• 제목/요약/키워드: Ultra-high-pressure consolidation

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Fundamental Aspects of Resistance Sintering under Ultrahigh Pressure Consolidation

  • Zhou, Zhangjian;Kim, Ji-Soon;Yum, Young-Jin
    • 한국분말재료학회지
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    • 제19권1호
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    • pp.19-24
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    • 2012
  • The consolidation results of fine tungsten powders, W-Cu composite and W/Cu FGM by using a novel method combining resistance sintering with ultra high pressure have been reviewed. The densification effects of the consolidation parameters, including pressure, input power and sintering time, have been investigated. The sintering mechanism of this method was quite different from other sintering methods. Particle rearrangement, sliding, distortion and crushing due to the ultra high pressure are the dominant mehanisms at the initial stage, then the dominant sintering mechanisms are transient arc-fused processes controlled by the input power.

Bulk Amorphous and/or Nanocrystalline Finemet Alloy Prepared by Super-high-pressure Consolidation

  • Lu, Wei;Yanb, Biao
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.788-789
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    • 2006
  • Microstructure and soft magnetic properties of bulk amorphous and/or nanocrystalline $Fe_{73.5}Cu_1Nb_3Si_{13.5}B_9$ alloys prepared by consolidation at 5.5GPa were investigated. The relative density of the bulk sample 1 (from amorphous powders) was 98.5% and the grain sizes were about 10.6nm. While the relative density and grain sizes of bulk sample 2 (from nanocrystalline powders) are 98% and 20.1nm, respectively. Particularly, the bulk samples exhibited a good combined magnetic property: for Sample1, $M_s=125emu/g$ and $H_c=1.5Oe;$ for Sample2, $M_s=129emu/g$ and $H_c=3.3Oe$. The success of synthesizing the nanocrystalline Fe-based bulk alloys will be encouraging for the future development of bulk nanocrystalline soft magnetic alloys.

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Fabrication of W-Cu Composite by Resistance Sintering under Ultrahigh Pressure

  • Kwon, Y.S.;Kim, J.S.;Zhou, Z.J.
    • 한국분말재료학회지
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    • 제10권3호
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    • pp.181-185
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    • 2003
  • Resistance sintering under ultra-high pressure if developed to fabricate W-Cu composite containing 5 to 80v/o copper. The consolidation was carried out under pressure of 6 to 8 GPa and input power of 18 to 23 kW for 50 seconds. The densification effect and microstructure of these W-Cu composites are investigated. The effect of W particle size on ,sintering density was also studied. The micro hardness was measured to evaluate the sintering effect.

급속 소결 공정에 의한 초미립 WC-10Co와 WC-10Fe 초경재료 제조와 기계적 성질 (Mechanical Properties and Consolidation of Ultra-Fine WC-10Co and WC-10Fe Hard Materials by Rapid Sintering Process)

  • 정인균;박정환;도정만;김기열;우기도;고인용;손인진
    • 대한금속재료학회지
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    • 제46권4호
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    • pp.223-226
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    • 2008
  • The comparison of sintering behavior and mechanical properties of ultra-fine WC-10wt.%Co and WC-10wt.%Fe hard materials produced by high-frequency induction heated sintering (HFIHS) was accomplished using ultra fine powder of WC and binders(Co, Fe). The advantage of this process allows very quick densification to near theoretical density and prohibition of grain growth in nano-structured materials. Highly dense WC-10Co and WC-10Fe with a relative density of up to 99% could be obtained with simultaneous application of 60 MPa pressure and induced current within 1 minute without significant change in grain size. The hardness and fracture toughness of the dense WC-10Co and WC-10Fe composites produced by HFIHS were investigated.