• Bulletin of the Korean Chemical Society
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• v.14 no.2
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• pp.200-206
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• 1993

Structures of two polymorphs of ${\alpha},{\alpha}$-trehalose octaacetate monohydrate, $C_{28}H_{38}O_{19}\;{\cdot}\;H_2O$, have been studied by X-ray diffraction method. ${\alpha},{\alpha}$-trehalose (${\alpha}$-D-glucopyranosyl ${\alpha}$-D-glucopyranoside) is a nonreducing disaccharide. The polymorph I belongs to the monoclinic $P2_1$, and has unit cell parameters of a=10.725(l), b=15.110(4), c=11.199(5) ${\AA}$, ${\beta}=108.16(2)^{\circ}$ and Z=2. The polymorph II is orthorhombic $P2_12_12_1$, with a=13.684(4), b=15.802(4), c=17.990(9) ${\AA}$ and Z=4. The final R and R$_w$ values for monoclinic polymorph I are 0.043 and 0.048 and for orthorhombic polymorph II are 0.116 and 0.118, respectively. Those R values of polymorph II are high because the large thermal motions of acetyl groups and the poor quality of the crystal. The molecular conformations in the two polymorphs are similar. Both D-glucopyranosyl rings have chair $^4C_1$ conformations and atoms of glycosidic chain ${\alpha}(1{\rightarrow}1)$ linkage are coplanar. The primary acetate groups of the pyranose residues assume both gauche-trans conformations. The molecules of two polymorphs have pseudo-C$_2$ symmetry at glycosidic O(1) atom. The bond lengths and angles are normal compared with those in other acetylated sugar compounds. The molecules in the monoclinic crystal are held by the hydrogen bonds with the water molecules and by van der Waals forces.

• Transactions of Materials Processing
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• v.31 no.5
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• pp.253-260
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• 2022

In this study, the microstructural characteristics of a high-speed-extruded Mg-5Bi-3Al (BA53) alloy and its tensile, compressive, and high-cycle fatigue properties are investigated. The BA53 alloy is successfully extruded at a die-exit speed of 16.6 m/min without any hot cracking using a large-scale extruder for mass production. The homogenized BA53 billet has a large grain size of ~900 ㎛ and it contains fine and coarse Mg₃Bi₂ particles. The extruded BA53 alloy has a fully recrystallized microstructure with an average grain size of 33.8 ㎛ owing to the occurrence of complete dynamic recrystallization during high-speed extrusion. In addition, the extruded BA53 alloy contains numerous fine lath-type Mg₃Bi₂ particles, which are formed through static precipitation during air cooling after exiting the extrusion die. The extruded BA53 alloy has a high tensile yield strength of 175.1 MPa and ultimate tensile strength of 244.4 MPa, which are mainly attributed to the relative fine grain size and numerous fine particles. The compressive yield strength (93.4 MPa) of the extruded BA53 alloy is lower than its tensile yield strength, resulting in a tension-compression yield asymmetry of 0.53. High-cycle fatigue test results reveal that the extruded BA53 alloy has a fatigue strength of 110 MPa and fatigue cracks initiate at the surface of fatigue test specimens, indicating that the Mg₃Bi₂ particles do not act as fatigue crack initiation sites. Furthermore, the extruded BA53 alloy exhibits a higher fatigue ratio of 0.45 than other commercial extruded Mg-Al-Zn-based alloys.

• 한국해양학회지
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• v.18 no.2
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• pp.104-110
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• 1983

The Intermittent phenomena of the turbulent momentrm transports were closely examined in order to know the nature of intermittency and its fluid dynamic implications in the oceanic turbulent boundary layer. Also the connection between the observed intermittency and the bursting phenomenon was studied in detail. In this investigation, strong intermittency of turbulent momentum transports were found and the peak values of Reynolds stress (i,e., u'w') was about 408 times greater than average Reynolds stress (u',w') in the mid-layer and 270 times greater in the uppcrlayer of the turbulent boundary layer. These values are far greater than presently known maximum value, namely 30 times greater than the average Reynolds stress reported by Gordon (1974) and Heathersaw (1974). The distribution of Reynolds stress were extremely non-normal with the mean peak occurrence period of 5 minutes in the mid-layer and 1. 1 minutes in the upper layer of the turbulent boundary layer. Each teak lasted about 2 seconds in the mid-layer and 1.1 seconds in the upper layer of the turbulent boundary layer. Our dimensionless period of peak occurrence are found to be 33.3 in the mid-layer and 7.3 in the upper-layer, which are substantially larger than the often quoted values of 3.2-6.8 for the bursting period (Jackson, 1976). Some workers have interpreted that the intermittency phenomenon is the retlect of burst across their probe of the currentmeter (Gordon, 1974; Heathersaw, 1974). However, it was known that the burst can be found very near bottom boundary with smoothed bottom (i,e., friction Reynolds number$\leq$3,000) in the laboratory experiments. Through this investigation, it was found that the intermittent strength of the turbulent momentum transports does not conclusively indicate the characteristic feature of the boundary layer turbulence with a rough bottom (i,e., friction Reynolds number$\geq$10$\^$5/).

• Asian-Australasian Journal of Animal Sciences
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• v.23 no.3
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• pp.385-395
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• 2010

The objective of this study was to determine optimal lysine requirement of lactating Mong Cai sows and their piglets. An experiment was conducted using 30 Mong Cai sows in a factorial randomized design with 5 dietary total lysine levels (0.60, 0.70, 0.85, 1.0 and 1.15%) for one-week pre-partum and 5 dietary total lysine levels (0.60, 0.75, 0.90, 1.05 and 1.2%) for lactation diets. Mong Cai sows were about 1 to 2 years old and had an initial body weight of 120 kg (sd = 2.5) after farrowing. Sows were restrictively fed 1.7 kg feed during gestation and were fed ad libitum during lactation. Diets of sows contained about 12% CP during pregnancy and about 14% CP for the lactation period. DE concentration of the diets ranged between 12.5-13.0 MJ of DE. Water was supplied at up to 8 liters per sow per day in a basin. Studied traits were related to both sows and their progeny. Sows were weighed at 107 days of gestation, after farrowing and at weaning. Sow back-fat depth was measured at 110 days of gestation, after farrowing, at 21 days of lactation and at weaning. Number of piglets born, at 24 h after birth, at 21 days of age and at weaning were recorded. Piglets were weighte at birth, at 21 days and at weaning. Supplying lysine one week pre-partum had no effect on the number of piglets born nor litter weight at birth (p = 0.776 and p = 0.224). A positive effect of increasing dietary lysine level during lactation from 0.60 to 1.20% was observed with regard to less sow weight loss, and increased piglet weight at 21 days and at weaning. The level of lysine that resulted in the lowest sow backfat loss and the highest weaned piglet weight was 1.05%; this may be the optimum level of lysine for the diet of lactating Mong Cai sows. At this lysine level, the number of weaned piglets was also highest.

• The Journal of the Korea Contents Association
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• v.20 no.4
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• pp.99-110
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• 2020

Recently, as User Experience (UX) is considered as an important concept in the service design process of various fields, securing usability of Enterprise UX, UX developed for professional users, is acknowledged as an essential factor to increase work efficiency. The interface of Enterprise UX is complex and technically difficult for it is targeted for professional users. Thus, creating problems with complicated planning and relatively insufficient concerns regarding usability due to emphasis on development efficiency. It is necessary to consider various methods of usability, regarding further improvement is arduous in aspects of development and the cost. Therefore, this study aims to define the concept and specificity of Enterprise UX to improve usability and system effectively, and verify the main factors that reduce the usability of Enterprise UX. The evaluation of the research enterprise service, RDP (Research Data Platform), was conducted to establish and verify hypothesis. Furthermore, an independent evaluation standard for Enterprise UX is proposed after testing speculating factors that lower the usability of Enterprise UX. It is expected to utilize the Enterprise UX usability criteria defined through this study as a base data in enhancing usability and in designing Enterprise S/W.

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 2017.04a
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• pp.78-78
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• 2017

현재 국내에 공급되고 있는 잡곡류 수확기는 보행형 예취기, 탈곡기 위주의 저능률 기계화 수준으로 고능률의 콤바인 수확기 개발이 필요하며, 특히 잡곡류가 소규모 경작지의 영세농가 위주로 재배되어 저가격의 소형 콤바인 수확기 개발이 절실히 요구되고 있다. 따라서 본 연구는 소규모 밭의 두류 및 잡곡 수확작업에 적응성이 뛰어나며, 농기계 임대사업소의 활용도를 높일 수 있고, 여성과 고령자도 쉽게 운전할 수 있어 수확작업의 노동력을 크게 절감할 수 있는 저가격의 25kW급 자주식 소형 콤바인을 개발하고자 시작기를 설계 제작하였다. 시작기의 주요부로 엔진은 25kW/2600rpm 3기통 디젤엔진을 탑재하였으며, 동력전달부는 주변속 3단, 부변속 2단의 선택맞물림 기어식의 변속장치를 이용하였다. 주행부는 궤도형으로 조향클러치와 습식 원판식 제동장치를 채용하였다. 전처리부는 선단거리 1700 mm의 디바이더와 상하좌우 수동 조절되는 회전속도 약 42 rpm의 정오각형 릴로 구성하였으며, 전처리부의 최대 승강높이는 740 mm이었다. 작물이송부는 돌기부착 오거와 체인컨베이어로 구성되어 있으며, 탈곡부는 단동형 축류식의 직경 440 mm, 길이 1180 mm의 급동과 높이 65 mm, 지름 10 mm의 46개 강봉형 급치, 격자형 수망으로 구성하였으며, 회전속도는 약 325 rpm으로 작동하도록 하였다. 선별 정선부는 요동 송풍선별식으로 곡립판, 볏짚체, 곡립체, 송풍팬으로 구성하였고 송풍팬의 회전속도는 약 850 rpm, 요동진동수는 약 5.8 Hz로 작동하도록 하였다. 곡물이송부와 재처리부는 수평이송 외경 103 mm, 수직이송 외경 110 mm의 피치가 모두 82 mm인 스크류컨베이어를 이용하였으며, 곡물탱크는 용량이 250 로 2개의 배출구로 곡물을 포대에 담도록 하였다. 그 외 시작기는 운전조작부, 유압장치부, 전기장치부 등을 갖도록 설계 제작하였다. 전체적인 기체의 크기는 길이${\times}$폭${\times}$높이 $3935{\times}1900{\times}2440mm$이었으며, 기체 중량은 약 1753 kg이었다. 콩 대상 기초 성능시험 결과 시작기의 작업속도는 약 0.5 m/s, 작업능률은 약 11 a/h로 나타났다.

• Journal of Bio-Environment Control
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• v.6 no.3
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• pp.133-142
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• 1997

Most of the greenhouses employ the roll-up type ventilation control system. Torque required to roll-up and down might be theoretically expressed with the weight times radius of the ventilation roll; however, measured torques were two times of the theoretically estimated values. As the window film of roll-up vent is used over the periods of time, the warping and crumpling of the material caused the increase of the torque in addition to a span deformation. Therefore, this study was performed to develop an empirical torque formulae to present basic torque data and to assist the development of roll-up type ventilation control system. The empirically adjusted rolling radius (r＋a) exponentially increased at the maximum span deformation. The coefficient of rolling resistance (Cr) was about 0.7―0.8 depending upon the wrinkle status of film material.

• Journal of the Korean Institute of Telematics and Electronics
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• v.18 no.3
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• pp.42-51
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• 1981

Boron was predeposited into p (100) Si wafer at 94$0^{\circ}C$ for 60minutes to make the back surface field. High tempreature diffusion process at 1145$^{\circ}C$ for 3 hours was immediately followed without removing boron glass to obtain high surface concentration Back boron was annealed at 110$0^{\circ}C$ for 40minutes after boron glass was removed. N+ layer was formed by predepositing with POCI3 source at 90$0^{\circ}C$ for 7~15 minutes and annealed at 80$0^{\circ}C$ for 60min1es under dry Of ambient. The triple metal layers were made by evaporating Ti, Pd, Ag in that order onto front and back of diffused wafer to form the front grid and back electrode respectively. Silver was electroplated on front and back to increase the metal thickness form 1~2$\mu$m to 3~4$\mu$m and the metal electrodes are alloyed in N2 /H2 ambient at 55$0^{\circ}C$ and followed by silicon nitride antireflection film deposition process. Under artificial illumination of 100mW/$\textrm{cm}^2$ fabricated N+PP+ cells showed typically the open circuit voltage of 0.59V and short circuit current of 103 mA with fill factor of 0.80 from the whole cell area of 3.36$\textrm{cm}^2$. These numbers can be used to get the actual total area(active area) conversion efficiency of 14.4%(16.2%) which has been improved from the provious N+P cell with 11% total area efficiency by adding P+ back.

• Journal of the Mineralogical Society of Korea
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• v.14 no.2
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• pp.99-110
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• 2001

A gem-quality yttria-stabilized zirconium oxide crystals were synthesized by the skull-melting method, using the RF electrical apparatus. Principal raw materials used were $ZrO_2$and 25 wt.% $Y_2O_3$as stabilizer and 0.03~0.05 wt.% $Nd_2O_3$decolorizing agent were added to it. The single crystals were approximately 20$\times$63 mm in size with chemical composition $Zr_{0.73}$ $Y_{0.27}$ $O_{1.87}$ . The crystals are isotropic with no appreciable anisotropism under a polarizing microscope. Their refractive indices are in the range of 2.15~2.18, specific gravity 5.85, Mohs' hardness 8~8.5, and reflectivity 13.47%. The zirconia crystals were confirmed to have cubic structure with Face-centered lattice(Z=4), space group Fm3m ($CaF_2$-type structure) and unit cell parameters are a=5.157 $\AA$. The optimal growing conditions for yttria-stabilized zirconia are 50 kW, 2.94 MHz in power and to use a crucible with 105 mm $\times$ 135 mm in size. When the lowering speed of the crucible was set 16mm/hr gave the best yield, 42%. Since the refractive index(2.15~2.18) of cubic zirconia is smaller than that of diamond, the angle between crown and pavilion should be fashioned to make it smaller than $40.5^{\circ}$ to show the maximum brilliancy and fire.

• Proceedings of the Korean Vacuum Society Conference
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• 2000.02a
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• pp.108-108
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• 2000

급증하는 무선통신 정보수요는 특히, 고주파대역 (300NHz-300GHz)에서 사용되는 공진기, 필터, 발진기 등과 같은 소자의 품질향상을 요구하고 있다. 고주파용 유전체 중 ZrTiO4 는 $\alpha$-PbO2 계열의 사방정구조를 갖고 있는 유전체로서 높은 유전율 ($\varepsilon$=40)과 높은 품질계수 (Q=1/tan$\delta$=4700 at 7GHz)를 갖고 있고, Sn 첨가시 0ppm/$^{\circ}C$의 공진주파수 온도계수를 얻을 수 있다고 보고되어 있다. 본 연구에서는 약 110$0^{\circ}C$ 이상에서 안정한 상으로 존재하는 ZrTiO4를 저온에서 증착하여 준안정한 상태로 결정화되게 한후, 유전손실 (tan$\delta$)과 유전율($\varepsilon$)을 측정하였다. 또한 증착온도와 열처리과정에 따른 박막의 us형 (Strain) 정도의 변화를 X-선 회절결과로부터 분석하였으며 이를 측정된 유전특성 값과 비교하였다. ZrTiO4 박막은 DC magnetron reactive sputter로 Zr과 Ti 타겟으로부터 high phosphorous doped Si (100) 기판위에 증착하였다. 압력은 4mTorr로 유지하고 박막의 화학양론적 조성비를 맞추기 위해 각 타겟에 가해지는 power는 Zr/Ti=500W/650W로 고정하고, 반응가스의 비율을 Ar/O2=17sccm/3.5sccm으로 유지하여 박막내에 인입되는 산소량을 제어하였다. 증착 직후와 열처리 후의 박막특성을 비교하기 위해 증착온도를 상온에서부터 $600^{\circ}C$까지 변호시키고 증착후 각각의 시편을 80$0^{\circ}C$ 산소분위기에서 2시간동안 열처리하여 시편을 준비하였다. 박막의 상형성 여부와 결정성변화는 $ heta$-2$\theta$X-선 회절법을 사용하여 조사하였고, EPMA를 이용하여 박막의 조성을 확인하였다. 유전특성의 측정을 위해 백금 상부전극을 증착한 후, impedance analyzer를 이용하여 100kHz 영역에서의 유전손실을 측정하고, 측정된 정전용량과 박막의 두께로부터 유전율을 계산하였다. ZrTiO4 박막은 증착온도 20$0^{\circ}C$ 이상에서 결정성을 보이기 시작했으며, 열처리 이후에는 상온에서 비정질이었던 시편이 $650^{\circ}C$ 이상의 온도에서 결정화되기 시작하였다. 증착온도에 따라 유전손실은 0.038에서 0.017 정도로 감소하는 경향을 나타냈으며, 각각 열처리에 의해서 0.034, 0.005 정도로 다시 감소하였다. 박막의 유전율은 약 35 정도의 값을 나타내었으며 X-선 회절 data로부터 분석한 박막의 변형은 증온도에 따라 7.2%에서 0.04%로 감소하였고 이 이경향은 유전손실은 감소경향과 일치하였다.