• Title/Summary/Keyword: Wet Process

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Corrosion Monitoring of Reinforcing Bars in Cement Mortar Exposed to Seawater Immersion-and-dry Cycles (해수침지-건조 환경에 노출된 모르타르속 철근의 부식속도 평가)

  • Kim, Je-kyoung;Kee, Seong-Hoon;Yee, Jurng-Jae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.4
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    • pp.10-18
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    • 2018
  • The primary purposes of this study are to understand a fundamental aspect of current uniformity around a reinforcing bar (rebar) in cement mortar, and to develop an accurate monitoring method in a wet-dry cycling process with the alternative current (AC) impedance method. Three cement mortar specimens with two embedded rebars were prepared in the laboratory. As a main variable, the distance between two rebars was designed to be 10, 20 and 30 mm with the same thickness of 20 mm. To simulate the corrosion of rebars in concrete structures in a marine environment, three cement mortar specimens were exposed to 15 wet-drying cycles (24-hour-immersion in seawater and 48-hour-drying in a room temperature) in the laboratory. It was observed that the potential level shifted to a noble value during corrosion potential monitoring, which is attributed to acceleration of dissolved oxygen diffusion at the drying process. AC impedance was measured in a frequency range from 100 kHz to 1 mHz on a wet-drying process. A theoretical model was proposed to explain the interface condition between the rebars and cement mortar by using the equivalent circuit consisting of a solution resistance, a charge transfer resistance and a CPE (constant phase element). It was observed that the diffusion impedance appeared in a low frequency range as corrosion of rebars progresses. At the drying stage of the wet-drying cycles, the currents line for monitoring tended to be non-uniform at the interface of rebar/mortar, being phase shift, ${\theta}$, close to $-45^{\circ}$.

Thermal Performance Characteristics of Closed-Wet Cooling Tower (밀폐형 냉각탑의 열성능 특성에 관한 실험적 연구)

  • Sarker, M.M.A.;Kim, E.P.;Moon, C.G.;Yoon, J.I.
    • Journal of Power System Engineering
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    • v.9 no.2
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    • pp.88-92
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    • 2005
  • The experiment of thermal performance about closed-wet cooling tower was conducted in this study. A closed cooling tower is a device similar to a general cooling tower, but with cooling tower replaced by a heat exchanger. The test section for this experiment has the process that the cooling water flows from the top of the heat exchanger to the bottom side in the inner part of the tube, and spray water flows in the gravitational direction in the outer side. Air comes in direct contact with the spray water at the outer side of the tube while passing from the lower the upper part having a counterflow to the spray water. The heat transfer pipe used in this experiment is a bare-type tube having an outer diameter of 15.88mm. The heat exchanger is consisted of seven rows and fifteen columns. In this experiment, thermal performance of the cooling tower is derived from overall heat transfer coefficients between the process fluid and sprayed water and volumetric overall mass transfer coefficient between sprayed water and air.

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Trends of phosphorus recovery technology from sewage sludge ash by wet chemical method (습식 화학적 방법에 의한 하수 슬러지 소각재에서의 인 회수 기술동향)

  • Lee, Min-Su;Kim, Dong-Jin
    • Journal of Korean Society of Water and Wastewater
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    • v.32 no.2
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    • pp.131-143
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    • 2018
  • Phosphorus (P) is a limited, essential, and irreplaceable nutrient for the biological activity of all the living organisms. Sewage sludge ash (SSA) is one of the most important secondary P resources due to its high P content. The SSA has been intensively investigated to recover P by wet chemicals (acid or alkali). Even though $H_2SO_4$ was mainly used to extract P because of its low cost and accessibility, the formation of $CaSO_4$ (gypsum) hinders its use. Heavy metals in the SSA also cause a significant problem in P recovery since fertilizer needs to meet government standards for human health. Therefore, P recovery process with selective heavy metal removal needs to be developed. In this paper some of the most advanced P recovery processes have been introduced and discussed their technical characteristics. The results showed that further research is needed to identify the chemical mechanisms of P transformation in the recovery process and to increase P recovery efficiency and the yields.

Design and Fabrication of a Micro-Heat Pipe with High-Aspect-Ratio Microchannels (고세장비 미세채널 기반의 마이크로 히트파이프 설계 및 제조)

  • Oh, Kwang-Hwan;Lee, Min-Kyu;Jeong, Sung-Ho
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.9 s.186
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    • pp.164-173
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    • 2006
  • The cooling capacity of a micro-heat pipe is mainly governed by the magnitude of capillary pressure induced in the wick structure. For microchannel wicks, a higher capillary pressure is achievable for narrower and deeper channels. In this study, a metallic micro-heat pipe adopting high-aspect-ratio microchannel wicks is fabricated. Micromachining of high-aspect-ratio microchannels is done using the laser-induced wet etching technique in which a focused laser beam irradiates the workpiece placed in a liquid etchant along a desired channel pattern. Because of the direct writing characteristic of the laser-induced wet etching method, no mask is necessary and the fabrication procedure is relatively simple. Deep microchannels of an aspect ratio close to 10 can be readily fabricated with little heat damage of the workpiece. The laser-induced wet etching process for the fabrication of high-aspect-ratio microchannels in 0.5mm thick stainless steel foil is presented in detail. The shape and size variations of microchannels with respect to the process variables, such as laser power, scanning speed, number of scans, and etchant concentration are closely examined. Also, the fabrication of a flat micro-heat pipe based on the high-aspect-ratio microchannels is demonstrated.

Wet Air Oxidation Pretreatment of Mixed Lignocellulosic Biomass to Enhance Enzymatic Convertibility

  • Sharma, A.;Ghosh, A.;Pandey, R.A.;Mudliar, S.N.
    • Korean Chemical Engineering Research
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    • v.53 no.2
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    • pp.216-223
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    • 2015
  • The present work explores the potential of wet air oxidation (WAO) for pretreatment of mixed lignocellulosic biomass to enhance enzymatic convertibility. Rice husk and wheat straw mixture (1:1 mass ratio) was used as a model mixed lignocellulosic biomass. Post-WAO treatment, cellulose recovery in the solid fraction was in the range of 86% to 99%, accompanied by a significant increase in enzymatic hydrolysis of cellulose present in the solid fraction. The highest enzymatic conversion efficiency, 63% (by weight), was achieved for the mixed biomass pretreated at $195^{\circ}C$, 5 bar, 10 minutes compared to only 19% in the untreated biomass. The pretreatment under the aforesaid condition also facilitated 52% lignin removal and 67% hemicellulose solubilization. A statistical design of experiments on WAO process conditions was conducted to understand the effect of process parameters on pretreatment, and the predicted responses were found to be in close agreement with the experimental data. Enzymatic hydrolysis experiments with WAO liquid fraction as diluent showed favorable results with sugar enhancement up to $10.4gL^{-1}$.

Ethylene gas adsorption capacity and preserving effect of fruit freshness of Charcoal-fiberboard by wet forming process (습식공법으로 제조한 목탄-목재섬유복합재료의 에틸렌가스 흡착력과 과일 신선도 유지 효과)

  • Lee Hwa Hyoung;Kim Gwan Eui
    • Journal of the Korea Furniture Society
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    • v.14 no.1
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    • pp.1-9
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    • 2003
  • This research was carried out for packing materials and building materials to examine thylene gas adsorption and effect of keeping fruit fresh of wet formed charcoal-fiber mposite made from defibrated fiber of Pinus densiflora Sieb. et Zucc. and white charcoal from uercus variabilis Bl.(wood fiber: charcoal=8:2, 6:4, 4:6, 2:8), with/without phenol formaldehyde resin(PF, Non volatile content:$52\%$, resin content $1,3,5\%$). The results are summarized as follows: 1. The higher the charcoal content, the more the ethylene gas adsorption. At the same mixing ratio of fiber to charcoal, $\#100-200$ of charcoal particle size gave the better reslts than $\#60-100$. 2. Adding PF into the charcoal fiber composite decreased the capacity of ethylene gas adsorption but there was no significant difference until $5\%$ adding amount of PF. 3. For keeping fruit fresh for a long time, Charcoal fiber composite was $66\%$ longer than control. The higher the white charcoal content, the longer fresh time.

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Effects of Spinning Conditions on Properties of Polyester Yarn Prepared using an Ultra-high-speed Melt Spinning Technique Equipped with a Steam Chamber

  • Ho, Yo-Seung;Kim, Hak-Yong;Jin, Fan-Long;Park, Soo-Jin
    • Bulletin of the Korean Chemical Society
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    • v.31 no.11
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    • pp.3252-3258
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    • 2010
  • In this study, the effects of the various parameters of spinning and drawing processes on the properties of polyester full drawn yarn (FDY) prepared by steam processing during high-speed spinning were investigated using several techniques. The wet shrinkage ratio of the FDY was able to be manipulated by controlling the temperature and draw ratio. The FDY made using the steam high speed spinning technique exhibited identical properties (such as tenacity, elongation, and wet shrinkage ratio) to that of regular FDY, made using the spin-draw process. FDY prepared using the steam process during high-speed spinning showed excellent dyeability. The dye pick-up of the polyester yarn spun at high-speed spinning was found to be improved when dyed under an atmospheric pressure of $100^{\circ}C$. This result was the same as regular FDY dyed under a high pressure of $130^{\circ}C$.

Fabrication of Micro Diamond Tip Cantilever for AFM and its Applications (AFM 부착형 초미세 다이아몬드 팁 켄틸레버의 제작 및 응용)

  • Park J.W.;Lee D.W.
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2005.05a
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    • pp.395-400
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    • 2005
  • Nano-scale fabrication of silicon substrate based on the use of atomic force microscopy (AFM) was demonstrated. A specially designed cantilever with diamond tip, allowing the formation of damaged layer on silicon substrate by a simple scratching process, has been applied instead of conventional silicon cantilever for scanning. A thin damaged layer forms in the substrate at the diamond tip-sample junction along scanning path of the tip. The damaged layer withstands against wet chemical etching in aqueous KOH solution. Diamond tip acts as a patterning tool like mask film for lithography process. Hence these sequential processes, called tribo-nanolithography, TNL, can fabricate 2D or 3D micro structures in nanometer range. This study demonstrates the novel fabrication processes of the micro cantilever and diamond tip as a tool for TNL using micro-patterning, wet chemical etching and CVD. The developed TNL tools show outstanding machinability against single crystal silicon wafer. Hence, they are expected to have a possibility for industrial applications as a micro-to-nano machining tool.

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Use of Calcium Carbonate for Improving Solid Content of KOCC Wet Web (탄산칼슘 적용에 의한 KOCC 지필의 고형분 증대)

  • Hwang, In-Young;Ji, Sung-Gil;Seo, Yung-Bum
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.6
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    • pp.1-9
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    • 2013
  • For the manufacture of linerboard with 100% KOCC, we tried to increase the solid content of wet web by employing GCC (grounded calcium carbonate) in the fiber furnish to save drying energy. Three different diameters of GCC, namely, 5, 10, and $35{\mu}m$, were used. To complement the strength loss by the addition of GCC, cationic starch and refining treatment were tried. It was found that the addition of $10-35{\mu}m$ dia. GCC to KOCC for $180g/m^2$ basis weight sheets increased the solid content of the furnish about 1-1.5% with better bulk and drainage properties. The loss of strength properties were compensated by the application of cationic starch and/or refining process to the KOCC furnish. The dia. of GCC of $35{\mu}m$ was, however, too large to make smooth surface of the sample sheet. So, the optimization process was required before implementing the results to the mill by selecting proper diameter and shape of the calcium carbonate.

Fabrication of Micro Diamond Tip Cantilever for AFM-based Tribo-Nanolithography (AFM 기반 Tribo-Nanolithography 를 위한 초미세 다이아몬드 팁 켄틸레버의 제작)

  • Park Jeong-Woo;Lee Deug-Woo
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.8 s.185
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    • pp.39-46
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    • 2006
  • Nano-scale fabrication of silicon substrate based on the use of atomic force microscopy (AFM) was demonstrated. A specially designed cantilever with diamond tip, allowing the formation of damaged layer on silicon substrate by a simple scratching process, has been applied instead of conventional silicon cantilever for scanning. A thin mask layer forms in the substrate at the diamond tip-sample junction along scanning path of the tip. The mask layer withstands against wet chemical etching in aqueous KOH solution. Diamond tip acts as a patterning tool like mask film for lithography process. Hence these sequential processes, called tribo-nanolithography, TNL, can fabricate 2D or 3D micro structures in nanometer range. This study demonstrates the novel fabrication processes of the micro cantilever and diamond tip as a tool for TNL using micro-patterning, wet chemical etching and CVD. The developed TNL tools show outstanding machinability against single crystal silicon wafer. Hence, they are expected to have a possibility for industrial applications as a micro-to-nano machining tool.