• Title/Summary/Keyword: X선 회절

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Determination of the Residual Stress Distribution along the Depth of Silicon by XRD $p^+$ Method (X선 회절법을 이용한 $p^+$ 실리콘 내 잔류응력의 깊이 방향 분포 추정)

  • Jung, O.C.;Yang, E.H.;Yang, S.S.
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.593-595
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    • 1995
  • X-Ray Diffraction method that gives direct information about the deformation of crystal lattice is used for the determination of profiles of the residual stress along the depth of heavily boron doped silicon. The residual stress distribution is obtained by XRD method as measuring the deformation of the front surface of the $p^+$ silicon layer fabricated through different etch time. It is determined that the compressive residual stress exists in the most region except the font surface.

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The Change of Half Value Breadth and Residual Stress during Fatigue Process in S45C Steel (S45C강의 피로과정에 대한 반가폭 및 잔류응력의 변화)

  • Boo, Myung-Hwan;Koo, Hoo-Taek;Jeong, Jong-Hyun;Park, Young-Chul;Kim, Byeong-Soo;Kim, Young-Suk
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.591-596
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    • 2001
  • The purpose of this study is to examine the change of half value breadth and residual stress during fatigue process in S45C Steel by X-ray diffraction. For S45C Steel, the relationship between the change in fatigue damage of the specimen and the half value breadth, and residual stress of X-ray diffraction profiles during the fatigue processes has been investigated. The half value breadth(HVB) decreases in he early period of fatigue cycle. The change of HVB is relation to cyclic work hardening. In $10{\sim}20%$ of ratio of fatigue life, the change in the half value breadth is not marked. During fatigue process, the residual stress is changed with fatigue cycle increasing.

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Analysis of Wear Proccess in Sliding Contact by X-ray Diffraction (X선회절에 의한 미끄럼접촉시 발생하는 마모과정의 해석(제1보 : 저경도강의 적용))

  • 이한영
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1999.11a
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    • pp.19-24
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    • 1999
  • Understanding of wear mode and prediction of wear rate of parts in sliding contact are very important in field of meterial design relating with wear resistant. This paper has been undertaken to analyze the possibility of elucidation of wear mode and prediction of wear rate for annealed steel in sliding contact using the X-ray diffraction. The sliding wear test with various velocities using pin-on-disc machine and the X-ray diffraction test on the worn surface have been carried out. The results have been shown that the magnitude of residual stress and half-value breadth on the worn surface have a good correlation with wear mode. The difference between before and after test of half-value breadth on worn surface has been shown to be exponential relation with wear rate in the same wear mode.

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A Study on the Machinability and Machining properties of Composite Ceramics$(iC-Al_2O_3)$ by EDM (복합 세라믹스$(iC-Al_2O_3)$의 방전가공특성에 관한 연구)

  • 윤병주
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.4 no.4
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    • pp.61-68
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    • 1995
  • TiC-Al2O3 composite ceramics has high hardness, high strength, high wear and corrosion resistance. Therefore, composite ceramics have been concerned significantly with some excellent properties and many functions as new industrial materials to the industry at large. In present research, experiments are carried out to obtain the machinability and machining properties by EDM. As a result, the most suitable machining conditions of TiC-Al2O3 composite ceramics was that the pulse duration is 10-60$mutextrm{s}$, the peak current is 10-16A. The machining speed and the wear of the tool electrode increased with the increase in peak current.

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Assessment of Fatigue Life for Pipeline Welds Using X-ray Diffraction Method (X선 회절을 이용한 배관용접부의 피로수명 평가)

  • Lee, Sang-Guk;Yu, Geun-Bong;Kim, Ui-Hyeon;Choe, Hyeon-Seon
    • Proceedings of the KWS Conference
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    • 2005.11a
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    • pp.73-75
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    • 2005
  • The objective of this study is to estimate the feasibility of X-ray diffraction method application for fatigue life assessment of the high-temperature pipeline steel such as main steam pipe, reheater pipe and header etc. in power plant. In this study, X-ray diffraction tests using various types of specimen simulated low cycle fatigue damage were performed in order to analyze fatigue properties when fatigue damage conditions become various stages such as 1/4, 1/2 and 3/4 of fatigue life, respectively. As a result of X-ray diffraction tests for specimens simulated fatigue damages, we conformed that the variation of the full width at half maximum intensity decreased in proportion to the increase of fatigue life ratio.

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XRD Analysis of Portland Limestone Cement Paste (포틀랜드 석회석 시멘트에 관한 XRD 분석)

  • Bang, Mi-Jin;Shin, Ki-Su;Park, Ki-Bong
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2018.05a
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    • pp.189-190
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    • 2018
  • This study produced Portland limestone cement at the rate of limestone substitution by grinding limestone and clinker together, and it conducted an XRD analysis to determine the sign language response structure as a basic study on Portland Limestone Cement. As a result of the XRD analysis, the higher the substitution rate of limestone, the more likely it is that the detection rate of ettringite is decreased. Additionally, we could see that the production volume of Mono-carbonate was increasing.

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Analysis of crystalline structure of autogenous tooth bone graft material: X-Ray diffraction analysis (자가치아골이식재의 결정구조 분석: X선 회절 분석)

  • Kim, Gyung-Wook;Yeo, In-Sung;Kim, Su-Gwan;Um, In-Woong;Kim, Young-Kyun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.37 no.3
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    • pp.225-228
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    • 2011
  • This study evaluated the mineral crystalline structure of an autogenous tooth bone graft material. The crystalline structures of the autogenous tooth bone graft material enamel (AutoBT E+), dentin (AutoBT D+), xenograft (BioOss), alloplastic material (MBCP), allograft (ICB) and autogenous mandibular cortical bone were compared using XRD. The XRD pattern of AutoBT dentin and ICB was similar to that of autogenous bone.

Growth of superconducting thin film on metallic substrate by pulsed laser deposition (펄스 레이저 증착법에 의한 금속기판상 초전도 박막의 증착)

  • Jeong, Young-Sik;Lee, Sang-Yeol
    • Proceedings of the KIEE Conference
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    • 1997.07d
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    • pp.1298-1300
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    • 1997
  • 금속기판상 초전도 $YBa_2CU_3O_{7-{\delta}}$ (YBCO) 박막을 yttria-stabilized zirconia (YSZ) 완충막을 이용하여 in situ 펄스 레이저 증착법에 의해 증착하였다. YBCO 박막을 직접 금속기판에 증착하게 되면 YBCO 박막과 금속기판 사이의 계면에서 상호확산현상이 발생하기 때문에 이를 방지하기 위해 YSZ 완충막이 사용되었다. YSZ 완충막의 증착온도가 박막의 결정성과 전기적 특성에 미치는 영향을 알아보기 위해 YSZ 완충막은 여러 가지 온도로 증착되었다. YBCO 박막의 증착온도와 같은 온도로 YSZ 완충막을 증착했을 때보다 YBCO 박막의 증착온도보다 높은 온도로 YSZ 완충막을 증착했을 경우, 증착된 YBCO 박막은 x선 회절에 의해 c 축 방향으로 성장하였음을 알 수 있었고, 저항이 0이 되는 임계온도가 83K가 되는 실험 결과를 얻었다.

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A Study on the Welding Residual Stress Analysis of the Spot Welding Point (전기저항 점용접부의 용접잔류응력 해석에 관한 연구)

  • 손일선;배동호
    • Proceedings of the KWS Conference
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    • 1999.05a
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    • pp.233-236
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    • 1999
  • The welding residual stress should be considered in fatigue stress analysis because it develope during the process of the electric resistance spot welding and it causes bad affect on the fatigue crack initiation and growth at nugget edge of spot welded points. Therefore the accurate estimation of residual stress is crucial. In this study, nonlinear finite element analysis on welding residual stress generated during the process of the spot welding was conducted, and their results were compared with the experimental data measured by X-ray diffraction method. From the results, it was found that welding residual stress existed as tension in the nugget center and as compression around the nugget edge.

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Corrosion resistance behavior of homogenised the Al-Mg-Zn alloy (균질화된 Al-Mg-Zn 합금의 내식성 거동)

  • Choe, In-Gyu;Jo, Su-Ho;Kim, Sang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.170.1-170.1
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    • 2016
  • 일반적으로 Al-Mg-Zn 합금의 ${\beta}$상($Al_aMg_b$) 조직은 내식성의 큰 영향을 미치는 것으로 알려져 있으며 ${\beta}$상 조직이 입계에 연속적으로 형성될 경우 내식성이 감소하는 주요 원인이 되고 있다. 따라서 본 연구에서는 Al-Mg-Zn 합금을 균질화하여 ${\beta}$상 조직을 변화시켰고, 그 변화에 따른 내식성의 거동을 확인하였다. 균질화 조건은 ${\beta}$상 조직의 고용 가능한 온도인 $400^{\circ}C$이상의 온도에서 진행 하였으며 균질화 조건에 따른 미세조직, 조성 분석, ${\beta}$상 조직의 고용정도를 확인하기위해 광학현미경(optical microscpe), 전자현미경(scanning electron microscope), X선 회절 분석법(X-ray Diffraction)을 사용하였다. 또한, 미세조직에 의한 내식성은 $25^{\circ}C$, 3.5wt% NaCl용액에서 분극 시험으로 평가하였다.

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