• 대한치과교정학회지
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• 제12권2호
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• pp.139-144
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• 1982

저자(著者)는 3가지 종류(種類)의 bracket을 교정(矯正)을 위(爲)해서 발치(拔齒)한 20개(個)씩의 소구치(小臼齒)에 접착(接着)하여 24시간(時問) 후(後)에 인장강도(引張?度)를 측정(測定)한 결과(結果) 다음과 같은 결론(結論)을 얻었다. foil-mesh base bracket과 photo-etched base bracket의 평균인장강도(平均引張强度)는 통계학적(統計學的)으로 유의(有意)한 차(差)가 없으며, plastic bracket은 인장강도(引張强度) 측정(測定) 시(時) wing의 변형(變形)에 의(依)해서 정확(正確)한 측정(測定) 결과(結果)를 얻을 수 없 었다. 접착제(接着劑)가 떨어진 양상(樣相)은 foil-mesh base bracket과 photo-etched base bracket에서 접착제(接着劑)가 치아(齒牙)와 bracket 에 부분적(部分的)으로 붙어서 떨어진 것이 각기(各其) 50%로 가장 많았고, 접착제(接着劑)가 치아(齒牙)에만 붙어서 떨어진 것 (30%, 35%), 접착제(接着劑)가 bracket에만 붙어서 떨어진 것 (20%, 15%) 순(順)으로 나타났다.

• 대한치과보철학회지
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• 제44권4호
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• pp.383-393
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• 2006

Statement of problem : Limited research on flowable resin has been undertaken on its application directly on dentin associated with the adhesive systems. Purpose : This study was to evaluate the shear bond strengh and fracture aspect of flowable resin on human dentin with various types of dentin bonding adhesives with thermo cycling effect. Materials and methods: Filtek-Flow(3M ESPE, USA) was used as flowable resin and Eighty human molars were randomly divided into 4 groups : three dentin bonding adhesives (Scotchbond-Multipurpose : 3-step contentional system, One-Step : One-bottle system. Prompt L-Pop : All-in-one, self-etching primer) and 32% etching treatment without bonding adhesive as a control group. For evaluating their durability of bonding, each group was subdivided : storaging in the water at 37$^{\circ}C$(24 hours) and thermocycling (0$^{\circ}C$-55$^{\circ}C$, 30 seconds intervals, 1000 cycle). Shear bond strength tests were performed and resin-dentin interface and fracture mode were observed. Results were analysed by one-way ANOVA and Scheffe's multiple range test. Results and Conclusion : 1. At 0 cycle, the mean shear bond strength of One-Step exhibited the highest value of all groups(p<0.05), and there were no significant differences between Prompt L-Pop and Scotchbond-Multipurpose, Scotchbond-Multipurpose and control(p>0.05). After 1000 thermocycling, One-Step exhibited higher value than other groups(p<0.05), and there were no significant differences among other groups (p>0.05). 2. The shear bond strength of each group was significantly decreased after thermocycling except Scotchbond-Multipurpose (p>0.05). 3. The most common failure mode was adhesive type and mixed type, next in order.

• Restorative Dentistry and Endodontics
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• 제26권4호
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• pp.316-325
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• 2001

The purpose of this study was to evaluate the effect of adhesive curing timing on the direction of polymerization shrinkage of light-curing composite resin. In this study, the curing times of adhesive and composite resin were measured by differential scanning calorimeter(DSC). 28 extracted human molars were embedded in clear resin and box-type cavities were prepared. Based on DSC data, the experimental teeth were divided into 4 groups. Group 1: no bond; Group 2: late curing; Group 3: Intermediate curing; Group 4: Early curing. After treating with adhesive, the buccal cavities were filled with Z-100 hybrid composite resin and the lingual ones were filled with AEliteflo flowable composite resin. The depressions at the surface were measured by surface profilometer, then the specimens were embedded in clear resin and sectioned. Impressions were obtained and used to get epoxy resin replicas. The epoxy replicas were gold-coated and observed under SEM. Average Maximum Gap(AMG), Gap Proportion(GP), Average Marginal Index(AMI) were used to compare the shrinkage gap of each group. The results were statistically analyzed using the Kruskal-Wallis One Way ANOVA, Student-Newman-Keuls method. The results of this study were as follows. 1. Average Maximum Gap, Gap Proportion, Average Marginal Index and depression at the surface or Z-100 hybride composite resin were smaller than those of AEliteflo flowable composite resin(P<0.05). 2. When the bonding between composite resin and tooth structure was strong, the shrinkage gap was small, and depression at the surface was deep(P<0.05). 3. In the well-bonded group, light-curing composite resin shrank toward bonded cavity wall, not toward light source. The result suggested that the direction of polymerization shrinkage was affected by the quality of bonding in the dentin-resin interface. The strong was the bonding between composite resin and tooth structure, the smaller was the gap and the deeper was the depression at the surface. Then the flow to compensate the polymerization shrinkage proceeded from surface to bonded cavity wall.

• 대한치과교정학회지
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• 제20권3호
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• pp.583-591
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• 1990

If the bond strength is sufficient to resist orthodontic force, orthodontic brackets can be bonded to restorations. Orthodontic brackets were bonded to composite resin and glass ionomer cement restorations with no-mix adhesive or glass ionomer cement. The shear bond strength of adhesives bonded to restorations was studied in vitro. Orthodontic brackets were bonded to 10 extracted natural teeth, 40 composite resin restorations and 40 glass ionomer restorations. The surfaces of composite resin restorations were roughened or applied with bonding agent (Scothbond) after surface roughening. The surfaces of glass ionomer cement restorations were conditioned with acid etching or applied with Scotchbond to etched surface. The adhesive was no-mix resin or glass ionomer cement. The shear bond strength was measured. The results were as follows: 1. Orthodontic brackets could be bonded to composite resin restorations effectively as they could be bonded to acid etched enamel with no-mix adhesive. The shear bond strength was sufficient to resist orthodontic force and was not affected by bonding agent greatly. 2. The shear bond strength of no-mix adhesive bonded to acid etched glass ionomer cement restorations was sufficient to resist orthodontic force. However. the fracture risk of glass ionomer cement restorations was increased during debonding. The bonding agent couldn't increase the shear bond strength greatly. 3. The shear bond strength of glass ionomer cement bonded to glass ionomer cement restorations was lower than that of no-mix adhesive. The shear bond strength was sufficient to resist orthodontic force and was greatly decreased by bonding agent. 4. The shear bond strength of glass ionomer cement bonded to composite resin restorations was too low to resist orthodontic force.

• Composites Research
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• 제17권6호
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• pp.14-21
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• 2004

본 연구에서는 몇 가지 접합 방법에 따라 일방향 복합재료 단일 겹치기 접합 조인트의 파손 과정, 모드 및 강도를 실험적으로 평가하였다 접합 방법으로는 접착제 없는 동시성형, 접착제를 사용한 동시성형 및 이차 접합의 세 가지를 고려하였다 또한 이차 접합 조인트에서 몇 가지 파라미터의 영향도 살펴보았다. 접착제 없는 동시성형 시편은 가장 우수한 조인트 강도를 나타내었다. 이차접합 조인트에서는 접착제 층의 점진적인 파손이 발생하였다. 접착제의 재료 및 접합 강도가 상대적으로 강한 필름 접착제의 동시성형 조인트는 갑작스런 층간분리 파손이 발생하였으며 이차 접합 조인트보다 더 낮은 파손 강도를 나타내었다. 이차 집합 조인트에서 층간분리 파손이 발생하지 않은 것은 접착제 층에서의 균열 진전 및 점진적 파손이 층간분리 파손을 방지한 것으로 보인다. 따라서 복합재료 접합 조인트의 파손 강도는 접착제의 재료 강도 또는 접착 성능과 항상 비례하지 않으며 이것은 복합재료가 층간 분리 파손에 약하기 때문이다.

• Composites Research
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• 제23권6호
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• pp.32-38
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• 2010

폴리아미드 직물과 NBR의 최적 접착특성을 나타낼 수 있는 조건을 검토하기 위해 대기압 플라즈마(APP) 처리 효과에 대한 실험적 연구를 하였다. 대기압 화염 플라즈마(APFP) 처리의 경우 주어진 계면조건에서 최적의 처리횟수는 2회였다. APFP 처리 횟수가 증가함에 따라 직물의 열변형은 더욱 심하였다. APFP 처리 직물을 강화한 복합재료의 접착강도는 접착제를 한번 혹은 두번 도포한 계면에 대해 플라즈마를 처리하지 않은 경우에 비해 약 35% 증가하였다. 접착제를 중복 도포하였을 때, APFP 처리 직물 강화한 복합재료의 접착에너지는 약 4배 증가하였다. APFP 처리에 의한 폴리아미드 직물의 표면 개질이 다른 형태의 APP 처리방식과 비교했을 때, 경제적이고 빠르며 고무와의 접착강도를 개선시킬 수 있는 방법이라고 판단된다.

• The Journal of Advanced Prosthodontics
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• 제1권1호
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• pp.41-46
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• 2009

STATEMENT OF PROBLEM. The poor chemical bonding of a denture base resin to cast titanium framework often introduces adhesive failure and increases microleakage. PURPOSE. This study evaluated the shear bond strengths of a heat cure denture base resin to commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy using two adhesive primers. MATERIAL AND MATHODS. Disks of commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy were cast. Specimens without the primer were also prepared and used as the controls. The shear bond strengths were measured on a screw-driven universal testing machine. RESULTS. The primers significantly(P < .05) improved the shear bond strengths of the heat cure resin to all metals. However, the specimens primed with the Alloy $primer^{(R)}$(MDP monomer) showed higher bond strength than those primed with the MR $bond^{(R)}$(MAC-10 monomer) on titanium. Only adhesive failure was observed at the metal-resin interface in the non-primed specimens, while the primed specimens showed mixed failure of adhesive and cohesive failure. CONCLUSIONS. The use of appropriate adhesive metal primers makes it possible not only to eliminate the need for surface preparation of the metal framework before applying the heat cure resins, but also reduce the need for retentive devices on the metal substructure. In particular, the Alloy $primer^{(R)}$, which contains the phosphoric acid monomer, MDP, might be clinically more acceptable for bonding a heat cure resin to titanium than a MR $bond^{(R)}$, which contains the carboxylic acid monomer, MAC-10.

• Restorative Dentistry and Endodontics
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• 제20권1호
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• pp.113-128
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• 1995

The purpose of this study was to investigate the effect of stannous fluoride on the dentin bonding with three kinds of commercially available dentin bonding systems containing different adhesive monomers. Dentin specimens with exposed labial dentin prepared from freshly extracted bovine mandibular anterior teeth were divided into experimental and control groups. The specimens of experimental groups were bonded with dentin bonding systems and composite resins including All bond 2 ㅡ& Bisfil, Scotchbond Multi-Purpose & Z100, and Denthesive II Charisma after 2 % stannous& fluorided application for S minutes and washing for 1 minute. The specimens of control groups were bonded with the same dentin bonding systems and composite resins as used in the experimental groups. After bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, the tensile bond strength and cohesive failure rate were measured, and then the pretreated dentin surfaces and the fractured dentin surfaces were examined under scanning electron microscope. The results were as follows : Mean bond strength of stannous fluoride applied groups of All bond 2, Scotchbond MP, and Denthesive II were 2.5MPa, 1.1MPa, and 1.1MPa respectively, and those of control groups were 7.5MPa, 8.1MPa, and 4.6MPa. Bond strength values of stannous fluoride applied groups were significantly lower than those of the control groups(p<0.05). SEM findings of dentin surfaces after stannous fluoride application demonstrated an appearance of partially remained smear layer and smear plugs inspite of pretreatment with 10 % phosphoric aicd or maleic acid solution, and an appearance of smear layer covered surface under Denthesive II priming. But those of control groups commonly showed clean dentin surfaces without smear layer and smear plugs. On SEM observation of the fractured dentin-resin interface, while most of the specimens of stannous fluoride applied groups showed adhesive failure mode, those of All bond 2 and Scotchbond MP control groups showed mainly adhesive-cohesive mixed failure mode, and mainly adhesive failure mode in Denthesive II control group.

• Restorative Dentistry and Endodontics
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• 제12권1호
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• pp.95-105
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• 1986

For the purpose of obtaining a basic data in selecting a suitable material with clinical care, this study was designed to measure the shear stress and to examine the fracture pattern of various dentin bonding restorative materials using 43 extracted bicuspids. The following results were obtained. 1. In dentin, Silux/Scotchbond group showed the highest value ($34.5{\pm}14.7kg/cm^2$) and Fuji Ionomer Type II group and Heliosit/Dentin-Adhesit group showed almost same bond strength in the next place. Durafill/Dentin-Adhesive group showed an infinitesimal value. ($3.1{\pm}1.4kg/cm^2$) 2. Every group showed no difference in bond strength between upper and lower teeth. Between buccal and lingual surfaces. Fuji Ionomer Type II and Durafill/Dentin-Adhesive groups showed too. But, in Silux/Scotchbond and Heliosit/Dentin-Adhesit groups, it was shown that the bond strength in lingual was stronger than in buccal. 3. There was resin fracture with cohesive fracture of bonding agent in Enamel group. In dentin, adhesive-cohesive fracture and adhesive fracture were shown. 4. The stronger bond strength was, the more frequently cohesive fracture occurred. Dentin-Adhesit group showed specific shining appearance as if varnish became hard.

• 대한기계학회논문집A
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• 제32권4호
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• pp.354-361
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• 2008

Cold rolled steel sheet for automotive was treated by Ar/$O_2$ atmospheric pressure plasma to improve the adhesive bonding strength. Through the contact angle test and calculation of surface free energy for cold rolled steel sheet, the changes of surface properties were investigated before and after plasma treatment. The contact angle was decreased and surface free energy was increased after plasma treatment. And the change of surface roughness and morphology were observed by AFM(Atomic Force Microscope). The surface roughness of steel sheet was slightly changed. Based on Taguchi method, single lap shear test was performed to investigate the effect of experimental parameter such as plasma power, treatment time and flow rate of $O_2$ gas. Results shows that the bonding strength of steel sheet treated in Ar/$O_2$ atmospheric pressure plasma was improved about 20% compared with untreated sheet.