• Journal of Advanced Marine Engineering and Technology
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• v.25 no.6
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• pp.1341-1352
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• 2001

Vacuum freeze drying process by which frozen water in a drying material is removed sublimation under vacuum condition, is now applied to various industrial field such as the manufacturing and packaging of pharmaceuticals in pharmaceutical industry, the drying of bio- products in bio-technology industry, the treatment of various quality food stuff in food technology, and so on. The Knowledge about the heat and mass transfer characteristics related with the vacuum freeze drying process is crucial to improve the efficiency of the process as well as the quality of dried products. In spite of increasing needs for understanding of the process, the research efforts in this fields are still insufficient. In this paper, a numerical code that can predict primary drying in a vial is developed based on the finite volume method with a moving grid system. The calculation program can handle the axis- symmetric and multi-dimensional characteristics of heat and mass transfer of the vial freeze drying process. To demonstrated the usefulness of the present analysis, a practical freeze drying of skim Milk solution in a vial is simulated and various calculation results are presented.

• Journal of the Korean Wood Science and Technology
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• v.41 no.5
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• pp.456-465
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• 2013

Log cross sections of yellow poplar were dried in a radio frequency vacuum (RFV) dryer under alternating vacuum and release (AVR) process. The average moisture content (MC), temperature and vapor pressure at the volumetric center were monitored as functions of time. Three different log thicknesses (33, 60 and 75mm) were tested. The results show that the AVR process caused an increase in the drying rate when the moisture content was above fiber saturation point (FSP, about 30% MC) but that it had an inverse effect on the drying rate when the MC was below FSP. The effect of the AVR process on the drying rate decreased, and the severity of heart checks increased, with the increase in the thickness of the specimens.

• Journal of the Korean Applied Science and Technology
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• v.33 no.1
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• pp.58-66
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• 2016

This study was performed to investigate drying characteristics and quality properties of dried persimmon with vacuum drying process. Drying characteristic curve of the dried persimmon showed that the constant rate drying period and falling rate drying period exist definitely. $_{\circ}Brix$, sugar content and hardness value of the dried persimmon increased as the vacuum pressure and heating temperature increased, but L value of the dried persimmon lower. The results indicated that the optimal conditions were at vacuum pressure of 40~50kPa abs., heating temperature of $30^{\circ}C$ and drying time of 3~4days.

• Journal of the Korean Wood Science and Technology
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• v.30 no.2
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• pp.108-114
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• 2002

Red pine(Pinus densiflora) square timbers with 14.0 cm and 16.5 cm of face size and 24 m long were dried in a vacuum-press kiln and in a radio-frequency/vacuum(RF/V) kiln to compare drying rate, moisture content(MC) distribution and specific energy. RF/V drying rate was higher than vacuum-press drying rate. The effect of size of cross section on the RF/V drying rates were more pronounced than those of vacuum-press drying. The longitudinal- and the transverse MC distribution of dried square timber showed convex profile for the vacuum-press drying and concave profile for the RF/V drying. Moisture gradient of width direction was similar to the thickness direction in vacuum-press dried square timber and was more slight than that of the thickness direction in the RF/V dried large square timber. The specific energy consumption curve increased as MC decreased. Specific energy(kWh/kg of water evaporated) of the vacuum-press process required more than that of the RF/V process.

• Journal of Advanced Marine Engineering and Technology
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• v.26 no.2
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• pp.226-232
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• 2002

In tradition, there have been two kinds of drying methods, which are sun drying and artificial drying. The sun drying method which has been adopted traditionally has been replaced by the hot-air drying method which is one of the most general methods of artificial drying, with its simple drying system, low initial cost of drying plant, and easy operating method. But the hot-air drying method has some defects ; (1)much energy loss happens due to the discharge of hot air during the drying process, (2)control of drying rate is not easy on account of changing relative humidity of inlet air for uniform hot air temperature, (3)high temperature of floods in drying process brings about the production of low-grade drying products. Also, the hot-air drying method is inducing environmental and sanitary problems which are resulting from the emission of high temperature and high humidity air, including stick on the drying progress. Vacuum drying technique, whose drying time and 7uantity of exhausting energy is about 1/3 ~1/4 of hot air drying, is very excellent in the drying efficiency. As the results, it took about 20 hours for material to reach about 18% of the final moisture content in order to store products for a long time, from about 470% of the early moisture content at the beginning of drying, and maximum drying rate comes to about $0.35 kg/m^2hr$ at about 350% of the moisture content.

• Journal of Power System Engineering
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• v.5 no.1
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• pp.44-49
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• 2001

Low temperature vacuum drying technique shows very excellent energy efficiency and prominent drying performances compared with the conventional hot air drying technique. This study was focused on the thermal characteristics of the low temperature vacuum drying technique. From the results of this study, it was confirmed that the time consumption for drying with the new drying technique could be shortened to about 1/3 of the time consumption with the conventional hot air drying technique under the same drying conditions for wet products. Also, the maximum drying rate with the new drying technique reached to about $0.35kg/m^2h$ at about 400% of moisture content.

• Journal of Advanced Marine Engineering and Technology
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• v.24 no.4
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• pp.427-434
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• 2000

In tradition, there have been two kinds of drying methods, which are sun drying and artificial drying. The sun drying method which has been adopted traditionally has been replaced by the hot-air drying method which is one of the most general methods of artificial drying, with its simple drying system, low initial cost of drying plant, and easy operating method. But the hot-air drying method has some defects; (1) much energy loss happens due to the discharge of hot air during the drying process, (2) control of drying rate is not easy on account of changing relative humidity of inlet air for uniform hot air temperature, (3) high temperature of foods in drying process brings about the production of low-grade drying products. Vacuum drying takes advantage of energy saving and mass production because it reduces the drying time by increasing the drying rate under low temperature condition. The aim of this paper is to develop the low temperature vacum dryer, with low initial investments and operating costs, easy operating method and trouble-free operation.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.28 no.5
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• pp.208-215
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• 2016

This study was conducted to improve the performance of low-temperature vacuum dryer by applying desiccant to cold trap. Performance evaluation was carried out using several desiccants. The amounts of absorption and diffusivity were measured based on analytic model. Results of desiccant performance evaluation revealed that silica-gel had the most excellent performance for conditions of low-temperature vacuum drying process. Silica-gel was applied to cold trap for evaluating the drying performance. The experiment results showed that the drying time was extended as the thickness of sample was increased due to increased heat and mass transfer resistance of drying sample. In addition, as heating plate temperature was increased, drying time was decreased due to increased evaporation pressure of drying sample. Furthermore, drying time with desiccant was decreased approximately 20% than that without desiccant.

• Applied Chemistry for Engineering
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• v.35 no.1
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• pp.42-47
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• 2024

Limonene was separated from waste citrus peels by a vacuum drying process with a venturi, and bioethanol was produced from dried citrus peels. Vacuum drying using venturi was very effective in removing moisture and limonene compared to hot air drying and natural drying. Citrus peels prepared by venturi vacuum drying were the most suitable for ethanol fermentation. The moisture and limonene content of the citrus peels dried for 15 hours were 17.0% and 3.2%, respectively. By venturi vacuum drying, essential oil containing limonene and floral water were obtained, respectively. The amount of essential oil separated by venturi vacuum drying was 4.21 mL essential oil/kg citrus peel, 79.9% of the separated essential oil was limonene.

• Journal of Advanced Marine Engineering and Technology
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• v.28 no.6
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• pp.981-992
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• 2004

Freeze drying under vacuum condition is a complex process that involves simultaneous heat and mass transfer, sublimation of ice, and motion of sublimation front. Proper treatment of the motion of sublimation interface is crucial for an accurate prediction of the freeze drying process. Based on the enthalpy formulation that has been successfully used in liquid/solid phase change problems. a fixed grid method. streamlined for the freeze drying analysis. was developed in this study. The accuracy of the fixed grid method was checked by solving a one-dimensional tray freeze drying and a two-dimensional vial freeze drying problem and then comparing the results with those by the moving grid method. Finally. the freeze drying characteristics of two-dimensional slab and axis-symmetric cylinder was investigated using the fixed grid method.