• 제목/요약/키워드: Volume Fraction Ratio

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The Characteristics of Microstructure and the Mechanical Properties of Multi-Phase Sheet Steel. (다상조직강의 기계적 성질과 조직특성)

  • Park, Jong-Hyeon;Gang, Gye-Myeong;Song, Jin-Tae
    • Korean Journal of Materials Research
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    • v.1 no.3
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    • pp.115-124
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    • 1991
  • In this study, the relationship between mechanical properties and the effects of second phase in tri-phase steel which was composed of ferrite-martensite-bainite was investigated. In order to obtain different microstructure of ferrite+martensite(DP), ferrite+bainite(F+B), and ferrite+martensite+bainite(TP, different heat treatment has been accomplished. The effects of volume fraction and microstructure of each specimen were studied on tensile property, Charpy impact energy and stretch-flangeability. As the bainite content in triphase steels increased, the tensile strength, and yield strength decreased as well as the reduction of area and strength-uniform elongation increased. However, ferrite-bainite steel had high yield ratio and yield point elongation. The Charpy impact energy of TP and F+B steel was higher than that of DP steel. In addition, the characteristics of hole expanding limit($\lambda$) of TP steel and F+B steel were higher than that of DP steel. These mechanical properties of tri-phase steel have been improved, because bainite could be deformed easily within ferrite matrix. The effect of bainite on ductility in tri-phase steel has been found to be favorable. In this experiment, tri-phase steel contained within 27% bainite volume fraction had good nechanical properties and superior stretch-flangeability.

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Generation of Charged Clusters and their Deposition in Polycrystalline Silicon Hot-Wire Chemical Vapor Deposition (열선 CVD 증착 다결정 실리콘에서 전하를 띈 클러스터의 생성 및 증착)

  • Lee, Jae-Ik;Kim, Jin-Yong;Kim, Do-Hyeon;Hwang, Nong-Moon
    • 한국신재생에너지학회:학술대회논문집
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    • 2005.11a
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    • pp.561-566
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    • 2005
  • Polycrystalline silicon films were deposited using hot wire CVD (HWCVD). The deposition of silicon thin films was approached by the theory of charged clusters (TCC). The TCC states that thin films grow by self-assembly of charged clusters or nanoparticles that have nucleated in the gas phase during the normal thin film process. Negatively charged clusters of a few nanometer in size were captured on a transmission electron microscopy (TEM) grid and observed by TEM. The negatively charged clusters are believed to have been generated by ion-induced nucleation on negative ions, which are produced by negative surface ionization on a tungsten hot wire. The electric current on the substrate carried by the negatively charged clusters during deposition was measured to be approximately $-2{\mu}A/cm^2$. Silicon thin films were deposited at different $SiH_4$ and $H_2$ gas mixtures and filament temperatures. The crystalline volume fraction, grain size and the growth rate of the films were measured by Raman spectroscopy, X-ray diffraction and scanning electron microscopy. The deposit ion behavior of the si1icon thin films was related to properties of the charged clusters, which were in turn controlled by the process conditions. In order to verify the effect of the charged clusters on the growth behavior, three different electric biases of -200 V, 0 V and +25 V were applied to the substrate during the process, The deposition rate at an applied bias of +25 V was greater than that at 0 V and -200 V, which means that the si1icon film deposition was the result of the deposit ion of charged clusters generated in the gas phase. The working pressures had a large effect on the growth rate dependency on the bias appled to the substrate, which indicates that pressure affects the charging ratio of neutral to negatively charged clusters. These results suggest that polycrystalline silicon thin films with high crystalline volume fraction and large grain size can be produced by control1ing the behavior of the charged clusters generated in the gas phase of a normal HWCVD reactor.

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Effect of boron milling on phase formation and critical current density of MgB2 bulk superconductors

  • Kang, M.O.;Joo, J.;Jun, B.H.;Park, S.D.;Kim, C.S.;Kim, C.J.
    • Progress in Superconductivity and Cryogenics
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    • v.21 no.1
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    • pp.18-24
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    • 2019
  • This study was carried out to investigate the effect of milling of boron (B), which is one of raw materials of $MgB_2$, on the critical current density ($J_c$) of $MgB_2$. B powder used in this study is semi-amorphous B (Pavezyum, Turkey, 97% purity, 1 micron). The size of B powder was reduced by planetary milling using $ZrO_2$ balls (a diameter of 2 mm). The B powder and balls with a ratio of 1:20 were charged in a ceramic jar and then the jar was filled with toluene. The milling time was varied from 0 to 8 h. The milled B powders were mixed with Mg powder in the composition of (Mg+2B), and the powder mixtures were uniaxially pressed at 3 tons. The powder compacts were heat-treated at $700^{\circ}C$ for 1 h in flowing argon gas. Powder X-ray diffraction and FWHM (Full width at half maximum) were used to analyze the phase formation and crystallinity of $MgB_2$. The superconducting transition temperature ($T_c$) and $J_c$ of $MgB_2$ were measured using a magnetic property measurement system (MPMS). It was found that $B_2O_3$ was formed by B milling and the subsequent drying process, and the volume fraction of $B_2O_3$ increased as milling time increased. The $T_c$ of $MgB_2$ decreased with increasing milling time, which was explained in terms of the decreased volume fraction of $MgB_2$, the line broadening of $MgB_2$ peaks and the formation of $B_2O_3$. The $J_c$ at 5 K increased with increasing milling time. The $J_c$ increase is more remarkable at the magnetic field higher than 3 T. The $J_c$ at 5 K and 4 T was the highest as $4.37{\times}10^4A/cm^2$ when milling time was 2 h. The $J_c$ at 20 K also increased with increasing milling time. However, The $J_c$ of the samples with the prolonged milling for 6 and 8 h were lower than that of the non-milled sample.

An Experimental Study on the Mechanical Properties and Long-Term Deformations of High-Strength Steel Fiber Reinforced Concrete (고강도 강섬유보강 콘크리트의 역학적 특성 및 장기변형 특성에 관한 실험적 연구)

  • Yoon, Eui-Sik;Park, Seung-Bum
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.2A
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    • pp.401-409
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    • 2006
  • This study presents basic information on the mechanical properties and long-term deformations of high-strength steel fiber reinforced concrete(HSFRC). The Influence of steel fiber on modulus of elasticity, compressive, splitting tensile and flexural strength, and drying shrinkage and creep of HSFRC are investigated, and flexural fracture toughness is evaluated. Test results show that Test results show that the effect of steel fibers on the compressive strength is negligible, and the modulus of elasticity of HSFRC increased with the increase of fiber volume fraction. And the effect of fiber volume fraction($V_f$) and aspect ratio($l_f/d_f$) on tensile strength, flexural strength and toughness is extremely prominent. It is observed that the flexural deflection corresponded to ultimate load increased with the increase of $V_f$ and $l_f/d_f$, and due to fiber arresting cracking, the shape of the descending branch of load-deflection tends towards gently. Also, the effect of addition of various amounts of fiber on the creep and shrinkage is obvious. Especially, the effect of adding fibers to high-strength concrete is more pronounced in reducing the drying shrinkage than the creep.

Biochemical Changes of Liver Function in Patients with Hepatocellular Carcinoma Following Radiotherapy and Hyperthermia (진행된 원발성 간암 환자에서 방사선 치료 및 온열 요법에 따른 간 기능의 변화)

  • Oh Young Taek;Seong Jinsil;Shin Hyun Soo;Kim Gwi Eon
    • Radiation Oncology Journal
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    • v.11 no.1
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    • pp.109-117
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    • 1993
  • To analyze biochemical changes of liver function following combined radiotherapy and hyperthermia, we reviewed retrospectively 37 patients with hepatocellular carcinoma treated with radiotherapy and hyperthermia between July 1988 and December 1990 at Department of Radiation Oncology, Yonsei University College of Medicine. Mean age was 52.7 years and male to female ratio was 11:1. The patients were classified as follows; to A and B group by Child's classification, to M and L group by irradiated volume, and subclassified into BM, BL, AM and AL group according to the combination of Child's classification and irradiated volume. Radiation dose to the primary tumor was 3060 cGy with daily 180 cGy, 5 fraction per week using 10 MV or 4 MV linear accelerator. Hyperthermia (Thermotron RF-8) was performed more than 4 times in all patients. Biochemical parameters including albumin (Alb), total bilirubin (T. Bil), aspartate aminotransferase (AST or SGOT), alanine aminotransferase (ALT or SGPT), and alkaline phosphatase (ALP) were regularly followed from 1 week before the treatment to 3 months after the treatment. The results are summerized as follows; 1) In all the patient, mean ALP level peaked at 1 month, decreased at 2 months, slightly increased at 3 months after the treatment. Mean SGOT and SGPT levels peaked at 1 month after the treatment. Mean T. Bil level increased continuously and highest at 3 months after the treatment. Mean Alb level did not show significant changes.; 2) Mean ALP level retured to normal level at 3 month after the treatment in A but increased in B group and the differences were statistically significant (p<0.01). Mean SGOT and SGPT levels peaked 1 month in A and 2 months after the treatment in B group. All the biochemical parameters did not show significant difference between M and L group. Mean ALP level increased at 3 months after the treatment in BM and BL groups and decreased in AM and AL groups. Mean SGOT level increased at 3 months after the treatment in BL groups.; 3) Hepatic failure occurred within 3 months after the treatment in 4 patients, all of whom were in BL group. It is suggested that pre-treatment liver function and irradiated volume influence biochemical changes of liver in patients with hepatocellular carcinoma following combined radiotherapy and hyperthermia, and this treatment modality appears generally to be safe but might cause hepatic failure particularly in patient with poor liver function and large treatment volume.

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The Effect of Fe and Fe2O3 Powder Mixing Ratios on the Pore Properties of Fe Foam Fabricated by a Slurry Coating Process (슬러리 코팅 공정으로 제조된 Fe 폼의 기공 특성에 미치는 Fe 및 Fe2O3 분말의 혼합 비율의 영향)

  • Choi, Jin Ho;Jeong, Eun-Mi;Park, Dahee;Yang, Sangsun;Hahn, Yoo-Dong;Yun, Jung-Yeul
    • Journal of Powder Materials
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    • v.21 no.4
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    • pp.266-270
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    • 2014
  • Metal foams have a cellular structure consisting of a solid metal containing a large volume fraction of pores. In particular, open, penetrating pores are necessary for industrial applications such as in high temperature filters and as a support for catalysts. In this study, Fe foam with above 90% porosity and 2 millimeter pore size was successfully fabricated by a slurry coating process and the pore properties were characterized. The Fe and $Fe_2O_3$ powder mixing ratios were controlled to produce Fe foams with different pore size and porosity. First, the slurry was prepared by uniform mixing with powders, distilled water and polyvinyl alcohol(PVA). After slurry coating on the polyurethane(PU) foam, the sample was dried at $80^{\circ}C$. The PVA and PU foams were then removed by heating at $700^{\circ}C$ for 3 hours. The debinded samples were subsequently sintered at $1250^{\circ}C$ with a holding time of 3 hours under hydrogen atmosphere. The three dimensional geometries of the obtained Fe foams with an open cell structure were investigated using X-ray micro CT(computed tomography) as well as the pore morphology, size and phase. The coated amount of slurry on the PU foam were increased with $Fe_2O_3$ mixing powder ratio but the shrinkage and porosity of Fe foams were decreased with $Fe_2O_3$ mixing powder ratio.

Investigation on the Flexural and Shear Behavior of Fiber Reinforced UHSC Members Reinforced with Stirrups (전단철근과 강섬유로 보강된 초고강도 콘크리트 부재의 휨 및 전단 거동에 관한 연구)

  • Yuh, Ok-Kyung;Ji, Kyu-Hyun;Bae, Baek-Il
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.7
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    • pp.152-163
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    • 2019
  • In this paper, effect of steel fiber inclusion, compressive strength of matrix, shear reinforcement and shear span to depth ratio on the flexural behavior of UHPFRC(Ultra High Performance Fiber Reinforced Concrete) were investigated with test of 10-UHPFRC beam specimens. All test specimens were subjected to the flexural static loading. It was shown that steel fiber significantly improve the shear strength of UHPFRC beams. 2% volume fraction of steel fiber change the mode of failure from shear failure to flexural failure and delayed the failure of compressive strut with comparatively short shear span to depth ratio. UHPFRC beams without steel fiber had a 45-degree crack angle and fiber reinforced one had lower crack angle. Shear reinforcement contribution on shear strength of beams can be calculated by 45-degree truss model with acceptable conservatism. Using test results, French and Korean UHPFRC design recommendations were evaluated. French recommendation have shown conservative results on flexural behavior but Korean recommendation have shown overestimation for flexural strength. Both recommendations have shown the conservatism on the flexural ductility and shear strength either.

Synthetic Conditions and Rheological Characteristics of Barium Sulfate (황산바륨의 합성조건과 유동학적 특성)

  • Shin, Wha-Woo;Kim, Jun-Hea;Choi, Kwang-Sik;Chang, Young-Soo;Lee, Kwang-Pyo
    • YAKHAK HOEJI
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    • v.36 no.6
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    • pp.538-547
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    • 1992
  • Optimal synthetic condition of barium sulfate were investigated from the viewpoint of yield and bulkiness according to a randomized complete block design proposed by G.E.P. Box and K.B. Wilson. Barium chloride and magnesium sulfate were utilized as reactants in order to prepare barium sulfate in this study. It was found that optimum temperature range of reactant solutions was $60{\sim}100^{\circ}C$ and the optimum concentration range of the reactant solutions was $10{\sim}17.3%$ and $10{\sim}20%$ respectively, on the viewpoint of yield and bulkiness. The optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum mole ratio of $BaCI_2$ to $BaSO_4$ was in the range of $1.50{\sim}2.0$ and the optimum reacting time range was $15{\sim}20$ minutes. The optimum drying temperature range was $110{\sim}130^{\circ}C$ from the viewpoint of yield, but it was $90{\sim}110^{\circ}C$ on the basis of bulkiness. Apparent viscosity of barium sulfate suspensions dispersed in various concentrations of Na. CMC was measured by using Brookfield synchrolectric viscometer model LVT, the relative equation, log ${\eta}_{sp}=A+B.{\phi}$ was examined and the equation was found to agree fairly well. 1 w/v% Na. CMC aqueous solution and 0.1 volume fraction of $BaSO_4$ powder were optimum in the preparation of $BaSO_4$ suspension showing highest viscosity at infinite shearing.

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A Novel Frequency Selective Surface: Frequency Selective Fabric Composite (새로운 주파수 선택 표면: 주파수 선택적인 직물 복합 재료)

  • Lee, Sang-Eui;Kim, Chun-Gon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.17 no.10 s.113
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    • pp.920-928
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    • 2006
  • Fiber-reinforced composites transmitting microwaves of certain frequencies or bands were proposed. These frequency selective fabric composites(FSFCs) are fabricated by weaving carbon fibers and dielectric fibers that build periodic patterns. Design parameters affecting the electromagnetic characteristics of FSFCs were widely discussed, Then the electromagnetic characteristics of a fabricated plain-weave FSEC were investigated with regard to the electrical conductivities of carbon roving, the fiber undulation, and the aperture-to-cell ratio, for the electrical conductivities, its dependence on frequency as well as on the fiber volume fraction of carbon roving was taken into account. Constituent material properties and the fiber undulation had little effect on the EM properties of the fabricated FSFC, while the aperture-to-cell ratio made a profound effect on them.

A Study on Prediction of Effective Material Properties of Composites with Fillers of Different Sizes and Arrangements (강화재의 크기 및 배치에 따른 복합재의 등가 물성치 예측에 대한 연구)

  • Lee, J. K.;Kim, J. G.
    • Composites Research
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    • v.18 no.5
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    • pp.21-26
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    • 2005
  • The validity of Eshelby-type model with Mori-Tanaka's mean field theory to predict the effective material properties of composites have been investigated in terms of filler size and its arrangement. The 2-dimensional plate composites including constant volume fraction of fillers are used as the model composite for the analytical studies, where the filler size and its arrangement are considered as parameters. The exact effective material properties of the composites are computed by finite element analysis(FEA), which are compared with effective material properties from the Eshelby-type model. Although the fillers are periodically or randomly arranged, the average Young's moduli by Eshelby-type model and FEA are in good agreement, specially for the ratio of specimen size to filler size being smaller than 0.03. However, Poisson's ratio of the composite by the Eshelby-type model is overestimated by $20\%$.