• Title/Summary/Keyword: adhesive layer

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SELF-ADHESION OF LOW-VISCOSITY COMPOSITES TO DENTIN SURFACE (상아질에 대한 저점도 복합레진의 자가접착에 관한 연구)

  • Cho, Tae-Hee;Choi, Kyoung-Kyu;Park, Sang-Hyuk;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.28 no.3
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    • pp.209-221
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    • 2003
  • The objectiveness of this study was to evaluate whether low-viscosity composite can bond effectively to dentin surface without bonding resin. The low-viscosity composites being 50wt% filler content were made by the inclusion of bonding resin of two self-etching systems(Cleafil SE Bond, Unifil Bond) varied with contents as 0, 10, 20, 30, 40, 50wt%. Exposed dentin surfaces of extracted 3rd molars are used. Dentin bond strengths were measured. The tests were carried out with a micro-shear device placed testing machine at a CHS of 1mm/min after a low-viscosity composite was filled into an iris cut from micro tygon tubing with internal diameter approximately 0.8mm and height of 1.0mm. 1 Flexural strength and modulus was increased with the addition of bonding resin. 2. Micro-shear bond strength to dentin was improved according to content of bonding resin irrespective of applying or not bonding resin in bonding procedure, and that of Clearfil SE Bond groups was higher than Unifil Bond. 3. There were no significant difference whether use of each bonding resin in bonding procedure for S-40, S-50, U-50(p>0.05). 4. In SEM examination, resin was well infiltrated into dentin after primed with self-etching primer only for S-50 and U-50 in spite of the formation of thinner hybrid layer. Low viscosity composite including some functional monomer may be used as dentin bonding resin without an intermediary bonding agent. It makes a simplified bonding procedure and foresees the possibility of self-adhesive restorative material.

Corrosion Resistance Characteristics of Cold Rolled Steel by Cr-free Green Organic/Inorganic Hybrid Coating Solution (크롬 프리 친환경 유/무기 하이브리드 코팅액에 의한 냉연강판의 내식특성)

  • Nam, Ki Woo;Kim, Jung Ryang;Choi, Chang Min
    • Journal of Ocean Engineering and Technology
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    • v.27 no.2
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    • pp.33-38
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    • 2013
  • In the past, a very popular method for reducing the corrosion on zinc involved the use of chemical conversion layer coatings based on $Cr^{+6}$. However, there is an important problem with using chromium salts as a result of restrictive environmental protection legislation. This study investigated the optimum condition for galvanized steel using an organic/inorganic solution with a Ti composition. In the case of a fixed heat treatment time, the corrosion resistance values of LR-0727(1) and LR-0727(2) were improved as the heat treatment temperature increased, and the optimum minimum temperature decreased with the heat treatment time. At the optimum heat treatment condition of two coating solutions, the heat treatment time of the LR-0727(1) solution was shorter than LR-0727(2) for the same heat treatment temperature. LR-0727(1) coated specimens did not show desquamation, and all of the specimens showed a good adhesive property. In contrast, in the case of the LR-0727(2) coated specimens, desquamation arose. Therefore, the adhesive property of LR-0727(1) was superior to that of LR-0727(2). The pencil hardness had a 3H average for all of the coating solutions and heat treatment conditions. In the case of a corrosion resistance test with boiling water, the coated specimens of LR-0727(1) were discolored, but LR-0727(2) was not. Finally, LR-0727(1) was more moisture proof than LR-0727(2).

A New Steel Jacketing Method for Concrete Cylinders and Comparison of the Results with a Constitutive Model

  • Choi, Eun-Soo;Kim, Man-Cheol
    • International Journal of Railway
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    • v.1 no.2
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    • pp.72-81
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    • 2008
  • This paper introduces a new steel jacketing method for reinforced concrete columns with lap splice and evaluates its performance by a series of axial tests of concrete cylinders. At first, 45 concrete cylinders were fabricated with varying the design compressive strengths of 21, 27 and 35 MPa and, then, the part of them was jacketed with two-split-steel jackets under lateral confining pressure. The parameters in the first test were the steel jacket's thickness and the existence of adhesive between steel and concrete surface. In the second test, whole steel jackets were used to wrap cylinders with lateral pressure. Also, a double-layer jacket consisted of two steel plates was introduced; a cylinder was jacketed by two steel plates one after another. The effect of the new method was verified through comparing the results of the compressive tests for plain and jacketed cylinders. The steel jacket built following the new method showed good results of increasing the compressive strength and ductility of the jacketed cylinders with respect to the plain cylinders. The thicker steel jackets showed the more increased compressive strength, and the ductility at failure depended on the welding quality on steel jackets. The adhesive between steel and concrete surface reduced the confining effect of the steel jackets. The whole jacket showed more ductile behavior than the two-split jackets. The double-layered jackets were estimated to possess an equal performance to that of a single steel jacket having the same thickness of the double-layered jacket. Finally, the experimental results were compared with the constitutive model of steel-jacketed concrete; which showed a good agreement between the experimental results and the models.

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Oxidation-treated of Oxidized Carbons and its Electrochemical Performances for Electric Double Layer Capacitor (산화처리 탄소의 전기화학적 거동 및 이를 이용한 EDLC 특성)

  • Yang, Sun-Hye;Kim, Ick-Jun;Jeon, Min-Je;Moon, Seong-In;Kim, Hyun-Soo;An, Kye-Hyeok;Lee, Yun-Pyo;Lee, Young-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.481-481
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    • 2007
  • This work describes the effect of the number of roll pressing and the composition of carbon black on the electric and mechanical properties of carbon-PTFE electrode, in which composition is MSP 20 : carbon black: PTFE = 95-x : x : 5 wt.%. It was found that the best electric and mechanical properties were obtained in sheet electrode roll-pressed for about 15 times and in sheet electrode, in which composition is MSP 20 : carbon black: PTFE = 80 : 15 : 5 wt.%. These behaviors could be explained by the network structure of PTFE fibrils and conducting paths linked with carbon blacks, respectively. On the other hand, cell capacitor using the sheet electrode with 15 wt.% of carbon black attached on aluminum current collector with the electric conductive adhesive, in composition is carbon black : CMC = 70 : 30 wt.%, has exhibited the best rate capability in the current range of $0.5mA/cm^2$ $100mA/cm^2$ and the lowest equivalent series resistance.

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Properties of Glued Laminated Timber Made from Fast-growing Species with Mangium Tannin and Phenol Resorcinol Formaldehyde Adhesives

  • Hendrik, Jessica;Hadi, Yusuf Sudo;Massijaya, Muh Yusram;Santoso, Adi;Pizzi, Antonio
    • Journal of the Korean Wood Science and Technology
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    • v.47 no.3
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    • pp.253-264
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    • 2019
  • This study characterized the chemical compounds in tannin from mangium (Acacia mangium) bark extract and determined the physical-mechanical properties of glued laminated timber (glulam) made from sengon (Falcataria moluccana), jabon (Anthocephalus cadamba), and mangium wood. The adhesives used to prepare the glulam were based on mangium tannin and phenol resorcinol formaldehyde resin. Five-layer glulam beams measuring $5cm{\times}6cm{\times}120cm$ in thickness, width, and length, respectively, were made with a glue spread of $280g/m^2$ for each glue line, cold pressing at $10.5kgf/cm^2$ for 4 h and clamping for 20 h. Condensed mangium tannin consisted of 49.08% phenolic compounds with an average molecular weight of 4745. The degree of crystallinity was 14.8%. The Stiasny number was 47.22%. The density and the moisture content of the glulams differed from those of the corresponding solid woods with mangium having the lowest moisture content (9.58%) and the highest density ($0.66g/cm^3$). The modulus of rupture for all glulam beams met the JAS 234-2003 standard but the modulus of elasticity and the shear strength values did not. Glulam beams made with tannin had high delamination under dry and wet conditions, but glulam made from sengon and jabon wood met the standard's requirements. All glulam beams had low formaldehyde emissions and were classified as $F^{****}$ for formaldehyde emissions according to the JAS 234 (2003) standard.

Experimental Study on Mode-I Energy Release Rate of Polypropylene Adhesive Layer Manufactured by Microwave Composite Forming Process (마이크로파 복합재 성형 공정을 이용한 폴리프로필렌 접착층의 모드 I 에너지 해방률에 대한 실험적 연구)

  • Park, E.T.;Kim, T.J.;Kim, J.;Kang, B.S.;Song, W.J.
    • Transactions of Materials Processing
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    • v.31 no.1
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    • pp.29-38
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    • 2022
  • Recently, the composite material market is gradually growing. Various composite forming processes have been developed in order to reduce the production cost of the composite material. Unlike the conventional forming process, the microwave composite forming process has the advantage of reducing the processing time because the composite material is heated directly or indirectly at the same time. Due to this advantage, in this study, a double cantilever beam test was conducted with specimens manufactured by the microwave composite forming process. The purpose of this study was to compare mode-I energy release rate for specimens manufactured by prepreg compression forming and microwave composite forming processes. First, a microwave oven was proposed to conduct the microwave composite forming process. Double cantilever beam specimens were manufactured. After that, the double cantilever beam test was conducted to obtain the mode-I energy release rate. Mode-I energy release rates of specimens manufactured by the microwave composite forming and prepreg compression forming processes were then compared. As a result, mode-I energy release rates of specimens fabricated by the microwave composite forming process were similar to those fabricated with the prepreg compression forming process with a relatively reduced process time.

Acoustic Emission Characteristics and Fracture Behaviors of GFRP-Aluminum Honeycomb Hybrid Laminates under Compressive and Bending Loads (GFRP-알루미늄 하니컴 하이브리드 적층판의 압축 및 굽힘 파괴거동과 음향방출해석)

  • Lee, Ki-Ho;Gu, Ja-Uk;Choi, Nak-Sam
    • Composites Research
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    • v.22 no.6
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    • pp.23-31
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    • 2009
  • This paper investigated acoustic emission (AE) characteristics in association with various fracture processes of glass fiber reinforced plastic skin/ aluminum honeycomb core (GF-AH) hybrid composites under compressive and bending loads. Various failure modes such as skin layer fracture, skin/core interfacial fracture, and local plastic yield buckling and cell wall adhesive fracture occurring in the honeycomb cell wall were classified through the fracture identification in association with the AE frequency and amplitude analysis. The distribution of the event-rate in which it has a high amplitude showed a procedure of cell wall adhesive fracture, skin/core interfacial debonding and fiber breakage, whereas distribution of different peak frequencies indicated the plastic deformation of aluminum cell wall and the friction between honeycomb walls. Consequently, the fracture behaviors of GF-AH hybrid composites could be characterized through a nondestructive evaluation employing the AE technique.

A Study on the Application of Dobak-glue for Fixation Painting Layer of Earthen Mural (토벽화 채색층 고착처리를 위한 도박풀 적용 연구)

  • Kim, Seol Hui;Han, Kyeong Soon;Lee, Hwa Soo
    • Journal of Conservation Science
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    • v.33 no.6
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    • pp.553-564
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    • 2017
  • This report compared and analyzed the degree of surface change and results of a deterioration experiment to assess the possibility of using Dobak glue as an adhesive in the fossilizing treatment of the paint layer in earthen mural paintings. The weathering experiments were performed with a color-difference meter (CR-400, MINOLTA). After the experiment, Cinnabar 3% specimens, which exhibited diverse changes in the durability test, were additionally tested with a reflection-transmission device (CARY-5000, AGILENT). Post UV degradation, most of the Dobak-glue samples exhibited lesser color change than animal-glue samples, and after moisture absorption and drying, the 0.5% and 3% Dobak samples displayed a lower degree of change in the value of color difference. Furthermore, results of the reflection-transmission test after deterioration indicated that Dobak glue presented a lesser color change than animal glue. Therefore, if Dobak glue is used as a consolidating agent, discoloration on account of degradation is minimal.

Design Analysis/Manufacturing /Performance Evaluation of Curved Unsymmetrical Piezoelectric Composite Actuator LIPCA (곡면형 비대칭 압전복합재료 작동기 LIPCA의 설계해석/제작/성능평가)

  • Gu, Nam-Seo;Sin, Seok-Jun;Park, Hun-Cheol;Yun, Gwang-Jun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.10
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    • pp.1514-1519
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    • 2001
  • This paper is concerned with design, manufacturing and performance test of LIPCA ( Lightweight Piezo- composite Curved Actuator) using a top carbon fiber composite layer with near -zero CTE(coefficient of thermal expansion), a middle PZT ceramic wafer and a bottom glass/epoxy layer with high CTE. The main point of this design is to replace the heavy metal layers of THUNDER by thigh tweight fiber reinforced plastic layers without losing capabilities to generate high force and large displacement. It is possible to save weight up to about 30% if we replace the metallic backing material by the light fiber composite layer. We can also have design flexibility by selecting the fiber direction and the size of prepreg layers. In addition to the lightweight advantage and design flexibility, the proposed device can be manufactured without adhesive layers when we use epoxy resin prepreg system. Glass/epoxy prepregs, a ceramic wafer with electrode surfaces, and a graphite/epoxy prepreg were simply stacked and cured at an elevated temperature (177 $^{circ}C$ after following an autoclave bagging process. It was found that the manufactured composite laminate device had a sufficient curvature after detached from a flat mold. The analysis method of the cure curvature of LIPCA using the classical lamination theory is presented. The predicted curvatures are fairly in agreement with the experimental ones. In order to investigate the merits of LIPCA, a performance test of both LIPCA and THUNDE$^{TM}$ were conducted under the same boundary conditions. From the experimental actuation tests, it was observed that the developed actuator could generate larger actuation displacement than THUNDERT$^{TM}$.

Transmit-receive Module for Ka-band Seekers using Multi-layered Liquid Crystal Polymer Substrates (다층 액정폴리머 기판을 이용한 Ka대역 탐색기용 송수신 모듈)

  • Choi, Sehwan;Ryu, Jongin;Lee, Jaeyoung;Lee, Jiyeon;Nam, ByungChang
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.20 no.5
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    • pp.63-70
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    • 2020
  • In this paper, the transmit-receive module for military seekers has been designed and fabricated in 35 GHz. To increase the performance of substrates and high integration of circuits in millimeter-wave band, a 4-layer LCP(Liquid Crystal Polymer) substrate was developed. This substrate was implemented with three FCCL substrates and two adhesive layers, and a process using the difference in melting point between the substrates was used for lamination. Using a strip line and a microstrip line was confirmed by the transmission loss along the length of the substrate, and the performance of LCP substrates was validated with a power divider in 35 GHz. After confirming the performance of individual blocks such as power amplifier and low noise amplifier, a single channel Ka-band transmission/reception module was developed using a 4-layer liquid crystal polymer substrate. The transmit power of this module has above 1.1W in pulse duty 10% and has an output power of 1.1W and it has receive noise figure less than 8.5 dB and receive gain more than 17.6 dB.