• 한국진공학회:학술대회논문집
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• 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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• pp.221.1-221.1
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• 2015

The vapor-liquid-solid (VLS) method, where the "liquid" catalytic droplets collecting atoms from vapor precursors build the solid crystal layers via supersaturation, is a ubiquitous technique to synthesize 1-dimensional nanoscale materials. However, the lack of fundamental understanding of chemical information governing the process inhibits the rational route to the structural programming. By combining the in situ or operando IR spectroscopy with post-growth high resolution electron microscopy, we show the strong correlation between the surface chemical species concentration and nanowire structures. More specifically, the critical role of surface adsorbed hydrogen, generated from the decomposition of Si2H6 precursor on the interplay between nanowire / kinking and the defect propagation is demonstrated. Our results show that adsorbed hydrogen atoms are responsible for selecting -oriented growth and indicate that a twin boundary imparts structural coherence. The twin boundary, only continuous at / kinks, reduces the symmetry of the trijunction and limits the number of degenerate directions available to the nanowire. These findings constitute a general approach for rationally engineering kinking superstructures and also provide important insight into the role of surface chemical bonding during VLS synthesis.

• 한국진공학회지
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• 제14권1호
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• pp.7-16
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• 2005

두 개의 쌍원통 실린더를 구성하고 있는 기름-물 펌프는 차세대 저진공 펌프로의 활용이 가능하다. 하지만 설계개선을 위한 유동 해석 결과가 충분하지 않다. 경제적 측면에서 상업화 이전에 수치해석 방법에 의한 유동해석이 요구되고 있다. 유동 해석에 사용되는 상업용 코드(Fluent)을 사용하여 펌프의 설계에 필요한 자료를 제공하였다. 쌍원통 실린더와 고정 실린더 사이의 속도와 압력 분포 등의 유동변수를 분석하기 위하여 2차원 해석을 수행하였다. 본 수치해석 방법은 쌍원통 실린더로 구성된 펌프의 성능향상에 유용하게 사용할 수 있다.

• 대한기계학회논문집B
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• 제24권10호
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• pp.1300-1308
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• 2000

The objectives of this study was to investigate the spray characteristics of single spray and twin spray in the overlap region such as mean axial velocity, mean radial velocity, mean droplet size and probability density function of droplet size. A phase doppler anemometer was used as the measurement system for droplet size and velocity. In case of single spray, injection pressure was varied from 0.2MPa to 0.7MPa. Mean axial velocity, mean radial velocity and droplet size were decreased as the distance below nozzle tip was increased. In case of twin spray, the spray characteristics were measured by varying the distance between two nozzles from 127mm to 155mm. In the overlap region, the boundary of the overlap region was determined by obtaining the distribution of mean axial and radial velocity. Droplet size was increased as the distance from nozzle tip was increased. It was found that the distribution of droplet size for twin spray in the overlap region was different to single spray.

• The Journal of the Acoustical Society of Korea
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• 제25권1E호
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• pp.25-31
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• 2006

Two twin microphones may produce particular patterns of binaural directivity by time delays between the twin microphones. The boundary element method (BEM) was used for the simulation of the sound pressure field around the KEMAR head model in order to quantify the acoustic head effect. The sound pressure onto the microphone was calculated by the BEM to an incident sound pressure. Then a planar directivity pattern was formed by four sound pressure signals from four microphones. The optimal binaural directivity pattern may be achieved by adjusting time delays at each frequency while maintaining the forward beam pattern is relatively bigger than the backward beam pattern. The simulation results were verified by the experimental measurement.

• 대한기계학회논문집
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• 제12권2호
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• pp.359-372
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• 1988

본 연구에서는 두 노즐간의 거리와 분사압력을 변화시켜 하류로 전개되는 이중분무의 분무형태를 살펴보았다.

• 대한기계학회논문집
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• 제18권3호
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• pp.662-669
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• 1994

In the combustion system, the optimum spray conditions reduce the pollutant emission of exhaust gas and enhance the fuel efficiency. The spray characteristics-the drop size, the drop velocity, the number density and the mass flux, become increasingly important in the design of combustor and in testifying numerical simulation of spray flow in the combustor. The purposes of this study are to clarify the spray characteristics of twin-fluid nozzle and to offer the data for combustor design and the numerical simulation of a spray flow. Spatial drop diameter was measured by immersion sampling method. The mean diameter, size distribution and uniformity of drop were analyzed with variations of air/liquid mass flow ratio. The results show that the SMD increases with the liquid supply flow rate and decreases with the air supply velocity. The radial distribution of SMD shows the larger drops can diffuse farther to the boundary of spray. And the drop size range is found to be wider close to the spray boundary where the maximum SMD locates.

• 한국결정학회지
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• 제6권2호
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• pp.69-74
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• 1995

Ge bicrystal 기판 위에 OMVPE 기법을 이용하여 GaAs 에피층을 성장시킴으로써 특정한 교차각을 갖는 GaAs 기울임입계를 제조하였다. 또한 (110) Ge 기판 위에 성장된 GaAs 에피층 내의 쌍정들로부터 ∑ =9 기울임입계들이 생성되었다. 고분해 투과전자현미경을 이용하여 1차 및 2차 쌍정계면들의 구조적 특징들을 고찰하였다. 입계에서의 결합극성은 특정한 회절조건에서 입계 양쪽의 입자로부터 기록된 (200) 수렴성 빔 디스크 내의 HOLZ 선 콘트라스트를 응용하여 파악하였으며, 원자컬럼이나 채널등과 상관된 구조상 콘트라스트 양태를 동일한 사진 내의 1차 쌍정계면 거울면의 콘트라스트로부터 파악하였다. ∑ =9, (115)/(111)[110] 기울입입계는 5-6-7- 모서리 링으로 구성된 단위구조를 나타내며, 입계 양쪽에 놓인 입자들은 입계에서 anti-site type cross-boundary bonding의 분율이 최소화되도록 배향되어 있다.

• 열처리공학회지
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• 제35권2호
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• pp.74-81
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• 2022

This study aims to mitigate the microstructural heterogeneity arising from the manufacture of magnesium alloy plates using the twin roll casting (TRC) process. Homogenization was introduced through hot rolling and heat treatment, followed by confirmation of observed changes in the microstructure. Following the TRC process, the hot rolled 2mm plate exhibited a dendritic cast structure tilted in the roll rotation direction, while central segregation were developed. This nonuniform structure and central segregation disappeared upon heat treatment, followed by recrystallization to form uniform and fine grains. Abnormal grain growth (AGG) was observed over the course of heat treatment; grains exhibiting AGG occupied up to 75% of the total area after having held the sample at 400℃ for 64 h. The formation of coarse grains was also observed during heat treatment at 340℃ over a relatively long duration, though the maximum grain size was significantly smaller than that corresponding to the heat treatment at 400℃. AGG in the 400℃ heat treatment occurred because of movement of the grain boundary, which had been fixed prior as a result of the grain boundary fixing effect of the precipitation phase. The re-dissolution of the Ca₂Mg₅Zn₅ precipitated phase over the long duration of the high-temperature annealing process caused the surrounding grains to disappear and regrow.

• 한국주조공학회지
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• 제26권3호
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• pp.140-145
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• 2006

Sr, added in the hypereutectic Al-Si alloys, is absorbed on the surfaces of primary Si as well as eutectic Si, and can change the growth mode of primary Si from non-faceted to faceted mode, as the amount of Sr increases larger than 0.04 wt.%, even though it cannot affect the grain size of primary Si, significantly. The EBSD analysis shows that the traction of ${\Sigma}3$ boundary(twin boundary) increases as the amount of Sr in the hypereutectic Al-Si alloys increase until the over-modification occurs at 1.6 wt.%Sr and proves that the change in growth mode of primary Si results from the change of TPRE growth to IIT growth.

• 대한전자공학회논문지
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• 제25권8호
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• pp.950-958
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• 1988

We have implemented a RTA system using W-halogen lamps and tried to recrystallize the phosphorus ion implanted amorphous silicon on insultor (SOI) taking advantages of seeding window. The purpose of this study is to investigate the possibility of a typical crystalline orientation occurred during the solidifying process of molten amorphous silicon layer. Experimental results show that several twin boundaries are found on the seeding window region after annealing for 15 sec at 1040\ulcorner. These twin boundaries represent that the recrystallization is partialy possible and when the annealing is done at 1150\ulcorner, (100) etch pits with <110> facets are found on the solidified amorphous silicon layer. Consequently, Hall mobility of recrystallized silicon film is measured and the thermal behavior of grain boundary is also observed by SEM.