• Title/Summary/Keyword: Water droplet ion beam

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Generation of Water Droplet Ion Beam for ToF-SIMS Analysis

  • Myoung Choul Choi;Ji Young Baek;Aram Hong;Jae Yeong Eo;Chang Min Choi
    • Mass Spectrometry Letters
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    • v.14 no.4
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    • pp.147-152
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    • 2023
  • The increasing demand for two-dimensional imaging analysis using optical or electronic microscopic techniques has led to an increase in the use of simple one-dimensional and two-dimensional mass spectrometry imaging. Among these imaging methods, secondary-ion mass spectrometry (SIMS) has the best spatial resolution using a primary ion beam with a relatively insignificant beam diameter. Until recently, SIMS, which uses high-energy primary ion beams, has not been used to analyze molecules. However, owing to the development of cluster ion beams, it has been actively used to analyze various organic molecules from the surface. Researchers and commercial SIMS companies are developing cluster ion beams to analyze biological samples, including amino acids, peptides, and proteins. In this study, a water droplet ion beam for surface analysis was realized. Water droplets ions were generated via electrospraying in a vacuum without desolvation. The generated ions were accelerated at an energy of 10 keV and collided with the target sample, and secondary ion mass spectra were obtained for the generated ions using ToF-SIMS. Thus, the proposed water droplet ion-beam device showed potential applicability as a primary ion beam in SIMS.

Investigation of Vortical Flow Field Visualization by Micro Water Droplet and Laser Beam Sheet (미세수적과 레이저 평면광에 의한 와류장의 가시화 연구)

  • 이기영;손명환
    • Journal of the Korean Society of Propulsion Engineers
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    • v.6 no.1
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    • pp.55-62
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    • 2002
  • A new off-surface visualization method of using the micro water droplet and laser beam sheet was presented. About a size of 5 to TEX>$10\mu\textrm{m}$ micro water droplet could be made from home-style ultrasonic humidifier, A 3 W Argon ion laser and cylindrical lens were used to generate a laser beam sheet, which interrogate specific cross section of the vortical flow field. Application of this new visualization method was conducted in KAFA small-sized low speed wind tunnel of having the test section of 0TEX>$0.9 m(W){\times}$0.9 m(H){\times}2.1 m(L)$$$. Visualization results show this method relatively easy and safe flow visualization method for wind tunnel testing. Moreover, this method is also make up for the disadvantage of smoke visualization, and can be applied to higher flow velocity range than that of smoke visualization.

The Effect of Ion-Beam Treatment on TiO2 Coatings Deposited on Polycarbonate Substrates

  • Park, Jung-Min;Lee, Jai-Yeoul;Lee, Hee-Young;Park, Jae-Bum
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.6
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    • pp.266-270
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    • 2010
  • The effect of an Ar plasma treatment on polycarbonate substrates was investigated using $TiO_2$ coatings produced by reactive ion-beam assisted sputtering. The typical pressure used during sputtering was about $10^{-4}$ Torr. After the Ar plasma treatment, the contact angle of a water droplet was reduced from $88^{\circ}$ to $52^{\circ}$ and then further decreased to $12^{\circ}$ with the addition of oxygen into the chamber. The surface of the polycarbonate substrate hanged from hydrophobic to hydrophilic with these treatments and revealed its changing nano-scale roughness. The $TiO_2$ films on the treated surface showed various colors and periodic ordering dependant on the film thickness due to optical interference.