• Title/Summary/Keyword: X-선 에너지 스펙트럼

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A Study on Quantitative Thickness Evaluation Using Film Density Variation in Film Radiography (Film Radiography에서 농도차를 이용한 정량적 두께 평가에 관한 연구)

  • Lee, Sung-Sik;Lee, Jeong-Ki;Kim, Young-H.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.19 no.5
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    • pp.356-362
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    • 1999
  • Based on the assumption that film density increases exponentially with exposure in the industrial radiographic film. an equation representing the characteristic curves of industrial radiographic films and a new density-thickness relation are suggested. The accuracy and reliability of the suggested relation has been tested using radiographs of a carbon steel step wedge with known thickness variation by polychromatic X-ray and ${\gamma}$-ray ($Ir^{192}$). The experimental results were well agreed to the proposed relation in the range of film densities from 1.0 to 3.5 and it was more accurate than the conventional relation. It is also found that ${\gamma}$-ray is more effective in this purpose than polychromatic X-ray, which results in variation of effective linear absorption coefficient due to beam hardening effect as thickness increases. Therefore using the equation and experimentally determined parameters the quantitative evaluation of thickness variation is possible and it can be used to evaluate the depth of local corrosion of pressure vessels in plants.

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Dyeing of Cotton Knitted Fabrics with Volcanic Ash(I) -The Compositions of Volcanic ash Deposited on the Cotton Knitted Fabrics- (화산재를 이용한 면 편성물의 염색(I) - 면 편성물에 부착된 화산재의 성분분석을 중심으로 -)

  • 유복선;신인수
    • Journal of the Korean Home Economics Association
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    • v.41 no.8
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    • pp.55-62
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    • 2003
  • Natural dyes generally fan into two categories; organic dyes coming from animals and plants and inorganic dyes obtained from various minerals such as bengala, loess, ultramarine, prussian blue and etc. The main components of volcanic ash is clay mineral such as kaolinite, illite, quartz. Clay minerals Composing volcanic ash are kaolinite[$Al_4Si_4O_{10}{(OH)_{8}}$], illite[$K_{X}Al_2(Si,\;Al)_4O_{10}{(OH)}_2$], quartz[$SiO_2$], homblende[$Na_{0-1}\;Ca_2{(Mg,\;Fe,\;Al)}_5{(Si,\;Al)}_{8}O_{22}{(OH)}_2$]and etc. And the redish color mainly comes from iron oxide. In this paper, two different classes of dyeing process were tested; dyeing with volcanic ash only and cationic agent pre-treatment followed by dyeing with volcanic ash. The compositions of the volcanic ash powder and the volcanic ash deposited on the cotton knitted fabrics identified by energy dispersive spectrometer and XRD analysis. The major chemical components of volcanic ash deposited on the cotton knitted fabrics were confirmed to be the saicon oxide, iron oxide, and aluminum oxide and etc. According to the analysis by XRD and EDS-SEM, kaolinite, illite and quartz were also identified.

Growth and Photocurrent Properties of CuGaTe2 Single Crystal Thin Films by Hot Wall Epitaxy (Hot Wall Epitaxy (HWE) 방법에 의한 CuGaTe2 단결정 박막 성장과 광전류 특성)

  • 백승남;홍광준
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.158-158
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    • 2003
  • 수평 전기로에서 CuGaTe2 다결정을 합성하여 HWE 방법으로 CuGaTe2 단결정 박막을 반절연성 GaAs(100) 위에 성장하였다. CuGaTe2 단결정 박막은 증발원과 기판의 온도를 각각 67$0^{\circ}C$, 41$0^{\circ}C$로 성장하였다. 이때 단결정 박막의 결정성이 10K에서 측정한 광발광 스펙트럼은 954.5nm (1.2989eV) 근처에서 exciton emission 스펙트럼이 가장 강하게 나타났으며, 또한 이중결정 X-선 요동곡선(DCRC)의 반폭치(FWHM)도 139arcsec로 가장 작게 측정되어 최적 성장 조건임을 알 수 있었다. Hall 효과는 van der Paw방법에 의해 측정되었으며, 온도에 의존하는 운반자 농도와 이동도는 293K에서 각각 8.72$\times$$10^{23}$개/㎥, 3.42$\times$$10^{-2}$$m^2$/V.s였다. 상온에서 CuGaTe2 단결정 박막의 광흡수 특성으로부터 에너지 띠간격이 1.22 eV였다 Band edge에 해당하는 광전도도peak의 온도 의존성은 Varshni 관계식으로 설명되었으며, Varshni 관계식의 상수값은 Eg(0) = 1.3982 eV, $\alpha$= 4.27$\times$$10^{-4}$ eV/K, $\beta$= 265.5 K로 주어졌다. CuGaTe2 단결정 박막의 광전류 단파장대 봉우리들로부터 10K에서 측정된 $\Delta$cr (crystal Field splitting)은 0.0791eV, $\Delta$s.o (spin orbit coupling)는 0.2463eV였다. 10K에서 광발광 봉우리의 919.8nm (1.3479eV)는 free exciton(Ex), 954.5nm (1.2989eV)는 donor-bound exciton 인 I2(DO,X)와 959.5nm (1.2921eV)는 acceptor-bound exciton 인 I1(AO,X) 이고, 964.6nm(1.2853eV)는 donor-acceptor pair(DAP) 발광, 1341.9nm (0.9239eV)는 self activated(SA)에 기인하는 광발광 봉우리로 고찰되었다.

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Analysis of Photon Characteristics and Absorbed Dose with Cone Beam Computed Tomography (CBCT) using Monte Carlo Method (몬테칼로 기법을 이용한 CBCT의 광자선 특성 및 선량 분석)

  • Kim, Jong-Bo;Kim, Jung-Hoon;Park, Eun-Tae
    • Journal of the Korean Society of Radiology
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    • v.11 no.3
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    • pp.161-169
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    • 2017
  • The cone beam computed tomography(CBCT) which can acquire 3-dimensions images is widely used for confirmation of patient position before radiation therapy. In this study, through the simulation using the Monte Carlo technique, we will analyze the exposure dose by cone beam computed tomography and present the standardized data. For the experiment, MCNPX(ver. 2.5.0) was used and the photon beam spectrum was analyzed after Cone beam was simulated. As a result of analyzing the photon beam spectrum, the average energy ranged from 25.7 to 37.6 keV at the tube voltage of 80 ~ 120 kVp and the characteristic X-ray energy was 9, 60, 68 and 70 keV. As a result of using the water phantom, the percentage depth dose was measured, and the maximum dose appeared on the surface and decreased with depth. The absorbed dose also decreased as the depth increased. The absorbed dose of the whole phantom was 9.7 ~ 18.7 mGy. This is a dose which accounts for 0.2% of about 10 Gy, which is generally used for radiation therapy per week, which is not expected to have a significant effect on the treatment effect. However, it should not be overlooked even if it is small compared with prescription dose.

The Study on the Intercalation-Deintercalation of Potassium-Carbon Fiber Intercalation Compounds (칼륨-탄소섬유층간화합물의 Intercalation-Deintercalation에 관한 연구)

  • Oh, Won-Chun;Cho, Sung-Jun;Choi, Young-Jai;Ko, Young-Shin
    • Analytical Science and Technology
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    • v.7 no.2
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    • pp.193-199
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    • 1994
  • We have synthesized K-CFICs by the modified two-bulb method. These synthesized compound were analysed with X-ray diffractometer and UV/VIS spectrophotometer. According to X-ray diffraction analysis, the intercalation of potassium between the carbon layers of carbon fiber was better then other intercalants. From obtained data for this deintercalation process, we can see that a number of potassiums were presented as a residue between the carbon layers and this residue compounds had a stability for a long term. Therefore, it is appear that these compounds have a capability as new useful material. From UV/VIS spectrometry data, we can suppose that spectrum of K-CFICs synthesized at $250^{\circ}C$ had only a $R_{min}$, and spectra of any other compounds were not appeared charecteristic peaks because potassium ions were little affect the energy levels of original carbon fiber.

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Fabrication of Virtual Frisch-Grid CdZnTe ${\gamma}$-Ray Detector (가상 Frisch-그리드를 이용한 CdZnTe 감마선 소자 제작)

  • Park, Chansun;Kim, Pilsu;Cho, PyongKon;Choi, Jonghak;Kim, Jungmin;Kim, KiHyun
    • Journal of radiological science and technology
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    • v.37 no.4
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    • pp.253-259
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    • 2014
  • Large volume of $6{\times}6{\times}12mm^3$ CdZnTe ${\gamma}$-ray detector was fabricated with CdZnTe single crystals grown by Traveling Heater Method (THM) to evaluate the energy resolution of 662 keV in $^{137}Cs$. Hole tailing effect which originated from the large mobility difference in electron and hole degrade energy resolution of radiation detector and its effects become more severe for a large volume detectors. Generally, single carrier collection technique is very useful method to remove/minimize hole tailing effect and thereby improvement in energy resolution. Virtual Frisch-grid technique is also one of single charge collection method through weighting potential engineering and it is very simple and easily applicable one. In this paper, we characterized CZT detector grown by THM and evaluated the effectiveness of virtual Frisch-grid technique for a high energy gamma-ray detector. The proper position and width of virtual Frisch-grid was determined from electric field simulation using ANSYS Maxwell ver. 14.0. Energy resolution of 2.2% was achieved for the 662 keV ${\gamma}$-peak of $^{137}Cs$ with virtual Frisch-grid CdZnTe detector.

Study of Nonstoichiometry and Physical Properties of the Mixed Valency $Sr_xEu_{1-x}FeO_{3-y}$ ($0.00{\leq}x{\leq}$1.00) System (혼합원자가 $Sr_xEu_{1-x}FeO_{3-y}$ ($0.00{\leq}x{\leq}$1.00)계의 비화학량론과 물성 연구)

  • Ji Young Min;Kwon Sun Roh;Chul Hyun Yo
    • Journal of the Korean Chemical Society
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    • v.38 no.12
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    • pp.873-879
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    • 1994
  • A series of samples of solid solutions in the $Sr_xEu_{1-x}FeO_{3-y}(0.00{\leq}x{\leq}1.00)$ system has been prepared at $1200^{\circ}C$ under an atmospheric air pressure. The structures of solid solutions are studied by X-ray diffraction, thermal, Mohr salt, and Mossbauer spectroscopic analyses. Their physical properties are also discussed with the electrical conductivities. X-ray diffraction data for the compositions of x = 0.00, 0.25, and 1.00 are assigned to the orthorhombic and the compositions of x = 0.50 and 0.75 to the cubic systems. The lattice volume reduced to cubic cell increases with the x value. The mole ratio of $Fe^{4+}$ iometric chemical formulas of the system are formulated from the x, $\tau$, and y values. The mixed valency state of Fe ions, the oxygen coordination, and covalent bond character are discussed with the Mossbauer spectroscopic data. The activation enegy of the electrical conductivities depends on the $\tau$ value in the temperature range of -$100^{\circ}C$ to $600\circC$ under the air pressure. The Mossbauer spectrum and electrical conductivity of the solid solutions are discussed with nonstoichiometric chemical compositions.

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A Study on the Reduction of Absorbed Dose through the Insertion of a Shielding Material in the Intraoralsensor of Dental Radiography (치과 방사선촬영 시 구내 센서 내 차폐체 삽입을 통한 피폭선량 감소 연구)

  • Kim, A Yeon;Lee, Seung-Jae
    • Journal of the Korean Society of Radiology
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    • v.16 no.3
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    • pp.273-279
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    • 2022
  • In order to reduce the absorbed dose given to the patient during dental radiography, a sensor that inserts a shield into the intraoralsensor was designed. Using the designed sensor, the change in absorbed dose depending on whether or not a shield was used was evaluated. The system used to evaluate the absorbed dose is VEX-S300C from Vatech, and the energy spectrum of X-rays was obtained through SPEKTR simulation based on the irradiation conditions of 65 kV, 3 mA, and 0.15 sec, and the number of photons for each energy was derived. After designing the system through Genat4 Application for Tomographic Emission(GATE) simulation, the energy spectrum obtained was used as a radiation source to calculate the absorbed dose. Lead was used for the shield, and simulations were performed at 0.1 mm thickness intervals from 0.1 mm to 0.5 mm was evaluated. In the case of using an X-ray field with a diameter of 60 mm, the decrease in absorbed dose according to the presence or absence of a shield decreased exponentially as the thickness of the shield increased. In addition, when a 20 mm × 30 mm field was used, the absorbed dose was significantly reduced even when no shield was used, and it was confirmed that the absorbed dose was further reduced when a shield was used.

$[Pt/Co]_4$ 다층박막과 이온선 혼합된 Pt-Co 합금박막의 자기적 특성에 대한 비교 연구

  • 강성준;이연승;이재용;황정남
    • Proceedings of the Korean Vacuum Society Conference
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    • 2000.02a
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    • pp.161-161
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    • 2000
  • Ferromagnetic 3d 전이금속과 paramagnetic 5d 금속으로 이루어지진 Pt-Co 계는 자기이방적 (magnetic anisotropy) 성질로 인하여 많은 관심을 모으고 있는 계로서는 다층박막 및 합금박막에 대한 지기적 성질에 대한 많은 연구가 있어 왔다. 최근 sputtering method 에 의해 제작된 Pt-Co 합금박막에 대해 Ar 기체분압에 따라 보자력 (coercivity)이 변화되고 PMA (perpendicular magnetic anisotropy)를 갖는 것을 관측하였다. PMA의 근원은 주로 계면에서의 anisotropy 에너지와 관련이 있는 것으로 이해되기 때문에 합금박막의 경우는 PMA가 불가능한 것으로 여겨져 왔다. 그럼으로서 PMA에 대한 근원에 대한 명확한 해석이 필요하게 되었다. 또한 보자력(coercivity)은 불순물의 함량이 감소할수록, 그리고 내부적 변형이 제거될수록 감소하기 때문에, 계면 및 결정구조와 관련이 있는 것으로 알려져 있다. 이러한 자기적 특성을 관찰하고자 [Pt(51 )/Co(112 )]4, [Pt(90 )/Co(66 )]4, 그리고 [Pt(121 )/Co(30 )]4, 다층박막과 이들 박막을 80kV Ar+ 이온선 혼합후 박막의 결정성 변화를 관찰하기 위하여 GXRD (glancing x-ray diffraction) 스펙트럼을 얻어보았다. 그 결과 세 system 모두 disordered fcc 합금박막임을 확인하였다. fcc(111) 방향에 대한 평균 격자공간(lattice spacing)의 크기변화는 한층 당의 Co 두께가 두꺼울수록 거의 선형적으로 감소함을 볼수 있었다. MOKE 실험에 의하면, 이들 다층박막이나 합금박막의 경우 모두, in-plane 방향에 대해 자화 용이축(easy magnetization axis)을 가지고 있었다. 그리고 보자력의 크기에 있어서, 다층 박막의 경우에 있어서 Co 층에 두께 두꺼울수록 보자력의 크기가 감소하였지만 그림1에서와 같이 합금박막의 경우는 정반대로 Co층의 두께가 얇을수록 보자력의 크기가 감소함을 관찰하였다.

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Evaluation of Shielding Performance of 3D Printer Materials for High-energy Electron Radiation Therapy (고 에너지 전자선 치료를 위한 3D 프린터 물질의 차폐 성능평가)

  • Chang-Woo, Oh;Sang-Il, Bae;Young-Min, Moon;Hyun-Kyoung, Yang
    • Journal of the Korean Society of Radiology
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    • v.16 no.6
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    • pp.687-695
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    • 2022
  • To find a 3D printer material that can replace lead used as a shield for high-energy electron beam treatment, the shielding composites were simulated by using MCNP6 programs. The Percent Depth Dose (PDD), Flatness, and Symmetry of linear accelerators emitting high-energy electron beams were measured, and the linear accelerator was compared with MCNP6 after simulation, confirming that the source term between the actual measurement and simulation was consistent. By simulating the lead shield, the appropriate thickness of the lead shield capable of shielding 95% or more of the absorbed dose was selected. Based on the absorption dose data for lead shield with a thickness of 3 mm, the shielding performance was analyzed by simulating 1, 5, 10, and 15 mm thicknesses of ABS+W (10%), ABS+Bi (10%), and PLA+Fe (10%). Each prototype was manufactured with a 3D printer, measured and analyzed under the same conditions as in the simulation, and found that when ABS+W (10%) material was formed to have a thickness of at least 10mm, it had a shielding performance that could replace lead with a thickness of 3mm. The surface morphology and atomic composition of the ABS+W (10%) material were evaluated using a scanning electron microscope (SEM) and an energy dispersive X-ray spectrometer (EDS). From these results, it was confirmed that replacing the commercialized lead shield with ABS+W (10%) material not only produces a shielding effect such as lead, but also can be customized to patients using a 3D printer, which can be very useful for high-energy electron beam treatment.