• Title/Summary/Keyword: X-ray measurement

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Microstructure and Strengthening Mechanism Characteristics of Titanium Fabricated by SPS Method after Mechanical Milling Treatment (기계적 밀링 처리하여 SPS법으로 제작한 티타늄의 미세조직과 강화기구 특성)

  • Chang-Suk Han;June-Sung Kim;Woo-Bin Sim
    • Korean Journal of Materials Research
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    • v.33 no.6
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    • pp.242-250
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    • 2023
  • Titanium, which has excellent strength and toughness characteristics, is increasingly used in the aerospace field. Among the titanium alloys used for body parts, more than 80 % are Ti-6Al-4V alloys with a tensile strength of 931 MPa. The spark plasma sintering (SPS) method is used for solidification molding of powder manufactured by the mechanical milling (MM) method, by sintering at low temperature for a short time. This sintering method avoids coarsening of the fine crystal grains or dispersed particles of the MM powder. To improve the mechanical properties of pure titanium without adding alloying elements, stearic acid was added to pure titanium powder as a process control agent (PCA), and MM treatment was performed. The properties of the MM powder and SPS material produced by solidifying the powder were investigated by hardness measurement, X-ray diffraction, density measurement and structure observation. The processing deformation of the pure titanium powder depends on the amount of stearic acid added and the MM treatment time. TiN was also generated in powder treated by MM 8 h with 0.50 g of added stearic acid, and the hardness of the powder was higher than that of Ti-6Al-4V alloy when treated with MM for 8 h. When the MM-treated powder was solidified in the SPS equipment, TiC was formed by the solid phase reaction. The SPS material prepared as a powder treated with MM 8 h by adding 0.50 g of stearic acid also formed TiN and exhibited the highest hardness of Hv1253.

Measurement of Skin Dose for Rectal Cancer Patients in Radiotherapy using Optically Stimulated Luminescence Detectors (OSLDs) (광자극발광선량계(OLSDs)를 이용한 직장암 방사선치료 환자의 피부선량 측정)

  • Im, In-Chul;Yu, Yun-Sik;Lee, Jae-Seung
    • Journal of Radiation Protection and Research
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    • v.36 no.2
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    • pp.86-92
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    • 2011
  • This study used the optically stimulated luminescence dosimeters (OSLDs), recently, received the revaluation of usefulness in vivo dosimetry, and the diode detecters to measure the skin dose of patient with the rectal cancer. The measurements of dose delivered were compared with the planned dose from the treatment planning system (TPS). We evaluated the clinical application of OSDs in radiotherapy. We measured the calibration factor of OSLDs and used the percent depth dose to verified, also, we created the three point of surface by ten patients of rectal cancer to measured. The calibration factors of OSLD was 1.17 for 6 MV X-ray and 1.28 for 10 MV X-ray, demonstrating the energy dependency of X-ray beams. Comparison of surface dose measurement using the OSLDs and diode detectors with the planned dose from the TPS, The skin dose of patient was increased 1.16 ~ 2.83% for diode detectors, 1.36 ~ 2.17% for OSLDs. Especially, the difference between planned dose and the delivery dose was increased in the perineum, a skin of intense flexure region, and the OSLDs as a result of close spacing of measuring a variate showed a steady dose verification than the diode detecters. Therefore, on behalf of the ionization chamber and diode detecters, OSLDs could be applied clinically in the verification of radiation dose error and in vivo dosimety. The research on the dose verification of the rectal cancer in the around perineal, a surface of intense flexure region, suggest continue to be.

The Crystallographic and Magnetic Properties of $Fe_{1-x}Co_x$System ($Fe_{1-x}Co_x$계의 결정구조와 자기적인 성질)

  • 김정기;한경훈;서정철
    • Journal of the Korean Magnetics Society
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    • v.9 no.4
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    • pp.190-195
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    • 1999
  • The crystallographic and magnetic properties of the system of $Fe_{1-x}Co_x$(x=0.2 and 0.4) prepared by microwave arc-melting with the maximum power of 3.5 kW and a iron-foil with thickness of 25 ${\mu}{\textrm}{m}$ have been studied by the methods of X-ray diffraction and the measurement of the magnetic hysteresis using the vibrating sample magnetometer at room temperature. The samples were prepared in three different ways: First, pellet form pressed under the pressure of 9,000 N/$\textrm{cm}^2$. Second, the sheet cold rolled. Third, thin sheet treated with the temperature of 90$0^{\circ}C$. The X-ray diffraction pattern of the sample prepared by the first method shows that the crystal structure of the sample is bcc as same as that of Fe with a good uniformity. The iron-foil has the coercivity of 43 Oe and the initial slope of magnetization of 0.328 emu/gOe. The coervicity and magnetization of the sample prepared by the second method increased as the Co content increased. But the initial slop of the magnetization decreased as the Co content increased. This means that the displacement of domain wall is suppressed by the increases of coercivity as the Co content increased. The saturation magnetization of the samples made by the third method increased. On the other hand, the coercivity of these samples decreased. The increase of saturation magnetization of the samples seems to be related to the changes in X-ray intensity after heat treatment. Also some magnetic parameters of the samples were calculated by using a simple model and compared with other values.

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Superconducting property in the Zn substituted MgC$Ni_3$ (Zn로 치환된 MgCN $i_3$의 초전도 특성)

  • 이용우;김진수;박민석;이성익;심지훈;민병일;최은집
    • Progress in Superconductivity
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    • v.4 no.2
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    • pp.144-147
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    • 2003
  • We investigated superconducting property of ($Mg_{1-x}$$Zn_{x}$)$CNi_3$ (x=0,0.03, 0.06, 0.09, 0.12, 0.15, and 0.18) sample where Mg is substituted with Zn. The samples were synthesized us ins the solid state reaction method under As atmosphere. X -ray diffraction spectra show that the $MgCNi_3$ structure is maintained up to x=18. With increasing x, the lattice constant (or the Ni-Ni distance) decreases. Magnetic susceptibility measurement shows that $T_{c}$ decreases systematically with x and becomes ~2K at x =0.18. Surprisingly, the transition width remains sharp (~0.3K). Under some assumptions, we estimate the coupling constant in the McMillan formula as a function of x which we interpret in terms of the BCS theory.y.y.y.

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The signal property and structure design of CsI:Na/a-Se for diagnostic x-ray imaging (진단 X선 영상을 위한 CsI:Na/a-Se 구조설계 및 신호특성)

  • Park, Ji-Koon;Heo, Ye-Ji;Park, Jeong-Eun;Park, Sang-Jin;Kim, Hyun-Hee;No, Ci-Chul;Kang, Sang-Sik
    • Journal of the Korean Society of Radiology
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    • v.3 no.4
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    • pp.35-38
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    • 2009
  • Flat-panel x-ray detectors using a phosphor and photoconductor material have been used for application in various medical modalities. In this study, the monte carlo simulation, optical and x-ray response characteristics were investigated in the conversion structure obtained by a columnar CsI:Na scintillation layer with a photosensitive amorphous selenium layer. Firstly, from the measurement of luminescent spectrum of CsI:Na and absorption spectrum of a-Se layer, the signal conversion characteristics are analysed. And also, the x-ray sensitivity is measured and compared with conventional a-Se($500{\mu}m$) as a function of electrical field. From the experimental result, the x-ray sensitivities of the CsI:Na($180{\mu}m$)/a-Se($30{\mu}m$) detector and the a-Se($500{\mu}m$) detector were $7.31nC/mR-cm^{2}$ and $3.95nC/mR-cm^{2}$at an electric field of $10V/{\mu}m$, respectively.

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Application of the Equivalent-Field Method for Output Calculation: Is it safe for elongated x-ray fields\ulcorner (출력인자 계산에 이용되는 등가면법의 타당성 연구 : 장방형 X-선 조사면에 대해서 안전한가\ulcorner)

  • Kim, Chang-Seon;Kim, Chul-Yong;Park, Myung-Sun
    • Progress in Medical Physics
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    • v.9 no.4
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    • pp.195-200
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    • 1998
  • Purpose: When an elongated x-ray field is used for treating a patient, the equivalent- field method is commonly used for the output calculation. This study is intended for investigating potential factors such as, beam quality, field elongation ratio, and depth of measurement, which might effect on the applicability of the equivalent square technique for output calculation. The derivation of a 'rule of thumb' for the application criteria of the equivalent-field method is also aimed. Materials and Methods: Three x-ray beams, 4-, 6- and 10-MV, were employed for this study. Width of the rectangular field was ranged from 5-40 cm and the elongation ratio (length/width) 1:0 to 10:0. An elongation effect was measured in a water phantom at three different depths, dmax, 5-cm, and 10-cm. For an elongated field and its equivalent square field, the output factor was measured and the difference in the output factor were examined between two fields. Results and Discussions: As the elongation ratio increases, a larger discrepancy in outputs is observed between the elongated rectangular field and its corresponding equivalent square field. Output was measured larger for an elongated field than for its corresponding equivalent square field and the maximal difference over 10 % was found. The difference was found larger for the smaller field with the same elongation ratio. The effect of the beam quality and the depth of measurement on the output difference was minimal. Conclusion: Based on the study, there is criteria for the application of the method for output calculation. For the combination of long axis and elongation ratio whose relationship satisfies Elongation ratio < (0.48) (Long axis) - 0.5, the equivalent-field method is valid for output calculation within 2 % for the field whose long axis < 25-cm. For other combinations, instead of using the equivalent-field method, direct output measurement is recommended. This criteria can be applied for 4-10 MV x-ray beams up to 10-cm depth.

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A Study on the Characteristics of Therapy Radiation Detector with Diode (다이오드를 이용한 치료방사선 검출기의 특성에 관한 연구)

  • 이동훈;지영훈
    • Journal of Biomedical Engineering Research
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    • v.16 no.2
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    • pp.129-138
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    • 1995
  • High-energy and high-dose X-ray and electron beam have been used in radiation therapy after developing particle accelerators. It is recommended to irradiate patients exect real dose for improving therapy effectiveness by International Committee on Radiation Units and Measurement. The radiation detector for daily beam checks of medical accelerators is described. Using thirteen silicon diodes, we have designed the diode detector providing information about calibration, beam symmetry, flatness, stability variation according to radiation damage, time and general quality assurance for both photon and eletron beams. we also compared these measurement values with those of using ionization chamber, film and semiconductor dosimeter.

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Growth and Optical Properties for $AgGaSe_2$ Single Crystal Thin Films by Hot Wall Epitaxy (Hot Wall Epitaxy (HWE)법에 의한$AgGaSe_2$ 단결정 박막 성장과 광학적 특성)

  • Hong, Kwang-Joon;Back, Seoung-Nam
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.124-127
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    • 2003
  • The stochiometric $AgGaSe_2$ polycrystalline mixture of evaporating materials for the $AgGaSe_2$ single crystal thin film was prepared from horizontal furnance. To obtain the single crystal thin films, $AgGaSe_2$ mixed crystal and semi-insulating GaAs(100) wafer were used as source material and substrate for the Hot Wall Epitaxy (HWE) system, respectively. The source and substrate temperature were fixed at $630^{\circ}C$ and $420^{\circ}C$, respectively. The thickness of grown single crystal thin films is $2.1{\mu}m$. The single crystal thin films were investigated by photoluminescence and double crystal X-ray diffraction(DCXD) measurement. From the photoluminescence measurement of $AgGaSe_2$ single crystal thin film, we observed free excition ($E_x$) observable only in high quality crystal and neutral bound excition ($D^{\circ}$,X) having very strong peak intensity. And, the full width at half maximum and binding energy of neutral donor bound excition were 8 meV and 14.1 meV, respectively. By Haynes rule, an activation energy of impurity was 141 meV.

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Piezoelectric Properties and Phase Transition behaviors of (Bi1/2Na1/2)1- xCaxTiO3Ceramics ((Bi1⁄2Na1⁄2)1-xCaxTiO3 세라믹스의 압전 특성 및 상전이 거동)

  • Lee, Yong-Hyun;Cho, Jeong-Ho;Kim, Byung-Ik;Choi, Duck-Kyun
    • Journal of the Korean Ceramic Society
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    • v.45 no.5
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    • pp.263-267
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    • 2008
  • $(Bi_{1/2}Na_{1/2})TiO_3$-based ceramics have been intensively studied as lead-free piezoelectric ceramics. In this study, the piezoelectric properties and phase transition behaviors of BNT based solid solution $(Bi_{0.5}Na_{0.5})_{1-x}Ca_xTiO_3$ ($X=0.01{\sim}0.25$) were investigated. The morphotropic phase boundary(MPB) zone which BNT is transformed from rhombohedral to cubic structure was appeared by adding $CaTiO_3$ with 0.12 mol by the measurement of permittivity and X-ray diffraction. The behavior which ferroelectric BNT with adding $CaTiO_3$ was changed to antiferroelectric and paraelectric state was confirmed by the measurement ofhysterisis loop and depolarization temperature as a function of temperature. As $CaTiO_3$ concentration was increased, the phase transition temperature was decreased. The piezoelectric properties were highest at 0.01 mol of $CaTiO_3$ concentration. The electromechanical coupling factor($K_t$) and mechanical quality factor($Q_m$) were 42% and 254, respectively.

Measurement of Depth Dose Distribution Using Plastic Scintillator

  • Hashimoto, Masatoshi;Kodama, Kiyoyuki;Hanada, Takashi;Ide, Tatsuya;Tsukahara, Tomoko;Maruyama, Koichi
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.244-247
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    • 2002
  • We examined a possibility to use inorganic plastic scintillator, which has the effective atomic number close to that of human soft tissue, for the measurement of dose distributions in a shorter time period. The method was to irradiate a block of plastic scintillator as a phantom, and to measure the distribution of the scintillation light by a wave length analyzer through a thread of plastic optical fiber. By irradiating the diagnostic x-ray, we observed the emission spectrum of the scintillation light from the scintillator. It showed a peak at around 420nm with a full width of 140 nm. The emission spectrum was integrated to determine the total number of photons. The dependences of the amount of photons on the irradiated dose were measured. The results of the experiment show that the amount of emission light is in proportional to the irradiated dose. From this fact, we conclude that the present method can be used for the measurement of the depth dose distribution of the diagnostic x-rays.

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