• Journal of the Korean Wood Science and Technology
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• 제46권5호
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• pp.486-496
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• 2018

4점 휨 시험에서 지간 길이에 따른 낙엽송 제재목의 휨 성능 변화를 알아보기 위하여 연구를 진행하였다. 연구에 사용된 시험편의 크기는 38(너비) ${\times}$ 89(깊이) ${\times}$ 3,600(길이) $mm^3$이며, 평균 기건 밀도와 함수율은 각각 $543.5kg/m^3$, 10.5%이었다. 낙엽송 육안 등급 1등급 248본을 두 그룹으로 나눠, 지간 거리 1,650 mm와 3,000 mm에서 휨 실험을 진행하여 휨 강도와 휨 탄성계수를 도출하였다. 휨 탄성계수는 유의 수준 5%에서 지간 거리에 따라 차이가 없다고 판단된 반면 휨 강도는 차이가 있었으며, 지간에 반비례하였다. 지간 거리 1,650와 3,000 mm에서 휨 강도의 5% 하한치는 각각 28.65와 25.70 MPa로 확인되었다. 지간 거리에 따른 휨 강도 차이는 백분위 수가 증가함에 따라 커지는 것으로 확인되었으며, 이는 와이블 최약 링크 파손 이론에 의한 치수 효과 때문으로 사료된다. 따라서 지간 대 깊이 비가 15 이상으로만 제한되어 있는 목구조용 실대재 휨 시험법(KS F 2150)에 치수 효과를 고려할 수 있는 방법이 포함되어야 할 것으로 판단된다. 이를 통해 다양한 치수의 제재목에서 얻어지는 강도를 설계 값에 반영할 수 있을 것으로 기대된다.

• Carbon letters
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• 제24권
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• pp.97-102
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• 2017

Graphite fibers are materials with a high specific modulus that have attracted much interest in the aerospace industry, but their high manufacturing cost and low yield are still problems that prevent their wide applications in practice. This paper presents a laser-based process for graphitization of carbon fiber (CF) and explores the effect of laser radiation on the microstructure of CF. The obtained Raman spectra indicate that the outer surface of CF evolves from turbostratic structures into a three-dimensional ordered state after being irradiated by a laser. The X-ray diffraction data revealed that the growth of crystallite was parallel to the fiber axis, and the interlayer spacing $d_{002}$ decreased from 0.353 to 0.345 nm. The results of scanning electron microscopy revealed that the surface of irradiated CFs was rougher than that of the unirradiated ones and there were scale-like small fragments that had peeled off from the fibers. The tensile modulus increased by 17.51% and the Weibull average tensile strength decreased by 30.53% after being irradiated by a laser. These results demonstrate that the laser irradiation was able to increase the graphitization degree of the CFs, which showed some properties comparable to graphite fibers.

• 한국세라믹학회지
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• 제42권8호
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• pp.582-587
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• 2005

AlN-BN ceramic composites were fabricated and their mechanical properties were investigated. The relative density of hot-pressed composites decreased with increasing BN content, but over $99\%$ could be obtained with 30 $vol\%$ BN in AlN. YAG was formed in the composites and monolithic AlN as a second phase by the reaction between $Y_2O_3$, added as sintering aid, and $Al_2O_3$. As expected, Vickers hardness and Young's modulus decreased with increasing BN content. The three-point flexural strength also showed similar behavior decreasing from 500 MPa of monolith down to 250 MPa by the addition 30 $vol\%$ BN. However, interestingly, the standard deviation of the strength values decreased significantly as BN was added to AlN. As a result, the Weibull modulus of the AlN-30 $vol\% BN composite was 21.3, which was extremely high. Fractography and crack path studies revealed that BN platelets induced grain pull-out and crack bridging in a bigger scale during crack propagation. Consequently, fracture toughness increased as more BN was added, reaching 4.5 $MPa\sqrt{m}$ at 40 $vol\%$ BN.

• Earthquakes and Structures
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• 제5권4호
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• pp.439-459
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• 2013

Main objective of the present study is to determine the statistical properties and suitable probability distribution functions of spectral displacements from nonlinear static and nonlinear dynamic analysis within the frame work of Monte Carlo simulation for typical low rise and high rise RC framed buildings located in zone III and zone V and designed as per Indian seismic codes. Probabilistic analysis of spectral displacement is useful for strength assessment and loss estimation. To the author's knowledge, no study is reported in literature on comparison of spectral displacement including the uncertainties in capacity and demand in Indian context. In the present study, uncertainties in capacity of the building is modeled by choosing cross sectional dimensions of beams and columns, density and compressive strength of concrete, yield strength and elastic modulus of steel and, live load as random variables. Uncertainty in demand is modeled by choosing peak ground acceleration (PGA) as a random variable. Nonlinear static analysis (NSA) and nonlinear dynamic analysis (NDA) are carried out for typical low rise and high rise reinforced concrete framed buildings using IDARC 2D computer program with the random sample input parameters. Statistical properties are obtained for spectral displacements corresponding to performance point from NSA and maximum absolute roof displacement from NDA and suitable probability distribution functions viz., normal, Weibull, lognormal are examined for goodness-of-fit. From the hypothesis test for goodness-of-fit, lognormal function is found to be suitable to represent the statistical variation of spectral displacement obtained from NSA and NDA.

• 한국세라믹학회지
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• 제39권1호
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• pp.51-56
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• 2002

고순도 알루미나 분말에 소결조제로서 초산 마그네슘과 질산 마그네슘을 1000ppm첨가하여 제작한 소결체에 대해서 소결조제로 사용한 MgO의 출발물질의 종류가 소결체 특성에 미치는 영향을 고찰하였다. 초산 마그네슘과 질산 마그네슘을 사용해서 제작한 소결체에 대해서 소결온도 1$600^{\circ}C$에서 상대밀도의 급격한 감소가 확인되었고 SEM관찰결과 소결조제로 사용한 두 종류의 출발물질을 첨가한 경우에 동일하게 소결체의 outer layer에서는 입성장 및 기공이 형성되어있고 inner layer에서는 알루미나 입계에 제2상의 존재가 관찰되었다. 이 시편의 EPMA을 이용한 원소분석결과로부터 소결온도 1$600^{\circ}C$에서 알루미나 입계에 존재하는 제2상은 Mg를 함유한 혼합물이라는 것을 알 수 있었다.

• 한국세라믹학회지
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• 제41권10호
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• pp.723-727
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• 2004

Three kinds of $Si_3N_4$ powders (M-11, SN-ESP, and SN-E10) were gas-pressure sintered at $1700-1900^{\circ}C$ for 2 h under 18 atm $N_2$. Their densification behavior was investigated and compared as well as the mechanical properties and microstructure of the resulting ceramics. SN-ESP and SN-E10 started to reach nearly full densification at $1750^{\circ}C$ and showed almost no decomposition up to $1900^{\circ}C$. In contrast, M-11 was not fully densified until $1800^{\circ}C$ and showed about $3\%$ weigh loss at $1900^{\circ}C$ indicating poor thermal stability. SN-ESP and SN-E10 showed much higher strength both at room temperature and $1200^{\circ}C$ than M-11 when fully densified. Compared with SN-ESP, SN-E10 was not only a little better in strength (both at room temperature and $1200^{\circ}C$) and fracture toughness but also much higher in the Weibull modulus due to more interlocked microstructure by well elongated grains.

• 한국세라믹학회지
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• 제35권3호
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• pp.219-230
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• 1998

Various interlayer materials have been tested for active metal(Cusil ABA) brazing of Si3N4/S. S316 joint. In general multilayer joint had higher strength(80-150 MPa) and better reliability than monolayered one. The joint with Cu(0.2)/Mo(0.3)/Cu(0.2mm) interlayer showed the highest bending strength of abou 490 MPa and the joint with Cu(0.2)/Mo(0.3mm) interlayer the best reliability (14.6 Weibull modulus). The stresses distributed in joint materials during 4-point bending test were estimated by CAE von Mises analysis; the estimated stresses were In good agreement with the measured data. In multilayer joint Cu was though to reduce the residual stresses induced by the difference in thermal expansion coefficient between the ceramic Mo and metal It apperared that a Cu/Mo was optimum interlayer material for Si3N4/S. S316 joint with high bending strength (420 MPa) and reliability. In addition the various shapes and types of compound were examined by EPMA in joining interface.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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• pp.317-318
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• 2012

현재의 반도체 산업에서 Hafnium oxide와 Hafnium silicates같은 high-k 물질은 CMOS gate와 DRAM capacitor dielectrics로 사용하기 위한 대표적인 물질에 속한다. MOSFET (metal oxide semiconductor field effect transistor)구조에서 gate length는 16 nm 이하로 계속 미세화가 연구 중이고, 또한 gate는 기존구조에서 Multi-gate구조로 다변화가 일어나고 있다. 이를 통해 게이트 절연막은 그 구조와 활용범위가 다양해지게 될 것이다. 동시에 leakage current와 dielectric break-down을 감소시키는 연구가 중요해지고 있다. 그러나 나노 영역에서의 기계적 특성에 대한 연구는 전무한 상태이다. 따라서 복잡한 회로 공정, 다양한 Multi-gate 구조, 신뢰도의 향상을 위해서는 유전박막 물질자체와 계면에서의 물리적, 기계적인 특징의 측정이 상당히 중요해지고 있다. 이에 본 연구는 Nano-indenter의 통해 경도(Hardness)와 탄성계수(Elastic modulus) 등의 측정을 통하여 시료 표면의 나노영역에서의 기계적 특성을 연구하고자 하였다. $HfO_2$게이트 절연막은 rf magnetron sputter를 이용해 Si (silicon) (100)기판위에 박막형태로 증착하였고, 이후 furnace에서 질소분위기로 온도(400, 450, $500^{\circ}C$)를 달리하여 20분 열처리를 하였다. 또한 Weibull distribution을 이용해 박막의 characteristic value를 계산하였으며, 실험결과 열처리 온도가 $400^{\circ}C$에서 $500^{\circ}C$로 증가함에 따라 경도와 탄성계수는 7.4 GPa에서 10.65 GPa으로 120.25 GPa에서 137.95 GPa으로 각각 증가하였다. 이는 재료적 측면으로 재료의 구조적 우수성이 증가된 것으로 판단된다.

• 한국세라믹학회지
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• 제37권3호
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• pp.211-218
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• 2000

The attrition-milled powder mixtures of Al and Al2O3 were oxidized below 140$0^{\circ}C$ for 1 hr and post-sintered at 150$0^{\circ}C$ and 1$600^{\circ}C$ for 2 hr. During attrition milling, ZrO2 was added to the system by grinding effect of ZrO2 balls. The average particle size of the powder mixtures was decreased by the attrition milling as the aluminum content decrease. Above 120$0^{\circ}C$, sintering behaviro was observed on the fine Al2O3 particles resulted from the oxidation of Al. The specimens heat-treated at 140$0^{\circ}C$ for 1 hr showed the bending strength of 166 MPa and hardness of 220 MPa. The specimens post-sintered at 1$600^{\circ}C$ for 2hr had a linear shrinkage of 9~12% and a relative density of about 95%. After the post-sintering, the specimens having 55 vol% Al content revealed the bending strength of 513 MPa and hardness of 718 MPa. The Weibull modulus to the bending strength was about 16.

• 대한기계학회논문집A
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• 제20권4호
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• pp.1241-1250
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• 1996

The characteristics of fatigue cumulative damage and fatigue life of 8-harness satin woven CFRP composites with a circular hole under constant amplitude and 2-level block loading are estimated by Stochastic Makov chain model. It is found in this study that the fatigue damage accumulation behavior is very random and the fatigue damage is accumulated as two regions under constant amplitude fatigue loading. In constant amplitude fatigue loading the predicted mean number of cycles to a specified damage state by Markov chain model shows a good agreement with the test result. The predicted distribution of the fatigue cumulative damage by Markov chain model is similar to the test result. The fatigue life predictions under 2-level block loading by Markov chain model revised are good fitted to the test result more than by 2-parameter Weibull distribution function using percent failure rule.