• Title/Summary/Keyword: Ultrafine grain

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Fabrication and Estimation of an Ultrafine Grained Complex Aluminum Alloy Sheet by the ARB Process Using Dissimilar Aluminum Alloys (이종 알루미늄의 ARB공정에 의한 초미세립 복합알루미늄합금판재의 제조 및 평가)

  • Lee, Seong-Hee;Kang, Chang-Seog
    • Korean Journal of Metals and Materials
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    • v.49 no.11
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    • pp.893-899
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    • 2011
  • Fabrication of a complex aluminum alloy by the ARB process using dissimilar aluminum alloys has been carried out. Two-layer stack ARB was performed for up to six cycles at ambient temperature without a lubricant according to the conventional procedure. Dissimilar aluminum sheets of AA1050 and AA5052 with thickness of 1 mm were degreased and wire-brushed for the ARB process. The sheets were then stacked together and rolled to 50% reduction such that the thickness became 1 mm again. The sheet was then cut into two pieces of identical length and the same procedure was repeated for up to six cycles. A sound complex aluminum alloy sheet was successfully fabricated by the ARB process. The tensile strength increased as the number of ARB cycles was increased, reaching 298 MPa after 5 cycles, which is about 2.2 times that of the initial material. The average grain size was $24{\mu}m$ after 1 cycle, and became $1.8{\mu}m$ after 6 cycles.

Effect of friction different channel conditions and temperatures during ECAP (IF-Steel의 ECAP 공정 중 채널 상태와 온도에 따른 마찰효과)

  • ;;;;Rahph Hellmig;Yuri Estrin
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.179-182
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    • 2003
  • Equal channel angular pressing (ECAP) provides an efficient procedure for introducing an ultrafine grain size into a material. In this study, ECAP were conducted on IF-steel to investigate the effect of friction and processing temperatures on the deformation characteristics of the samples. Due to the blocking effect of the previously pressed samples residing in the exit channel, the shear pattern (especially on the bottom region) changes.

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Effect of Prior Microstructures on the Behavior of Cementite and Mechanical Properties in Low Carbon Steels (저탄소강의 초기 미세조직에 따른 기계적 성질과 시멘타이트거동)

  • Lee, Jong-Chul;Kang, Ui-Gu;Lee, Jung-Won;Oh, Chang-Seok;Kim, Sung-Joon;Nam, Won-Jong
    • Transactions of Materials Processing
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    • v.18 no.6
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    • pp.471-475
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    • 2009
  • The effect of prior microstructures on mechanical properties in low carbon steels were examined by comparing the behavior of cementite and mechanical properties of cryo-rolled and subsequently annealed steels. Prior microstructures consisted of ferrite + pearlite, banite or martensite. Steels, consisting of bainitic microstructure, exhibited the better combination of strength - ductility than steels with other prior microstructures, such as ferrite + pearlite and martensite.

Fabrication of $Si_3N_4-SiC$ Nanocomposites by Hot Pressing (Hot Pressing에 의한 $Si_3N_4-SiC$ 나노복합체의 제조)

  • 김성현;김인술;박홍채;오기동
    • Journal of the Korean Ceramic Society
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    • v.31 no.9
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    • pp.1021-1029
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    • 1994
  • SiC ultrafine particles of 1, 10, 20 and 30 vol% were dispersed in $\alpha$-Si3N4 matrix and hot-pressed under the condition of 30 MPa at 1800 and 190$0^{\circ}C$ respectively. Physical, mechanical properties and microstructures of sintered Si3N4-SiC nanocomposites were investigated. Flexural strength and density of Si3N4-10 vol% SiC nanocomposites hot-pressed at 190$0^{\circ}C$ represented the 1002 MPa and 97.9%T.D respectively, and it was confirmed as a remarkable improvement of 67% compared to Si3N4 monolith. Fracture toughness was shown as 7.2 MPa.m1/2 when the same composition was hot pressed at 180$0^{\circ}C$. This effect was supposed to be due to the improvement of microstructure by the adequate suppression of the excessive growth of Si3N4 grain with SiC nano-particles.

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MAGNETIC PROPERTIES OF NANOCRYSTALLINE (Fe,Co)-B-Al-M (M=Nb/Mo/Ta) ALLOYS

  • Kang, D.B.;Cho, W.S.;Kim, T.K.;Cho, Y.S.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.483-486
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    • 1995
  • Soft magnetic properties of Fe-based (Fe,Co)-B-Al-M (M=Nb, Mo or Ta) nanocrystalline alloy have been investigated. The alloy obtained directly form the rapid solidification process. Microstructure of the alloy is a mixtu re of ultrafine bcc Fe(Co) nanocrystallines and a small amount of retained amorphous phase. Heat treatment of as-prepared alloys improves soft magnetic properties in high frequency range. ${(Fe_{.85}Co_{.15})}_{70}B_{18}Al_{10}Ta_{6}$ alloy alloy annealed at $500^{\circ}C$ for 1 h shows the most improved soth magnetic properties among the alloy examined. Average grain size of the nanocystalline is about 10 nm.

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Microstructural Evolution with Annealing of Ultralow Carbon IF Steel Severely Deformed by Six-Layer Stack ARB Process (6층겹침ARB공정에 의해 강소성가공된 극저탄소IF강의 어닐링에 따른 미세조직 변화)

  • Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.22 no.8
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    • pp.403-408
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    • 2012
  • A sample of ultra low carbon IF steel was processed by six-layer stack accumulative roll-bonding (ARB) and annealed. The ARB was conducted at ambient temperature after deforming the as-received material to a thickness of 0.5 mm by 50% cold rolling. The ARB was performed for a six-layer stacked, i.e. a 3 mm thick sheet, up to 3 cycles (an equivalent strain of ~7.0). In each ARB cycle, the stacked sheets were, first, deformed to 1.5 mm thickness by 50% rolling and then reduced to 0.5 mm thickness, as the starting thickness, by multi-pass rolling without lubrication. The specimen after 3 cycles was then annealed for 0.5 h at various temperatures ranging from 673 to 973 K. The microstructural evolution with the annealing temperature for the 3-cycle ARB processed IF steel was investigated in detail by transmission electron microscopy observation. The ARB processed IF steel exhibited mainly a dislocation cell lamella structure with relatively high dislocation density in which the subgrains were partially observed. The selected area diffraction (SAD) patterns suggested that the misorientation between neighboring cells or subgrains was very small. The thickness of the grains increased in a gradual way up to 873 K, but above 898 K it increased drastically. As a result, the grains came to have an equiaxed morphology at 898 K, in which the width and the thickness of the grains were almost identical. The grain growth occurred actively at temperatures above 923 K.

Effect of stress-strain curve changing with equal channel angular pressing on ultimate strength of ship hull stiffened panels

  • Sekban, Dursun Murat;Olmez, Hasan
    • Structural Engineering and Mechanics
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    • v.78 no.4
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    • pp.473-484
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    • 2021
  • Similar to other structures, ultimate strength values showing the maximum load that the structure can resist without damaging has great importance on ships. Therefore, increasing the ultimate strength values will be an important benefit for the structure. Low carbon steels used in ships due to their low cost and good weldability. Improving the ultimate strength values without interfering with the chemical composition to prevent of the weldability properties of these steels would be very beneficial for ships. Grain refinement via severe plastic deformation (SPD) is an essential strengthening mechanism without changing the chemical composition of metallic materials. Among SPD methods, equal channel angular pressing (ECAP) is one of the most commonly used one due to its capacity for achieving bulk ultrafine-grained (UFG) materials. When the literature is examined, it is seen that there is no study about ultimate strength calculation in ships after ECAP. Therefore, the mean purpose of this study is to apply ECAP to a shipbuilding low carbon steel to be able to achieve mechanical properties and investigate the alteration of ship hull girder grillage system's ultimate strength via finite element analysis approach. A fine-grained (FG) microstructure with a mean grain size of 6 ㎛ (initial grain size was 25 ㎛) was after ECAP. This microstructural evolution brought about a considerable increase in strength values. Both yield and tensile strength values increased from 280 MPa and 425 MPa to about 420 MPa and 785 MPa, respectively. This improvement in the strength values reflected a finite element method to determine the ultimate strength of ship hull girder grillage system. As a result of calculations, it was reached significantly higher ultimate strength values (237,876 MPa) compared the non-processed situation (192,986 MPa) on ship hull girder grillage system.

Magnetic Properties of Ultrafine grained Fe-Al-Nb-B-(Cu) Alloys. (Fe-Al-Nb-B-(Cu)계 초미세결정합금의 자기적 특성)

  • 박진영;서수정;김규진;김광윤;노태환
    • Journal of the Korean Magnetics Society
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    • v.6 no.4
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    • pp.218-224
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    • 1996
  • The magnetic properties and crystallization behaviors of $Fe_{83-x}Al_{x}Nb_{5}B_{12}(X=1~5at%)$ alloys were investigated. The $Fe_{80}Al_{3}Nb_{5}B_{12}$ alloy was developed a very good soft magnetic material with ultra-fine grain structure in Fe-Al-Nb-B system alloys. When 1 at% of Cu was added in Fe-Al-Nb-B alloy, the soft magnetic properties were found to improve significantly through the reduction of the grain size upto about 6~7 nm at $450^{\circ}C$. The magnetic properties of the $Fe_{79}Al_{3}Nb_{5}B_{12}Cu_{1}$ alloy were as follows : ${\mu}_{eff}(1\;kHz)=26,000,\;B_{10}=1.45\;T,\;H_{c}=25\;mOe,\;P_{c}(100\;kHz,\;0.2\;T)=55\;W/kg$, respectively.

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Consolidation and Mechanical Behavior of Gas Atomized MgZn4.3Y0.7 Alloy Powders using High Pressure Torsion (고압비틀림 공정을 통한 급속응고 MgZn4.3Y0.7 합금 분말의 치밀화 및 기계적 거동)

  • Yoon, Eun-Yoo;Chae, Hong-Jun;Kim, Taek-Soo;Lee, Chong-Soo;Kim, Hyoung-Seop
    • Journal of Powder Materials
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    • v.17 no.3
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    • pp.190-196
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    • 2010
  • In this paper, rapid solidified Mg-4.3Zn-0.7Y (at.%) alloy powders were prepared using an inert gas atomizer, followed by a severe plastic deformation technique of high pressure torsion (HPT) for consolidation of the powders. The gas atomized powders were almost spherical in shape, and grain size was as fine as less than $5\;{\mu}m$ due to rapid solidification. Plastic deformation responses during HPT were simulated using the finite element method, which shows in good agreement with the analytical solutions of a strain expression in torsion. Varying the HPT processing temperature from ambient to 473 K, the behavior of powder consolidation, matrix microstructural evolution and mechanical properties of the compacts was investigated. The gas atomized powders were deformed plastically as well as fully densified, resulting in effective grain size refinements and enhanced microhardness values.

A Study on the Microstructure and Anisotropic Mechanical Properties of Oxygen-Free Copper Fabricated by Equal Channel Angular Pressing (ECAP공법으로 제조된 무산소동의 미세조직 및 기계적 성질 이방성에 대한 고찰)

  • Lee, Jaekun;Hong, Younggon;Kim, Hyoungseop;Park, Sunghyuk
    • Journal of the Korea Institute of Military Science and Technology
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    • v.22 no.4
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    • pp.492-500
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    • 2019
  • Equal channel angular pressing(ECAP) is a severe plastic deformation technique capable of introducing large shear strain in bulk metal materials. However, if an ECAPed material has an inhomogeneous microstructure and anisotropic mechanical properties, this material is difficult to apply as structural components subjected to multi-axial stress during use. In this study, extruded oxygen-free copper(OFC) rods with a large diameter of 42 mm are extruded through ECAP by route Bc up to 12 passes. The variations in the microstructure, hardness, tensile properties, and microstructural and mechanical homogeneity of the ECAPed samples are systematically analyzed. High-strength OFC rods with a homogeneous and equiaxed-ultrafine grain structure are obtained by the repeated application of ECAP up to 8 and 12 passes. ECAPed samples with 4 and 8 passes exhibit much smaller differences in terms of the average grain sizes on the cross-sectional area and the tensile strengths along the axial and circumferential directions, as compared to the samples with 1 and 2 passes. Therefore, it is considered that the OFC materials, which are fabricated via the ECAP process with pass numbers of a multiple of 4, are suitable to be applied as high-strength structural parts used under multi-axial stress conditions.