• Title/Summary/Keyword: Water quality measurement

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LC-MS/MS analysis and antioxidant activity of Dendropanax morbiferus extract. (황칠나무(Dendropanax morbiferus) 잎 추출물의 LC-MS/MS 분석 및 항산화 효과)

  • Min Jung Kim;Jae Dong Son;Ye Jin Yang;Ji Woong Heo;Hu Jang Lee;Kwang Il Park
    • Herbal Formula Science
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    • v.32 no.3
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    • pp.235-245
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    • 2024
  • Objective : The study's objective is to assess the components of Dendropanax morbifera (DM) utilizing UPLC-MS/MS and assess their antioxidant properties in order to establish fundamental information for quality control of herbal formulations. Methods : The DM leaves were ground into powder and extracted with water at 80℃. The extract was subsequently concentrated and subjected to freeze-drying for subsequent analysis. The LC-MS/MS analysis was performed using a 1260 series HPLC system and a 3200 QTrap tandem mass system in positive ion mode, with detection conducted at 280 nm. The Folin-Ciocalteu method was employed to measure the phenolic content, while a colorimetric method using aluminum chloride was used to determine the flavonoid content, with gallic acid and quercetin as standards, respectively. The evaluation of antioxidant activity was conducted through the measurement of DPPH radical scavenging activity, by adding the DPPH solution to the extract and recording the absorbance at 517 nm. Results : The UPLC-MS/MS analysis identified five polyphenolic compounds in the DM extract, specifically syringin, 6-hydroxyluteolin 7-O-laminaribioside, shaftoside, rutin, and kaempferol-3-O-rutinoside. The extract was found to contain a total phenolic content of 83.106 ± 0.21 mg GAE/g and a total flavonoid content of 87.963 ± 1.014 mg QE/g. The DM extract demonstrated substantial antioxidant properties, resulting in a reduction of DPPH radicals that was evident at concentrations as low as 40 ㎍/㎖. Conclusions : The study determined important polyphenolic compounds in DM and established its considerable antioxidant efficacy. These findings provide evidence for the efficacy of DM in disease prevention related to oxidative stress and establish a foundation for ensuring quality control in herbal preparations.

A Method to Evaluate the Radar Rainfall Accuracy for Hydrological Application (수문학적 활용을 위한 레이더 강우의 정확도 평가 방법)

  • Bae, Deg-Hyo;Phuong, Tran Ahn;Yoon, Seong-Sim
    • Journal of Korea Water Resources Association
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    • v.42 no.12
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    • pp.1039-1052
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    • 2009
  • Radar measurement with high temporal and spatial resolutions can be a valuable source of data, especially in the areas where rain gauge installment is not practical. However, this kind of data brings with it many errors. The objective of this paper is to propose a method to evaluate statistically the quantitative and qualitative accuracy at different radar ranges, temporal intervals and raingage densities and use a bias adjustment technique to improve the quality of radar rainfall for the purpose of hydrological application. The method is tested with the data of 2 storm events collected at Jindo (S band) and Kwanak (C band) radar stations. The obtained results show that the accuracy of radar rainfall estimation increases when time interval rises. Radar data at the shorter range seems to be more accurate than the further one, especially for C-band radar. Using the Monte Carlo simulation experiment, we find out that the sampling error of the bias between radar and gauge rainfall reduces nonlinearly with increasing raingage density. The accuracy can be improved considerably if the real-time bias adjustment is applied, making adjusted radar rainfall to be adequately good to apply for hydrological application.

Analysis of wet chemical tunnel oxide layer characteristics capped with phosphorous doped amorphous silicon for high efficiency crystalline Si solar cell application

  • Kang, Ji-yoon;Jeon, Minhan;Oh, Donghyun;Shim, Gyeongbae;Park, Cheolmin;Ahn, Shihyun;Balaji, Nagarajan;Yi, Junsin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.406-406
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    • 2016
  • To get high efficiency n-type crystalline silicon solar cells, passivation is one of the key factor. Tunnel oxide (SiO2) reduce surface recombination as a passivation layer and it does not constrict the majority carrier flow. In this work, the passivation quality enhanced by different chemical solution such as HNO3, H2SO4:H2O2 and DI-water to make thin tunnel oxide layer on n-type crystalline silicon wafer and changes of characteristics by subsequent annealing process and firing process after phosphorus doped amorphous silicon (a-Si:H) deposition. The tunneling of carrier through oxide layer is checked through I-V measurement when the voltage is from -1 V to 1 V and interface state density also be calculated about $1{\times}1012cm-2eV-1$ using MIS (Metal-Insulator-Semiconductor) structure . Tunnel oxide produced by 68 wt% HNO3 for 5 min on $100^{\circ}C$, H2SO4:H2O2 for 5 min on $100^{\circ}C$ and DI-water for 60 min on $95^{\circ}C$. The oxide layer is measured thickness about 1.4~2.2 nm by spectral ellipsometry (SE) and properties as passivation layer by QSSPC (Quasi-Steady-state Photo Conductance). Tunnel oxide layer is capped with phosphorus doped amorphous silicon on both sides and additional annealing process improve lifetime from $3.25{\mu}s$ to $397{\mu}s$ and implied Voc from 544 mV to 690 mV after P-doped a-Si deposition, respectively. It will be expected that amorphous silicon is changed to poly silicon phase. Furthermore, lifetime and implied Voc were recovered by forming gas annealing (FGA) after firing process from $192{\mu}s$ to $786{\mu}s$. It is shown that the tunnel oxide layer is thermally stable.

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A Study on the Relation Characteristics between Bubble Size Distribution and Floating Time (버블의 크기별 입도분포와 부상시간과의 상관특성에 관한 연구)

  • Jeon, Gun;Park, Chul-Hwi
    • Journal of Korean Society of Environmental Engineers
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    • v.39 no.5
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    • pp.277-281
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    • 2017
  • Lately rainfall characteristics that it rains a lot in a short space of time often occurs. Because of this meteorological phenomena, the flow rate and concentration of initial rainfall for runoff and combined sewer overflows are changed. In the case of this inlet fluctuation, the flotation method at high surface loading rate is suitable for water quality management. the flotation method is able to meet the removal rate requirements of water public zone in 5 to 10 min which is irelatively short period. For assessment and diagonision of flotation method, A/S ratio is applied until now. But unfortunately, this has some limits for evaluation standard for certification and assessment of technical diagnosis and operation. This is why there is different efficiency in the bubble distribution at the same A/S ratio. The velocity and time of floating is changed by the different bubble distributions. The floating time affects the plant volume because the time factor make size dicision. Therefore the charateristics of bubble distribution and floating time at the same A/S ratio is necessary to apply to evaluation standard for certification and assessment of technical diagnosis and operation. For generalization of the method in certification and assessment, the characteristics of bubble distribution was studied. Until recently, using the optical device and shooting live video, there are some analysis technology of the floating factors. But this kind of technology is influenced by the equipment. with this level of confidence about the results, it is difficult to apply to generalize. According this reasons, this study should be applied on experiment generalization of method about measurement of relation between bubble distribution and floating time.

A Study on Characteristics of Animal Glue depending on Pretreatment and Evaluation Condition (아교 전처리 및 평가 조건에 따른 특성연구)

  • Oh, Seong Min;Yu, Ji A;Lee, Na Ra;Kim, Tae Heon;Kim, Seong Eun;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.35 no.6
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    • pp.701-708
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    • 2019
  • Animal glue is a natural adhesive made from processed skins or bones of animals. It is widely used in wooden crafts, papercrafts, dancheong painting, and pictures. Accurate evaluation of the quality of animal glues during production and use is difficult because there is no formal method for testing the glue's properties during pretreatment and measurement conditions. Thus, in this study, a series of tests were carried out by changing the conditions of swelling, temperature, and concentration of animal glue and gelatin sold on the market. Twelve types of animal glues were evaluated, having a viscosity range of 12.67 cP to 29.43 cP. The results showed that the physical characteristics of the glues were stable when allowed to swell for six h in distilled water(23℃). When 10%(by weight in distilled water) of the animal glue was measured in the reflective mode of a spectrophotometer, the optical characteristics of the glues were stable. Powdered animal glues have a medium brightness and middle-high chroma. Relative to powdered glues, stick animal glues have a low brightness and a medium chroma. Based on the results of this study, it is expected that the data can be assembled into a form so that animal glue workers can use it as a reference for the preparation of evaluation standards for testing the characteristics of animal glues.

A new method for determining OBS positions for crustal structure studies, using airgun shots and precise bathymetric data (지각구조 연구에서 에어건 발파와 정밀 수심 자료를 이용한 OBS 위치 결정의 새로운 방법)

  • Oshida, Atsushi;Kubota, Ryuji;Nishiyama, Eiichiro;Ando, Jun;Kasahara, Junzo;Nishizawa, Azusa;Kaneda, Kentaro
    • Geophysics and Geophysical Exploration
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    • v.11 no.1
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    • pp.15-25
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    • 2008
  • Ocean-bottom seismometer (OBS) positions are one of the key parameters in an OBS-airgun seismic survey for crustal structure study. To improve the quality of these parameters, we have developed a new method of determining OBS positions, using airgun shot data and bathymetric data in addition to available distance measurements by acoustic transponders. The traveltimes of direct water waves emitted by airgun shots and recorded by OBSs are used as important information for determining OBS locations, in cases where there are few acoustic transponder data (<3 sites). The new method consists of two steps. A global search is performed as the first step, to find nodes of the bathymetric grid that are the closest to explaining the observed direct water-wave traveltimes from airgun shots, and acoustic ranging using a transponder system. The use of precise 2D bathymetric data is most important if the bottom topography near the OBS is extremely rough. The locations of the nodes obtained by the first step are used as initial values for the second step, to avoid falling into local convergence minima. In the second step, a non-linear inverse method is executed. If the OBS internal clock shows large drift, a secondary correction for the OBS internal clock is obtained, as well as the OBS location, as final results by this method. We discuss the error and the influence of each measurement used in the determination of OBS location.

Development of a Simple In-Situ Data Logger (간단한 현장 데이타 수집장치의 개발에 관한 연구)

  • Yeo, Woo-Kwang;Yoon, Byung-Man;Lee, Jong-Kuk
    • Water for future
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    • v.29 no.2
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    • pp.249-260
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    • 1996
  • There have been easily found a number of examples that misleading or unreasonable measuring data set of physical variables are often produced in the field and the laboratory. The primary reason is that the specific requirements of civil engineers are initially disregarded in designing the experimental apparatus. It results from a lack of mutual understanding and co-operating between the user group and the maker. Therefore, their fundamental knowledge and apprehension become indispensible in order to obtain measuring data with high confidence and good quality In this study it is shortly explained the basic structure and the operation system of the experimental equipments commonly used at the present. A simple measuring set is developed which is quite easy for a general civil engineer to design and operate without any other specialty of mostly electricity electronics. Based upon this requirement, one of data logger named PPDL8 is newly designed by making use of the parallel port in the personal computer, consisting of multi-channels able to measure 8 different point values simultaneously. It can also use many valuable sub-programs existing in PC because the user makes his own programs necessary for measurement, by himself. Of all things, it has a great advantage to increase the applicability of field measurements much larger when adopting the notebook computer to operate with small battery only. In addition this study gives, in fact, the excellent agreements of in-situ field variables by showing their measuring results of temperature, distance and turbidity.

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Measurement of Dust Concentration in a Mechanically Ventilated Broiler House and Analysis of Dust Generation from Ground Beds (강제환기식 계사의 공기 중 분진 농도 측정 및 바닥재로부터의 분진 발생량 분석)

  • Kwon, Kyeong Seok;Jo, Ye Seul;Lee, In Bok;Ha, Tae Hwan;Hong, Se Woon
    • Journal of The Korean Society of Agricultural Engineers
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    • v.56 no.6
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    • pp.31-43
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    • 2014
  • Confined and mechanically ventilated broiler house has been recently come into wide use to increase productivity and control rearing conditions. However, high dust concentration inside facility can threaten respiratory welfare of farmers and broilers. In Korea, there is no regulation in terms of air quality control inside agricultural facilities and sufficient data is not available. To cope with these, periodic monitoring of inhalable and respirable dust concentration were conducted according to season, broiler's activity and specific events such as shipment work for broilers in mechanically ventilated broiler house. Chamber experiment was also designed to analyze mechanism of dust generation from ground beds according to water contents and surrounding wind environment. Results showed that significant increase of inhalable (p=0.002) and respirable (p=0.03) dust were observed when activity of broilers was high according to entrance of the workers. Even shipment work for matured broilers, high level of dust were observed; inhalable dust was exceeded the threshold limit over maximum 303 % and respirable dust was over maximum 1,550 %, implying that acute respiratory symptoms could be manifested for the workers. From the chamber experiment, critical water contents for interrupting of dust generation were measured; about 45 % for inhalable dust and about 50 % for respirable dust. These results can be a trigger for designing plan of dust control however it still needs consideration of various environmental conditions, hygiene problems, etc.

Relation of Freshwater Discharge and Salinity Distribution on Tidal Variation around the Yeomha Channel, Han River Estuary (한강하구 염하수로 주변의 조석변화에 따른 염분분포와 담수와의 상관관계)

  • Yoon, Byung-Il;Woo, Seung-Buhm
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.24 no.4
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    • pp.269-276
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    • 2012
  • Salinity distribution in estuary and tidal river is presented by many parameters including tidal forcing, river discharge and geographical effect. Understanding the characteristics of salinity structure is very important in the aspect of water-quality, ecological, and engineering viewpoint. Field measurement was carried out to study the distribution of salinity structure at 2 surface stations at Yeomha channel in the Han River estuary. The results of short- and long-term salinity change according to short and long tidal variability is investigated. For analyzing the axial salinity distribution at Yeomha channel, the salinity data from NFRDI is used in this study. The relationship between freshwater discharge and salinity distribution is represented through the nonlinear regression equation. The empirical equation for salt intrusion length scale, including tide, river discharge, and topographical effect is presented. As the comparison of empirical equation and existing data collected in study area, the characteristic of salt intrusion length and salinity distribution is changed by tide, fresh water, and geographical effect.

The Noise Performance of Diffusion Tensor Image with Different Gradient Schemes (확산 텐서 영상에서 확산 경사자장의 방향수에 따른 잡음 분석)

  • Lee Young-Joo;Chang Yongmin;Kim Yong-Sun
    • Journal of Biomedical Engineering Research
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    • v.25 no.6
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    • pp.439-445
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    • 2004
  • Diffusion tensor image(DTI) exploits the random diffusional motion of water molecules. This method is useful for the characterization of the architecture of tissues. In some tissues, such as muscle or cerebral white matter, cellular arrangement shows a strongly preferred direction of water diffusion, i.e., the diffusion is anisotropic. The degree of anisotropy is often represented using diffusion anisotropy indices (relative anisotropy(RA), fractional anisotropy(FA), volume ratio(VR)). In this study, FA images were obtained using different gradient schemes(N=6, 11, 23, 35. 47). Mean values and the standard deviations of FA were then measured at several anatomic locations for each scheme. The results showed that both mean values and the standard deviations of FA were decreased as the number of gradient directions were increased. Also, the standard error of ADC measurement decreased as the number of diffusion gradient directions increased. In conclusion, different gradient schemes showed a significantly different noise performance and the schem with more gradient directions clearly improved the quality of the FA images. But considering acquisition time of image and standard deviation of FA, 23 gradient directions is clinically optimal.