증가하였다(p<0.05). 이상의 결과를 종합하면, 한우 거세우 등심의 최적 숙성 조건은 $0^{\circ}C$에서는 14일간, $4^{\circ}C$에서는 7일간 숙성하는 것이 바람직한 것으로 사료되며, 향후 숙성기술의 산업적 적용을 위하여 한우의 부위 및 근육별 적정 숙성기간 설정 연구가 필요할 것으로 생각된다.

Al-Li-( Cu, Zr) 합금에서 시효에 따른 δ' 상의 형상 및 입자크기분포의 변화 (The Changes of the Shape and Particle Size Distribution of δ' Phase on Ageing in Al-Li-( Cu, Zr) Alloys)

  • 우기도;조현기
    • 열처리공학회지
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    • 제7권2호
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    • pp.96-102
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    • 1994
  • The present work was aimed to examine the changes of the shape and particle size distribution(PSD) of ${\delta}^{\prime}$ particles on ageing in Al-Li-(Cu, Zr) alloys which had low density, high specific strength and stiffness, Increasing ageing time and temperature resulted in particles whose aspect ratio tended toward 1. The aspect ratio of ${\delta}^{\prime}$ particles was not dependent upon the ageing temperature and time in Al-Li-Cu alloy but was dependent upon them in Al-Li-Zr alloy. The PSD of ${\delta}^{\prime}$ particles in Al-Li-Zr alloy skewed to the right hand compared with that in Al-Li-Cu alloy, because $Al_3Zr$ phase in Al-Li-Zr alloy formed before ageing promoted the precipitation and growth of ${\delta}^{\prime}$ phase. Therefore, the PSD of the ${\delta}^{\prime}$ particles was found to be affected by the presence of $Al_3Zr$ particles. The growth rate of ${\delta}^{\prime}$ phase was not affected by the existence of the third transition phase $T_1$ formed by the addition of Cu in Al-Li alloy but was affected by the existence of $Al_3Zr$ formed by the addition of Zr in Al-Li alloy.

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pH and Colour Characteristics of Carcasses of Broilers Fed with Dietary Probiotics and Slaughtered at Different Ages

  • Karaoglu, Mevulut;Aksu, M.I.;Esenbuga, N.;Macit, M.;Durdag, H.
    • Asian-Australasian Journal of Animal Sciences
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    • 제19권4호
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    • pp.605-610
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    • 2006
  • The objective of the present experiment was to determine the effects of slaughtering at different ages and the use of a commercial probiotic (115-Biogallinox) in broiler diets on the color properties of carcasses, during the first 24 h following slaughter. Ross 308 male broiler chickens obtained from a commercial hatchery were raised to either 35 or 42 days of age. Chickens were fed with different levels of probiotic ($P_0$: 0.0%, $P_1$: 0.1% and $P_2$: 0.2%) containing Saccharomyces cerevisiae during the experimental period. At the end of the trial all birds were slaughtered and then stored at $3^{\circ}C$ for 24 h. The pH and skin colour of carcasses were determined 1, 3, 7, 10, 13, 17 and 24 h after slaughter. Although the use of probiotic and post-mortem ageing time affected the pH (p<0.01), it was not affected by slaughter age (35 and 42 days) (p>0.05). The highest pH values occurred in carcasses of broilers fed 0.2% probiotic. The pH values of carcasses decreased with post-mortem ageing time (p<0.01). Main factors (treatment, slaughter age and post-mortem ageing time) had an effect on colour ($L^*$, $a^*$ and $b^*$) values (p<0.01). $L^*$ values of 42d-old slaughter and $P_2$ group were lower than those of 35d-old slaughter and other probiotic groups. The $a^*$ and $b^*$ values of 35d-old slaughter were lower than those of 42d-old slauhgter. The $a^*$ and $b^*$ values increased during post-mortem ageing (p<0.01). It was determined that changing of the colour traits of broiler carcasses was correlated with probiotic, pH and post-mortem ageing time. Also, it was observed that darkness of carcass colour increased as time progressed.

Influence of commercial detergents on UF membrane ageing: Case of drinking water

  • Moulin, P.;Regula, C.;Carretier, E.;Wyart, Y.;Sergent, M.;Gesan-Guiziou, G.;Ferry, D.;Vincent, A.;Boudot, D.
    • Membrane and Water Treatment
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    • 제4권1호
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    • pp.27-51
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    • 2013
  • During cleaning steps, ultrafiltration membranes are mechanically and chemically stressed. This may result in membrane degradations and failures. In this paper, polysulfone membranes were used to evaluate membrane deteriorations by commercial detergents in static conditions. Ageing of the membrane was simulated by immersing samples in solutions containing commercial detergents with various concentrations, temperatures and times defined by experimental designs. Indeed, an innovative approach in the chemical membranes ageing researches, based on methodological tools, was used in order to achieve significant ageing experiments without using an accelerated ageing protocol. The macroscopic changes were monitored by permeability measurements and mechanical strength tests coupled with a microscopic characterization by ATR-FTIR and HRSEM. The present work details results obtained for three commercial detergents: an alkaline, an acidic and an enzymatic detergent. It was found that the detergents used in the industrial advised conditions (concentration, temperature and time of contact) were not detrimental for membrane properties (permeability and elongation at break) and so for the quality of the produced water. Over the industrial cumulated time of contact, different ageing effects can be observed and compared with the ones induced by NaOCl.

시판치과주조용 고금합금의 물리적 성질 및 상변태 (Physical Property and Phase Transformation in a Commercial Dental Casting High Gold Alloy)

  • 이희경;박명호;이화식
    • 대한치과기공학회지
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    • 제28권1호
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    • pp.27-41
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    • 2006
  • The physical property and phase transformation in a commercial dental casting high gold alloy was investigated as a function of ageing temperature and time using microvickers hardness tester, X-ray diffraction, optical and electron microscopy and EPMA analyser. 1. With increasing ageing time, the hardness of solution-treated gold alloys increased slowly at the initial stage of ageing treatment at an ageing temperature of $300{\sim}400^{\circ}C$, and it reached a maximum value of hardness at the medium stage. Finally, it decreased gradually during further ageing. The maximum value of hardness at was similar with that of the conventional materials and suitable for using as the crown & bridge. 2. During isothermal ageing at a temperature range of $300{\sim}400^{\circ}C$, three phases consisting of the Au-rich ${\alpha}_1$phase with a face-centered cubic structure, the Pt3Zn ${\alpha}_2$phase with an ordered AuCu3(L12) type(f.c.c.) and the Pt-rich ${\alpha}_3$phase with face-centered cubic structure in solution-treated gold alloys were transformed into different three phases consisting of the ${\alpha}_1$phase, the ${\alpha}_3$phase and the PtZn $\beta$phase with an ordered AuCu I(L10) type. 3. The hardening of gold alloys was attributed to the lattice strains of the matrix resulting from the transformation of the ${\alpha}_2$phase to the $\beta$phase. 4. The softening of gold alloys during over-ageing was attributed to the coarsening of the nodules consisting of the $\beta$phase and ${\alpha}_1$matrix.

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열분석법에 의한 Cu를 함유한 HSLA강의 시효 거동에 관한 연구 (A Study on the Ageing Behavior of Cu-bearing HSLA steels by thermal analysis)

  • 박태원;심인옥;김영우;강정윤
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 1994년도 특별강연 및 춘계학술발표 개요집
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    • pp.44-47
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    • 1994
  • The ageing behavior of Cu-bearing HSLA steels was studied by using Differential scanning calorimetry(DSC), Transmission electron microscopy and hardness tester. Two heat evolution peaks were observed during DSC scans over the temperature range of 25~590$^{\circ}C$ at a heating rate of 5$^{\circ}C$/min. The peaks appeared in low (241∼319$^{\circ}C$ : HSLA-A, 224∼310$^{\circ}C$ : HSLA-B) and high temperature (514∼590$^{\circ}C$ : HSLA-A, 451∼558$^{\circ}C$ : HSLA-B) are attributed to the formation of coherent Cu-clusters and noncoherent $\varepsilon$-Cu phase, respectively. It was confirmed that as ageing proceeds, the coherent bcc Cu-clusters transform to noncoherent fcc $\varepsilon$-Cu phase. In the case of the ageing to peak hardness at 300$^{\circ}C$ and 400$^{\circ}C$, the coherent Cu-clusters contributed to the hardening. As ageing time and temperature increase over peak hardness, noncoherent $\varepsilon$-Cu are formed and hardness decreases.

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EXTENSION OF OPERATIONAL LIFE-TIME OF WWER-440/213 TYPE UNITS AT PAKS NUCLEAR POWER PLANT

  • Katona, Tamas Janos;Ratkai, Sandor
    • Nuclear Engineering and Technology
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    • 제40권4호
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    • pp.269-276
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    • 2008
  • Operational license of WWER-440/213 units at Paks NPP, Hungary is limited to the design lifetime of 30 years. Prolongation by additional 20 years of the operational lifetime is feasible. Moreover, enhancement of the reactor thermal power by 8% will increase both the net power output and the competitiveness of the plant. Paks NPP is a pioneer considering the power up-rate and preparation of long-term operation of WWER-440/213 design. Systematic preparatory work for long-term operation of Paks NPP has been started in 2000. A regulatory framework and a comprehensive engineering practice have been developed. According to the authors view, creation of a gapless engineering system via consequent application of best practices, and feed-back of experiences together with proper consideration of WWER-440/V213 features are the decisive elements of ensuring the safety of long-term operation. That systematic engineering approach is in the focus of recent paper. Key elements of justification and measures for ensuring the safety of long-term operation of Paks NPP WWER-440/213 units are identified and discussed. These are the assessment of plant condition and review of adequacy of ageing management programmes, also the review, validation and reconstitution of time limited ageing analyses as core tasks of licence renewal.