• Title/Summary/Keyword: acceptable limit

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Effect of 50 ㎛ class granules on the Injection Behavior of Brushite Bone Cement Prepared via Pre-dissolution Route

  • Mun, Da Hye;Lee, Sang Cheon;Oh, Kyung-Sik
    • Journal of Powder Materials
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    • v.27 no.6
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    • pp.468-476
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    • 2020
  • The bone cement used for vertebroplasty must be sufficiently injectable. The introduction of granules reduces the amount of liquid required for liquefaction, implying that higher fluidity is achieved with the same amount of liquid. By employing β-tricalcium phosphate granules with an average diameter of 50 ㎛, changes in injectability are observed based on the paste preparation route and granular fraction. To obtain acceptable injectability, phase separation must be suppressed during injection, and sufficient capillary pressure to combine powder and liquid must work evenly throughout the paste. To achieve this, the granules should be evenly distributed. Reduced injection rates are observed for dry mixing and excessive granular content, owing to phase separation. All these correspond to conditions under which the clustered granules weakened the capillary pressure. The injected ratio of the paste formed by wet mixing displayed an inverted U-type shift with the granular fraction. The mixture of granules and powder resulted in an increase in the solid volume fraction, and a decrease in the liquid limit. This resulted in the enhancement of the liquidity, owing to the added liquid. It is inferred that the addition of granules improves the injectability, provided that the capillary pressure in the paste is maintained.

Establishment of analytical methods for allergenic compounds in mouthwashes and sanitary napkins by ultra-high-performance liquid chromatography with tandem mass spectrometry

  • Hee-Jung Sim;Hee-Jin Jeong;Yeong-In Lee;Yu-Jin Cho;Seung-Hoon Baek;Jong-Hwan Kim
    • Analytical Science and Technology
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    • v.36 no.2
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    • pp.89-98
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    • 2023
  • Analytical methods for detecting atranol, chloroatranol, evernic acid, (+)-usnic acid, and atranorin in sanitary napkins and mouthwashes were developed using ultrahigh performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS). UHPLC-MS/MS conditions were optimized for rapid, sensitive, and simultaneous analysis of the five allergenic compounds. The methods were validated by assessing their specificity, matrix effects, limit of detection (LOD), limit of quantification (LOQ), linearity, accuracy, and precision. Good linearity was achieved with a determination coefficient of ≥0.99. The LOD and LOQ were 2.1-9.8 and 6.4-29.6 ng/g for sanitary napkins and 0.29-0.48 and 0.87-1.45 ng/mL for mouthwashes, respectively. The accuracy and precision were within an acceptable range according to the criteria reported in the European SANTE/11813/2017 guidelines (70-120 % recovery, <20 % relative standard deviation). Therefore, these methods can be used to analyze atranol, chloroatranol, evernic acid, (+)-usnic acid, and atranorin in sanitary napkins and mouthwashes.

A Comprehensive Analysis of 3D Body Scanning vs. Manual Measurements in a Large-Scale Anthropometric Survey -Insights from the 8th Size Korea Project- (대규모 인체치수조사 사업에서 3차원 측정치와 직접측정치의 차이 분석 -제8차 사이즈코리아 사업을 중심으로-)

  • Sunmi Park
    • Journal of the Korean Society of Clothing and Textiles
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    • v.48 no.2
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    • pp.233-253
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    • 2024
  • This study analyzed differences between three-dimensional (3D) body scanning and manual measurements, aiming to assess whether 3D scanning can replace traditional anthropometric tools, such as tape measures and calipers. Data from 4,478 participants in the 8th Size Korea Project were analyzed, covering 43 measurement items. Since Given that the 3D and manual measurements were performed on the same subjects in the 8th Size Korea Project, it was possible to determine the correlation more accurately between the two measurement methods more accurately. Using Applying ISO 20685-1(2018) standards, 15 out of the 43 items fell within allowable error limits. When classified into six types, "small circumferences" and "segment lengths" showed averages of 3.35 mm and 3.10 mm, respectively, within acceptable range. "Body heights" and "body depths" slightly exceeded the limit, with averages of 5.28 mm and 6.58 mm. "Body widths" and "large circumferences" surpassed the limit, with means of 16.77 mm and 16.18 mm. The study offers an objective basis to for validate validating 3D measurements' measurements' reliability and accuracy, addressing various industries' needs for information on the human body's dimensions information.

Assessment of Available Coastal Groundwater Resources Using Strack's Single-potential Analytical Solution (Strack의 단일 포텐셜 해석해를 이용한 해안지하수 개발가능량 평가)

  • Cui, Lei;Lee, Chang-Hae;Park, Nam-Sik
    • Journal of Korea Water Resources Association
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    • v.41 no.1
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    • pp.27-34
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    • 2008
  • Groundwater development in coastal areas induces saltwater intrusion. In many cases amount of groundwater resources available for development is limited by a pre-specified limit of additional saltwater intrusion. In this paper a simple equation is developed to assess available groundwater resources which depends on the constraint of acceptable additional saltwater intrusion. Strack#s single-potential analytical solution is used to derive the equation. Available groundwater increases as more additional intrusion is allowed. However, critical points limit both the maximum pumping rate and the allowed saltwater intrusion limit. The equation is presented in the form of design curves from which the maximum pumping rate can be read off quickly. The equation and the design curves are suitable for preliminary estimation of available groundwater resources in coastal areas.

Development and Assessment of Real-Time Quality Control Algorithm for PM10 Data Observed by Continuous Ambient Particulate Monitor (부유분진측정기(PM10) 관측 자료 실시간 품질관리 알고리즘 개발 및 평가)

  • Kim, Sunyoung;Lee, Hee Choon;Ryoo, Sang-Boom
    • Atmosphere
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    • v.26 no.4
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    • pp.541-551
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    • 2016
  • A real-time quality control algorithm for $PM_{10}$ concentration measured by Continuous Ambient Particulate Monitor (FH62C14, Thermo Fisher Scientific Inc.) has been developed. The quality control algorithm for $PM_{10}$ data consists of five main procedures. The first step is valid value check. The values should be within the acceptable range limit. Upper ($5,000{\mu}g\;m^{-3}$) and lower ($0{\mu}g\;m^{-3}$) values of instrument detectable limit have to be eliminated as being unrealistic. The second step is valid error check. Whenever unusual condition occurs, the instrument will save error code. Value having an error code is eliminated. The third step is persistence check. This step checks on a minimum required variability of data during a certain period. If the $PM_{10}$ data do not vary over the past 60 minutes by more than the specific limit ($0{\mu}g\;m^{-3}$) then the current 5-minute value fails the check. The fourth step is time continuity check, which is checked to eliminate gross outlier. The last step is spike check. The spikes in the time series are checked. The outlier detection is based on the double-difference time series, using the median. Flags indicating normal and abnormal are added to the raw data after quality control procedure. The quality control algorithm is applied to $PM_{10}$ data for Asian dust and non-Asian dust case at Seoul site and dataset for the period 2013~2014 at 26 sites in Korea.

Estimation of the Total Dietary Intake of Saccharin by Korean Population (한국인의 삭카린 섭취량 산정)

  • Park, Se-Mi;Lee, Su-Rae
    • Korean Journal of Food Science and Technology
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    • v.24 no.6
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    • pp.563-567
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    • 1992
  • Out of 74 food samples including pickled radish, soy sauce, Lactobacillus drinks, frozen sweets and snack confections, 60 samples were found to contain saccharin. The contents of sacchrain in terms of maximum and positive mean were 541, 306 ppm in pickled radish, 302, 153 ppm in soy sauce, 66, 37 ppm in Lactobacillus drinks, 90, 51 ppm in frozen sweets and 606, 285 ppm in snack confections, respectively. Most food items did not exceed the tolerance limit of saccharin while 70% of snack confections exceeded the limit, the average concentration being 2.9 times of the limit. Total daily intake of saccharin by Korean population for the period of $1985{\sim}1990$ was estimated to be $7{\sim}17\;mg/person$ from consumption data and $9{\sim}35\;mg/person$ from supply data. The intake level was $11{\sim}22%$ of acceptable daily intake for man (ADI) recommended by FAO/WHO whereas the level was slightly higher than that in USA or Japan. It is. therefore, judged that saccharin at the current pattern of usage will not exhibit any adverse effect on the safety of Korean population.

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Comparison with Threshold Limit Value (TLV) of Menthol Cigarettes between Expert and Consumer Panel

  • Lee Seung-Yong;Lee Whan-Woo;Kim Young-Hoh
    • Journal of the Korean Society of Tobacco Science
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    • v.28 no.1
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    • pp.58-66
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    • 2006
  • Threshold limit value (TLV) test between expert and consumer panel was conducted about absolute, recognition and difference threshold respectively. And we tried to suggest appropriate and minimum acceptable menthol concentration level by consumer panel. Determination of threshold value was based on ASTM E 679-79 method by forced-choice ascending concentration series. In addition, a semi-ascending paired difference method was referred to conduct test. The group threshold value was determined as the value of geometric mean individual threshold. The smokers were dividend by two groups, trained and consumer panel. Trained panel was selected according to sensitivity to menthol discrimination. Consumer panel wasrecruited in proportion as population ratios including female smokers. They were all over twenty years old volunteers and summed up thirty four persons. In terms of sensor evaluation, overall difference test with seven-category scale by both trained and consumer panelists were done. On judging correct or incorrect answer, two by three cut-off levels applied to. Every test was conducted with two sessions, before smoking and during smoking period. And, only two samples served each paneI per test with regard to sensory fatigue and reliable results. All tests were replicated, and in total 32 times per panelist. In conclusion, the recognition threshold about consumer and expert panel was 358 ppm/cig. and 276 ppm/cig. in separately. Besides, absolute and difference thresholds were obtained also. And, we conduct difference threshold test with two different ways, upward and downward. And, The results of each method were 246, 195 ppm/cig., 1414, 1336 ppm/cig. and 1047, 972 ppm/cig.

Fault Detection of Reactive Ion Etching Using Time Series Support Vector Machine (Time Series Support Vector Machine을 이용한 Reactive Ion Etching의 오류검출 및 분석)

  • Park Young-Kook;Han Seung-Soo;Hong Sang-J.
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2006.05a
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    • pp.247-250
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    • 2006
  • Maximizing the productivity in reactive ion etching, early detection of process equipment anomaly became crucial in current high volume semiconductor manufacturing environment. To address the importance of the process fault detection for productivity, support vector machines (SVMs) is employed to assist the decision to determine process faults in real-time. SVMs for eleven steps of etching runs are established with data acquired from baseline runs, and they are further verified with the data from controlled (acceptable) and perturbed (unacceptable) runs. Then, each SVM is further utilized for the fault detection purpose utilizing control limits which is well understood in statistical process control chart. Utilizing SVMs, fault detection of reactive ion etching process is demonstrated with zero false alarm rate of the controlled runs on a run to run basis.

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Seismic retrofit of steel structures with re-centering friction devices using genetic algorithm and artificial neural network

  • Mohamed Noureldin;Masoum M. Gharagoz;Jinkoo Kim
    • Steel and Composite Structures
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    • v.47 no.2
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    • pp.167-184
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    • 2023
  • In this study, a new recentering friction device (RFD) to retrofit steel moment frame structures is introduced. The device provides both self-centering and energy dissipation capabilities for the retrofitted structure. A hybrid performance-based seismic design procedure considering multiple limit states is proposed for designing the device and the retrofitted structure. The design of the RFD is achieved by modifying the conventional performance-based seismic design (PBSD) procedure using computational intelligence techniques, namely, genetic algorithm (GA) and artificial neural network (ANN). Numerous nonlinear time-history response analyses (NLTHAs) are conducted on multi-degree of freedom (MDOF) and single-degree of freedom (SDOF) systems to train and validate the ANN to achieve high prediction accuracy. The proposed procedure and the new RFD are assessed using 2D and 3D models globally and locally. Globally, the effectiveness of the proposed device is assessed by conducting NLTHAs to check the maximum inter-story drift ratio (MIDR). Seismic fragilities of the retrofitted models are investigated by constructing fragility curves of the models for different limit states. After that, seismic life cycle cost (LCC) is estimated for the models with and without the retrofit. Locally, the stress concentration at the contact point of the RFD and the existing steel frame is checked being within acceptable limits using finite element modeling (FEM). The RFD showed its effectiveness in minimizing MIDR and eliminating residual drift for low to mid-rise steel frames models tested. GA and ANN proved to be crucial integrated parts in the modified PBSD to achieve the required seismic performance at different limit states with reasonable computational cost. ANN showed a very high prediction accuracy for transformation between MDOF and SDOF systems. Also, the proposed retrofit showed its efficiency in enhancing the seismic fragility and reducing the LCC significantly compared to the un-retrofitted models.

Bolted connections to tubular columns at ambient and elevated temperatures - A review

  • Leong, S.H.;Sulong, N.H. Ramli;Jameel, Mohammed
    • Steel and Composite Structures
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    • v.21 no.2
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    • pp.303-321
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    • 2016
  • Tubular column members have been widely adopted in current construction due to its numerous advantages. However, the closed-section profile characteristics of tubular columns severely limit the connection possibilities. Welding type is acceptable but discouraged because of on-site issues. Blind-bolted connection is preferable because of its simplicity, economic benefit, and easy assembly. This paper presents a state-of-the-art review on bolted connections to tubular columns for bare steel tubes, including square and circular sections. Available studies on bolted connections at ambient and elevated temperatures are reviewed, but emphasis is given on the latter. Various methods of determining the connection performance through experimental, analytical, component based, and finite element approaches are examined. Future research areas are also identified.