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Specimen Preparation for Scanning Electron Microscope Using a Converted Sample Stage

  • Kim, Hyelan;Kim, Hyo-Sik;Yu, Seungmin;Bae, Tae-Sung
    • Applied Microscopy
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    • v.45 no.4
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    • pp.214-217
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    • 2015
  • This study introduces metal coating as an effective sample preparation method to remove charge-up caused by the shadow effect during field emission scanning electron microscope (FE-SEM) analysis of dynamic structured samples. During a FE-SEM analysis, charge-up occurs when the primary electrons (input electrons) that scan the specimens are not equal to the output electrons (secondary electrons, backscattered electrons, auger electrons, etc.) generated from the specimens. To remove charge-up, a metal layer of Pt, Au or Pd is applied on the surface of the sample. However, in some cases, charge-up still occurs due to the shadow effect. This study developed a coating method that effectively removes charge-up. By creating a converted sample stage capable of simultaneous tilt and rotation, the shadow effect was successfully removed, and image data without charge-up were obtained.

Effect of Sperm Selection by Glass Wool Filtration and Swim-up on the Fertilizing Capacity of Frozen-thawed Boar Sperm (동결융해 돼지정자의 수정능에 대한 Glass Wool여과법과 Swim-up법에 의한 정자 선별의 효과)

  • 박수봉;고대환;정진관
    • Journal of Embryo Transfer
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    • v.7 no.2
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    • pp.133-136
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    • 1992
  • Glass wool filtration and swim-up method resulted in inreasing to 58.3% and 62.7% of the progressive motility in frozen-thawed boar sperm, compared to 34.2% in the untreated sperm. Glass wool filtration tended to be more successful than swim-up method for the survival sfter incubation of 38.5$^{\circ}C$ for 3h. Sperm recovered by both the swim-up method and the glass wool filtration method were tested in an in vitro fertilization to determine which of the two techniques would yield sperm with high fertilizing capacity. The results indicated that there was a significantly(p

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A Study on the Start-up and Shut-down Characteristics for PEMFC System (고분자 연료전지시스템의 기동 및 정지특성에 관한 연구)

  • Lee, Jung-Woon;Seo, Won-Seok;Kim, Young-Gyu
    • 한국신재생에너지학회:학술대회논문집
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    • 2008.05a
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    • pp.29-32
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    • 2008
  • Testing was conducted to determine the performance of a residential fuel cell system when subjected to DSS and WSS operation, especially for start-up and shut-down characteristics. In terms of start-up time, it took about 70min to start output power generation and stably to reach 1kW at cold start. Measurement of the characteristics of heat and power generation were carried out at start-up and shut-down time. Fuel gas is used for heating both reformer and stack from start-up to the beginning of power generation. In terms of start-up and shut-down characteristics, it was important to control the reformer temperature precisely. The average output water temperature during the rated output operation(960W) was $63.2^{\circ}C$ constantly. The results of the investigation are being used to develop a new test protocols for residential fuel cell system.

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The physical properties and the dyeability of nylon fibers prepared by high speed spinning (고속방사 나일론 섬유의 물성 및 염색성)

  • 김태경;윤석한;임용진;손영아;한진완
    • Textile Coloration and Finishing
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    • v.14 no.4
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    • pp.197-207
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    • 2002
  • The physical properties and dyeability of the nylon 6 fibers prepared by high speed spinning at take-up speed of 4,100~5,600m/min were investigated. The strain decreased as the take-up speed was raised from 4,100m/min to 4,400m/min, but further increase of take-up speed could not decrease the strain. The stresses of the fibers spinned at various take-up speed did not make any noticeable differences. Birefringences, densities and crystallinities of the fibers increased with the take-up speed and then reached to a nearly maximum value at 5,300m/min. In DSC diagrams, the $\gamma$ form of crystal became dominant at higher take-up speed. The dye uptakes of C. I. Acid Blue 113 on the fibers decreased a little with the increase of take-up speed.

Design and Implementation of Up-converter for WCDMA Digital Optic Repeater (WCDMA 디지털 광 중계기용 Up-converter 설계 및 제작)

  • 최영선;강원구;장인봉
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2003.05a
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    • pp.586-589
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    • 2003
  • Repeater is developed. Based on the systems The up-converter of the WCDMA Digital Optic pecifications, the structure of the up-converter is accomplished and its block diagram is drawn. The up-converter is implemented according to these block diagrams. Subsequently the low pass filter, the automatic level controlled attenuator, the frequency synthesizer and other components for the up-converter are designed and implemented, and a main board to integrate these modules is also manufactured. To reduce the noise floor of system and suppress the RF spurious noise, a PCB layout is performed carefully. For each module consisting of the up-converter and the entire system, the performance tests are accomplished to check the performance about the specifications.

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Analytical Rapid Prediction of Tsunami Run-up Heights: Application to 2010 Chilean Tsunami

  • Choi, Byung Ho;Kim, Kyeong Ok;Yuk, Jin-Hee;Kaistrenko, Victor;Pelinovsky, Efim
    • Ocean and Polar Research
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    • v.37 no.1
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    • pp.1-9
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    • 2015
  • An approach based on the combined use of a 2D shallow water model and analytical 1D long wave run-up theory is proposed which facilitates the forecasting of tsunami run-up heights in a more rapid way, compared with the statistical or empirical run-up ratio method or resorting to complicated coastal inundation models. Its application is advantageous for long-term tsunami predictions based on the modeling of many prognostic tsunami scenarios. The modeling of the Chilean tsunami on February 27, 2010 has been performed, and the estimations of run-up heights are found to be in good agreement with available observations.

GLOBAL EXISTENCE AND BLOW-UP FOR A DEGENERATE REACTION-DIFFUSION SYSTEM WITH NONLINEAR LOCALIZED SOURCES AND NONLOCAL BOUNDARY CONDITIONS

  • LIANG, FEI
    • Journal of the Korean Mathematical Society
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    • v.53 no.1
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    • pp.27-43
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    • 2016
  • This paper deals with a degenerate parabolic system with coupled nonlinear localized sources subject to weighted nonlocal Dirichlet boundary conditions. We obtain the conditions for global and blow-up solutions. It is interesting to observe that the weight functions for the nonlocal Dirichlet boundary conditions play substantial roles in determining not only whether the solutions are global or blow-up, but also whether the blowing up occurs for any positive initial data or just for large ones. Moreover, we establish the precise blow-up rate.

A Tracking Gain-Up Controller Design for Controlling the Shake of Actuator (엑츄에이터 흔들림 제어를 위한 트랙킹 Gain-Up 제어기 설계)

  • Jin, Kyoung-Bog;Lee, Moon-Noh
    • Journal of Institute of Control, Robotics and Systems
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    • v.15 no.10
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    • pp.988-993
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    • 2009
  • In this paper, we deal with a tracking gain-up controller design problem to control effectively the shake of tracking actuator after a track seek. A minimum tracking gain-up open-loop gain can be calculated by estimating the shake of tracking actuator and a desired transient specification is considered to diminish effectively the shake of actuator. A tracking gain-up controller is designed by considering a robust $H_{\infty}$ control problem with a regional stability constraint. The proposed tracking gain-up controller design method is applied to the track-following system of a DVD recording device and is evaluated through the experimental results.

Dynamic Behavior of an Internal Loop Reactor during Scale-up (내부순환반응기의 Scale-up에 따른 동력학적 특성의 변화)

  • 최윤찬;박영식
    • Journal of Environmental Science International
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    • v.6 no.1
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    • pp.25-31
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    • 1997
  • The variations of gas hold-up, overall volumetric oxygen mass transfer coefficients and liquid circulation velocity in an internal loop reactor were investigated to manifest scale-up effect. The relationship between superficial gas velocity and gas hold-up were found as Ugr = 0.045 $\varepsilon$r in the pilot-scale and Ugr = 0.056 $\varepsilon$r in the bench-scale reactor. The overall volumetric oxygen mass tractsfer coefficient, KLa was slightly increased in the pilot-scale than in the bench-scale reactor. Flow regime was changed from the bubble flow to the churn-turbulent flow when the superficial gas velocity reached to 3.5 - 4 cm/sec in the pilot-scale.

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Characteristics of Latch-up Current of the Dual Gate Emitter Switched Thyristor (Dual Gate Emitter Switched Thyristor의 Latch-up 전류 특성)

  • 이응래;오정근;이형규;주병권;김남수
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.8
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    • pp.799-805
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    • 2004
  • Two dimensional MEDICI simulator is used to study the characteristics of latch-up current of Dual Gate Emitter Switched Thyristor. The simulation is done in terms of the current-voltage characteristics, latch-up current density, ON-voltage drop and electrical property with the variations of p-base impurity concentrations. Compared with the other power devices such as MOS Controlled Cascade Thyristor(MCCT), Conventional Emitter Switched Thyristor(C-EST) and Dual Channel Emitter Switched Thyristor(DC-EST), Dual Gate Emitter Switched Thyristor(DG-EST) shows to have the better electrical characteristics, which is the high latch-up current density and low forward voltage-drop. The proposed DG-EST which has a non-planer p-base structure under the floating $N^+$ emitter indicates to have the better characteristics of latch-up current and breakover voltage.