• Title/Summary/Keyword: Volume fraction of martensite

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Effect of Microstructure on Dynamic Tensile Characteristics of SPRC440 Sheet (SPRC440 강판재의 미세조직 구성이 동적 인장 특성에 미치는 영향)

  • Lee, S.H.;Rhyim, Y.M.;Lee, J.H.;Kim, I.B.;Kim, Y.D.
    • Transactions of Materials Processing
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    • v.20 no.4
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    • pp.309-315
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    • 2011
  • The behavior of metallic materials at high strain rates shows different characteristics from those in quasi-static deformation. Therefore, the strain rate should be considered when simulating crash events. The objective of this paper is to evaluate the dynamic tensile characteristics of SPRC440 as a function of the volume fraction of phases. As-received SPRC440 is composed of ferrite and pearlite phases. However, ferrite and martensite phases were observed after heat treatment at $730^{\circ}C$ and $780^{\circ}C$ for 5 minutes, as expected by calculations based on the curves from dilatometry tests. High cross-head speed tensile tests were performed to acquire strain-stress curves at various strain rates ranging from 0.001 to $300\;s^{-1}$, which are typical in real vehicle crashes. It was observed that the flow stress increases with the strain rate and this trend was more pronounced in the as-received specimens consisting of ferrite and pearlite phases. It is speculated that the dislocation density in each phase has an influence on the strain rate sensitivity.

The Effects of δ-ferrite on Weldment of 9-12% Cr Steels (9-12% Cr강의 용접부에 미치는 δ-ferrite의 영향)

  • Ahn, Sung-Yong;Kang, Namhyun
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.8-16
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    • 2013
  • As the energy consumption increases rapidly, power generation needs the high energy efficiency continuously. To achieve the high efficiency of power generation, the materials used have to endure the higher temperature and pressure. The 9-12%Cr steels possess good mechanical properties, corrosion resistance, and creep strength in high temperature due to high Cr contents. Therefore, the 9-12%Cr steels are widely used for the high-temperature components in power plants. Even though the steels usually have a fully martensitic microstructure, they are susceptible to the formation of ${\delta}$-ferrite specifically during the welding process. The formation of ${\delta}$-ferrite has several detrimental effects on creep, ductility and toughness. Therefore, it is necessary to avoid its formation. As the volume fraction of ${\delta}$-ferrite is less than 2% in microstructure, it has the isolated island morphology and causes no significant degradation on mechanical properties. For ${\delta}$-ferrite above 2%, it has a polygonal shape affecting the detrimental influence on the mechanical properties. The formation of ${\delta}$-ferrite is affected by two factors: a chemical composition and a welding heat input. The most effective ways to get a fully martensite microstructure are to reduce the chromium equivalent less than 13.5, to keep the difference between the chromium and nickel equivalent less than 8, and to reduce the welding heat input.

Correlation Between M-A Constituents and Tensile Properties in the Intercritical Coarse Grained HAZ of an Ultra Low Carbon Steel (극 저탄소강의 Intercritical coarse grained HAZ에서의 M-A상과 인장특성 간의 상관관계)

  • Lee, Yoon-Ki;Moon, Joon-Oh;Kim, Sang-Hoon;Lee, Chang-Hee
    • Journal of Welding and Joining
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    • v.28 no.3
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    • pp.99-103
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    • 2010
  • It is well known that martensite-austenite (M-A) constituents are formed in the intercritically reheated coarse grained heat affected zone (ICCGHAZ) of a multipass weld and they act on the local brittle zone (LBZ) in the welded structures. To investigate the effect of M-A constituents on the tensile properties of ICCGHAZ, specimens with M-A constituents of different volume fraction and size were prepared through the multipass welding cycles simulated by a Gleeble simulator and then tensile test was carried out. The results indicated that finely distributed M-A constituents contributed to decrease the yield ratio, which is mainly due to the increased tensile strength.

Changes in Microstructure and Texture during Annealing of 0.015% C-1.5% Mn-0~0.5% Mo Steels (0.015% C-1.5% Mn-0~0.5% Mo 강의 어닐링과정에서 미세조직과 집합조직의 변화)

  • Jeong, Woo Chang
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.5
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    • pp.251-261
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    • 2011
  • The changes in microstructure and texture during annealing were examined in a series of 0.015% C-1.5% Mn cold-rolled sheet steels with 0~0.5% Mo. Orientation distribution function data were calculated from the (110), (200), (211) pole figures determined on the rolled plane of cold-rolled and annealed steel sheets. Regardless of Mo content and annealing conditions, martensite volume fraction was less than 1.0%, not affecting the texture evolution. Textural change at the cooling stage after heating at $820^{\circ}C$ for 67 sec was not observed. Increasing the Mo content and annealing temperature markedly strengthened the intensities of ${\gamma}$-fiber texture, resulting in the increase in $r_m$ value. The desirable texture evolution for deep drawability in the 0.5% Mo steel may be mainly caused by the grain refining effect of Mo carbide in the hot-rolled steel sheet.

Effect of Effective Grain Size on Charpy Impact Properties of High-Strength Bainitic Steels (베이나이트계 고강도강의 샤르피 충격 특성에 미치는 유효결정립도 영향)

  • Shin, Sang Yong;Han, Seung Youb;Hwang, Byoungchul;Lee, Chang Gil;Lee, Sunghak
    • Korean Journal of Metals and Materials
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    • v.46 no.10
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    • pp.617-626
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    • 2008
  • This study is concerned with the effect of Cu and B addition on microstructure and mechanical properties of high-strength bainitic steels. Six kinds of steels were fabricated by varying alloying elements and hot-rolling conditions, and their microstructures and tensile and Charpy impact properties were investigated. Their effective grain sizes were also characterized by the electron back-scatter diffraction analysis. The tensile test results indicated that the B- or Cu-containing steels had the higher yield and tensile strengths than the B- or Cu-free steels because their volume fractions of bainitic ferrite and martensite were quite high. The B- or Cu-free steels had the higher upper shelf energy than the B- or Cu-containing steels because of their higher volume fraction of granular bainite. In the steel containing 10 ppm B without Cu, the best combination of high strengths, high upper shelf energy, and low energy transition temperature could be obtained by the decrease in the overall effective grain size due to the presence of bainitic ferrite having smaller effective grain size.

Effect of Quenching Heat-treatment on Mechanical Properties and Microstructure of Modified C95600 Bronze (개량형 C95600 청동의 기계적 성질과 미세조직에 미치는 퀜칭 열처리의 영향)

  • Lee, Sung-Yul;Moon, Kyung-Man;Oh, Jae-Hwan;Shin, Dong-Il
    • Journal of Ocean Engineering and Technology
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    • v.25 no.6
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    • pp.97-104
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    • 2011
  • Modified C95600 bronze contains Fe component of 0.7 weight percentage besides Cu-7Al-2.5Si composition. The shape of centrifugal cast is a circular pipe with thick wall. Specimens machined from the centrifugal cast were quenched in oil after isothermal holding at a given heat treatment temperature in the range of $700{\sim}900^{\circ}C$. Mechanical properties and structural morphology are depended on the quenching heat treatment temperature regardless of isothermal holding time. Tensile strength or Brinell hardness is increased with increasing heat treatment temperature. The microstructure caused by quenching contains mixing phases of ${\alpha}+{\beta}'+FeSi+{\kappa}$ which martensite of ${\beta}'$ phase has been transformed from ${\beta}$ phase. Effect of isothermal holding temperature on mechanical properties in case of quenching heat treatment attributes to the change of volume fraction of ${\beta}'$ on the structural morphology. Mechanical characteristics of specimen, initially quenched from $850^{\circ}C$, and then tempered at $500^{\circ}C$, does not show an obvious softening indication, because disappearance of ${\beta}'$ during tempering process can be compensated by precipitation of brittle phase ${\gamma}$.

Analysis of Correlation between the Hydrogen Embrittlement and the Small Punch Test for Hydrogen-charged Dual Phase Steels (수소주입시킨 DP박강판의 SP시험과 수소취성 관계 해석)

  • Park, Jae-Woo;Kang, Kae-Myung
    • Journal of the Korean Institute of Gas
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    • v.18 no.1
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    • pp.61-67
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    • 2014
  • Small punch(SP) tests were performed on high strength Dual Phase(DP) steels in order to evaluate the behavior of hydrogen embrittlement. For this purpose, three different kinds of DP steel specimens were charged with hydrogen by electochemical hydrogen charging experiment. After charging with hydrogen, the amount of charged hydrogen was measured. The measurement results showed that amounts of charged hydrogen were largely dependent on the martensite volume fraction of DP steel. The hydrogen charging time of 25 hrs with current densities of 150 and $200mA/cm^2$ was investigated as saturation condition with hydrogen. The analysis results on the SP energy and height of SP bulbs after SP tests showed that those were decreased as the amount of charged hydrogen increased. Fractographs of SP bulbs were observed a brittle fracture mixed with quasi-cleavage fractures, layered structures and clear facets.

Formation of Nano-structure and Compressive Residual Stress on AISI304 Stainless Steel by Ultrasonic Nanocrystalline Surface Modification (초음파 나노표면개질 공정기술에 의한 AISI304 스테인리스강의 표면나노구조화 및 압축잔류응력 형성)

  • Cho, In-Shik;Dong, Ji-Ling;Yoo, Dae-Hwang;Suh, Jung-Hwa;Amanov, Auezhan;Shin, Kee-Sam;Lee, Chang-Soon;Pyoun, Young-Shik;Park, In-Gyu
    • Korean Journal of Metals and Materials
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    • v.48 no.9
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    • pp.807-812
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    • 2010
  • In this paper, the Ultrasonic Nanocrystalline Surface Modification (UNSM) surface treatment process was used to induce compressive residual stress and nanocrystalline structure by severe plastic deformation on the UNSM-treated surface. The test results for AISI304 stainless steel demonstrated that the grain size was found to be 23 nm, the dislocation density was increased by $0.2085{\times}10^{18}\;m^{-2}$, and the volume fraction of martensite is defined as 27.6% from austenite so that the surface hardness of the surface is increased from 200 Hv up to 515 Hv. The initial tensile residual stress is changed from 300 MPa to a compressive residual stress of 500 MPa after UNSM treatment. In addition, UNSM was applied under five various conditions, and the results of those conditions were defined as a function of depth quantitative.

The Effect of Grain Size and Cooling Rate on Phase Transformation for Mechanically Alloyed Ni-36at.%Al Alloy (기계적 합금화된 Ni-36at.%Al 합금의 상변태에 미치는 결정립 크기 및 냉각속도의 영향)

  • Kim, Seong-Uk;Kim, Dae-Geon;Kim, Ji-Sun;An, In-Seop;Kim, Yeong-Do
    • Korean Journal of Materials Research
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    • v.10 no.9
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    • pp.642-647
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    • 2000
  • Nanocrystalline NiAl alloy containing 36at.%Al was synthesized by mechanical alloying (MA). Synthesized powder was sintered by a pulse electric current sintering (PECS) facility. Effecting parameters on the phase transformation were discussed in terms of cooling rate and time spent on heat treatment. The behavior of phase transformation for sintered parts was examined by differential scanning calorimetry (DSC) and X-ray diffraction (XRD) method. Microstructure was observed by scanning electron microscopy (SEM). Martensitic lattice parameter and volume fraction was calculated by direct comparison method in X-ray diffraction analysis.

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Effect of post heat treatment on fatigue properties of EBM 3D-printed Ti-6Al-4V alloy (분말 3D 프린팅된 Ti-6Al-4V 합금의 피로특성에 미치는 후열처리의 영향)

  • Choi, Young-Sin;Jang, Ji-Hoon;Kim, Gun-Hee;Lee, Chang-Woo;Kim, Hwi-Jun;Lee, Dong-Geun
    • Journal of Powder Materials
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    • v.25 no.4
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    • pp.340-345
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    • 2018
  • Additive manufacturing by electron beam melting is an affordable process for fabricating near net shaped parts of titanium and its alloys. 3D additive-manufactured parts have various kinds of voids, lack of fusion, etc., and they may affect crack initiation and propagation. Post process is necessary to eliminate or minimize these defects. Hot isostatic pressing (HIP) is the main method, which is expensive. The objective of this paper is to achieve an optimum and simple post heat treatment process without the HIP process. Various post heat treatments are conducted for the 3D-printed Ti-6Al-4V specimen below and above the beta transus temperature ($996^{\circ}C$). The as-fabricated EBM Ti-6Al-4V alloy has an ${\alpha}^{\prime}$-martensite structure and transforms into the ${\alpha}+{\beta}$ duplex phase during the post heat treatment. The fatigue strength of the as-fabricated specimen is 400 MPa. The post heat treatment at $1000^{\circ}C/30min/AC$ increases the fatigue strength to 420 MPa. By post heat treatment, the interior pore size and the pore volume fraction are reduced and this can increase the fatigue limit.