• 제목/요약/키워드: X-ray unit

검색결과 563건 처리시간 0.03초

X-ray Crystal Structure of Hetaryl Leuco-TAM Dyes, (2Z,2'E)-2,2'-(2-Phenyl Propane-1,3-diylidene) Bis(1,3,3-trimethyl indoline) Derivatives

  • Keum, Sam-Rok;Roh, Se-Jung;Kim, Young-Nan;Im, Do-Hyuck;Ma, So-Young
    • Bulletin of the Korean Chemical Society
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    • 제30권11호
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    • pp.2608-2612
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    • 2009
  • The unequivocal solid-state structure and stereochemistry of the hetaryl leuco-TAM dye, 2,2’-(2-phenyl propane- 1,3-diylidene) bis(1,3,3- trimethylindoline) derivatives were established using X-ray single crystal analysis. The X-ray crystal analysis showed that the (Z, E)-isomers only formed stereoselectively, with a so-called “threebladed propeller” conformation, from the reaction of a Fischer base and benzaldehyde derivatives. These isomers were stacked in a juxtaposition to form a dimer or a double dimer, adopting either a triclinic, with P-1, or monoclinic crystal system with a space group P21/n in the unit cell of the crystal.

Structure Study of Polycrystalline $Na_3YSi_3O_9$ and Its Substitutes Related to $Na_4CaSi_3O_9,\;Ca_3Al_2O_6$ Structure

  • Kim, Chy-Hyung;Banks, Ephraim
    • Bulletin of the Korean Chemical Society
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    • 제8권1호
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    • pp.6-9
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    • 1987
  • The study of the $Na_3YSi_3O_9$ structure, by x-ray diffraction and infrared spectrum, showed that $Na_3YSi_3O_9$ is similar to $Na_4CaSi_3O_9$ except for its being pseudo-cubic instead of cubic. The peaks in the x-ray diffraction pattern of $Na_3YSi_3O_9$ could therefore be indexed on the basis of the $Na_4CaSi_3O_9$ cell. Also, modified $Na_3MSi_3O_9$ (M = Lu, Yb, Tm, Er, Y, Ho, Dy, Gd, Eu, and Sm) type compounds were synthesized by introducing excess sodium, decreasing M(III) concentration, and substituting small amount of phosphorus for silicon. The unit cell parameters of the composition $Na_{3.2}M_{0.7}Si_{2.9}P_{0.1}O_{8.7}$ were estimated from x-ray powder diffraction patterns using the Cohen method.

Purification, crystallization and X-ray crystallographic analysis of nicotinamidase Pnc1 from Kluyveromyces lactis

  • Kim, Shinae;Chang, Jeong Ho
    • Biodesign
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    • 제7권1호
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    • pp.24-27
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    • 2019
  • Pnc1 converts nicotinamide to nicotinic acid to generate NAD+ through the Preiss-Handler pathway that is one of the NAD+-salvage pathway. By reducing levels of nicotinamide, an inhibitor of the NAD+-dependent histone deacetylase Sir2, yeast Pnc1 contributes gene silencing. In this study, to understand the structural features and molecular mechanism of nicotinamidase Pnc1, we overexpressed, purified, and crystallized the N-terminally His6-tagged Pnc1 protein from Kluyveromyces lactis and obtained X-ray diffraction data at a resolution of 2.2 Å. The crystals of the K. lactis Pnc1 (KlPnc1) belonged to space group P212121 with unit cell parameters a=38.5, b=77.3, c=83.3, and α=β=γ= 90°. There is one molecule in the asymmetric unit.

3D 동영상획득을 위한 Cone-Beam 형 X-Ray CT 시스템 구현에 관한 연구 (The Study on the Implementation of the X-Ray CT System Using the Cone-Beam for the 3D Dynamic Image Acquisition)

  • 정찬웅;전계석
    • 한국음향학회지
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    • 제28권4호
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    • pp.370-374
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    • 2009
  • 본 논문에서는 3차원 동영상을 구현하기 위하여 인체에 유해한 방사능 피폭량이 부챗살 형태의 Fan Beam 보다 상대적으로 적은 원추형 Cone Beam CT 시스템을 설계하였다. 설계된 시스템은 X-ray가 조사된 각도에서 획득한 데이터를 영상처리부로 전송하고 영상을 구성하는 계산 속도를 빠르게 하기 위하여 초월함수가 보다 적은 3단계 회전 행렬을 이용하여 3차원 영상을 구현하는 회전 기반법을 사용하였다. 본 연구에서는 3차원 영상을 구성하는 시간단축을 통해 초당 3~5장의 영상을 얻음으로써 3차원 동영상을 실시간으로 구현하였다.

X-RAY ASTRONOMY EXPERIMENT ON THE INDIAN SATELLITE IRS-P3

  • AGRAWAL P. C.;PAUL B.;RAO A. R.;SHAH M. R.;MCKERJEE K.;VARIA M. N.;YADAV J. S.;DEDHIA D. K.;MALKAR J. P.;SHAH P.;DAMLE S. V.;MARAR T. M. K.;SEETHA S.
    • 천문학회지
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    • 제29권spc1호
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    • pp.429-432
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    • 1996
  • An x-ray astronomy experiment consisting of three collimated proportional counters and an X-ray Sky Monitor (XSM) was flown aboard the Indian Satellite IRS-P3 launched on March 21, 1996 from SHAR range in India. The Satellite is in a circular orbit of 830 km altitude with an orbital inclination of $98^{\circ}$ and has three axis stabilized pointing capability. Each pointed-mode Proportional Counter (PPC) is a multilayer, multianode unit filled with P-10 gas ($90\%$ Ar + $10\%\;CH_4$) at 800 torr and having an aluminized mylar window of 25 micron thickness. The three PPCs are identical and have a field of view of $2^{\circ}{\times}2^{\circ}$ defined by silver coated aluminium honeycomb collimators. The total effective area of the three PPCs is about 1200 $cm^2$. The PPCs are sensitive in 2-20 keV band. The XSM consists of a pin-hole of 1 $cm^2$ area placed 16 cm above the anode plane of a 32 cm$\times$32 cm position sensitive proportional counter sensitive in 3-8 keV interval. The position of the x-ray events is determined by charge division technique using nichrome wires as anodes. The principal objective of this experiment is to carry out timing studies of x-ray pulsars, x-ray binaries and other rapidly varying x-ray sources. The XSM will be used to detect transient x-ray sources and monitor intensity of bright x-ray binaries. Observations of black-hole binary Cyg X-1 and few other binary sources were carried out in early May and July-August 1996 period. Details of the x-ray detector characteristics are presented and preliminary results from the observations are discussed.

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Building a Graphite Calorimetry System for the Dosimetry of Therapeutic X-ray Beams

  • Kim, In Jung;Kim, Byoung Chul;Kim, Joong Hyun;Chung, Jae-Pil;Kim, Hyun Moon;Yi, Chul-Young
    • Nuclear Engineering and Technology
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    • 제49권4호
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    • pp.810-816
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    • 2017
  • A graphite calorimetry system was built and tested under irradiation. The noise level of the temperature measurement system was approximately 0.08 mK (peak to peak). The temperature of the core part rose by approximately 8.6 mK at 800 MU (monitor unit) for 6-MV X-ray beams, and it increased as X-ray energy increased. The temperature rise showed less spread when it was normalized to the accumulated charge, as measured by an external monitoring chamber. The radiation energy absorbed by the core part was determined to have values of $0.798J/{\mu}C$, $0.389J/{\mu}C$, and $0.352J/{\mu}C$ at 6 MV, 10 MV, and 18 MV, respectively. These values were so consistent among repeated runs that their coefficient of variance was less than 0.15%.

Micro X-ray CT 촬영을 통한 동결 사질토 시료의 세립분 함유량에 따른 입자간 거리 분석 (Particle Spacing Analysis of Frozen Sand Specimens with Various Fine Contents by Micro X-ray Computed Tomography Scanning)

  • 채덕호;이장근;김광염;조완제
    • 한국지반환경공학회 논문집
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    • 제18권1호
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    • pp.31-35
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    • 2017
  • Chae et al.(2015)에 따르면 동결 사질토의 역학적 거동은 동결온도와 세립분 함유량에 따라 크게 영향을 받는 것으로 나타났다. 이러한 원인으로 동결온도에 따른 부동수분의 차이일 것이라는 의견과 세립분 함유량 및 간극 내 얼음에 의해 사질토 입자들 이격거리 차이에 의한 것이라는 의견이 제시되었다. 제시된 두 가지 의견 중 사질토 입자들 이격거리의 확인을 위해 micro X-ray CT 촬영을 수행하였다. X-ray CT 촬영에 의한 비파괴 검사는 최근 지반공학 분야에서 진행되고 있는 다양한 융복합 연구 중 하나로 CT 촬영을 통하여 지반재료의 내부 구조를 마이크로미터 단위의 높은 해상도를 통해 평가할 수 있는 방법이다. 본 연구에서는 -5, -10, $-15^{\circ}C$의 동결온도에서 성형된 5, 10, 15%의 세립분을 포함하고 있는 동결 사질토 공시체에 대하여 micro X-ray CT 촬영을 수행하고 기존의 개발된 이미지 해석 기법을 적용하여 동결 사질토 내의 조립질 입자들의 최단거리 및 평균거리를 통하여 세립분 함유량 및 동결온도가 조립질 입자간의 거리에 미치는 영향을 파악하고자 하였다. X-ray CT 촬영 결과, 동결온도 및 세립분 함유량은 동결 사질토 내 입자간 거리에는 큰 영향을 미치지 않는 것으로 나타났다.

염료감응형태양열 물질이 요오드화수은의 전기적 특성에 미치는 영향에 관한 연구 (Study on the effect of DSSC(Dye Sensitizer Solar Cell) Material on the electrical properties of Mercuric Iodide)

  • 조규석;박지군;허승욱;송용근;한무재;김금배;최상현
    • 한국방사선학회논문지
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    • 제11권6호
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    • pp.525-529
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    • 2017
  • 요오드화수은은 우수한 엑스선 민감도 특성을 가진 광도전체로 비정질 셀레늄을 대체할 수 있는 후보물질로 많은 연구가 진행되고 있지만 높은 누설전류로 인해 상용화에 많은 한계점을 나타내고 있다. 본 연구에서는 요오드화수은의 높은 누설전류를 저감하기 위해 요오드화수은에 비해 입자가 작은 이산화규소 및 이산화티타늄을 물리적으로 혼합하여 단위시편을 제작하였으며 제작된 단위시편의 전기적 특성을 비교 분석하였다. 그 결과 혼합한 두 물질 모두 요오드화수은의 높은 누설전류를 저감하는데 효과가 있었으며 요오드화수은-이산화티타늄 혼합물에서는 방사선 민감도 특성이 상당히 높아짐을 확인하였다.

Exposure Index를 이용한 이동형 디지털 X선 장치의 흉부촬영 적정노출조건에 관한 연구 (A Study on the Proper Chest Exposure Conditions of Mobile Digital X-ray Unit by Exposure Index)

  • 김재인;이양섭;장동수;정민철;배승호;이관섭;하동윤
    • 대한디지털의료영상학회논문지
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    • 제13권3호
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    • pp.139-144
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    • 2011
  • The purpose of this report is recommending a standard indicator which reflects the radiation exposure that is incident on a detector after every exposure event and that reflects the noise levels present in the image data. The experiment was performed with mobile digital X-ray unit and used a acrylic phantom for exposure index measurement. Exposure modality was kVp, mAs, SID. After every exposure, make a data sheet for characteristic curve of detector response. The equipment performed Mobile digital X-ray unit provide the user with values ralated to the incident exposure(air kerma)to the digital detector. They are showed as a logarithmic function shaped. As a result, DEI means a relative measure of exposure to the detector, as compared to the expected exposure for a particular anatomical view. Radiographic technique is the combination of factors used to exposure an anatomical part to produce a high quality radiography and technique charts used most commonly by radiographers to produce consistently exposure level which patient dose can be kept acceptably low.

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