• 한국안전학회지
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• 제12권1호
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• pp.19-28
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• 1997

This study was made of the effect of cold working on the stress corrosion cracking(SCC) of austenitlc 304 stainless steel in boiling 42% $MgCl_2$ solution. For this experiment, specimens cold-worked of 0%, 10%, 20%, 30%, 40% were fabricated respectively, and then experiments of mechanical properties and stress corrosion cracking(SCC) of these specimens were carried out. The results of these experiments indicate that the maximum resistance to SCC showed at 20% of cold working degree and that the SCC susceptibility depended on the volume fraction of deformation-induced martensite by cold working and the work hardening of matrix. On the other hand, the fracture mode was changed. This phenomenon was considered that deformation-induced martensite was grown from transgranular fracture mode to intergranular fracture mode and caused by increased of dislocation density along the slip planes.

• 한국세라믹학회지
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• 제36권4호
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• pp.372-379
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• 1999

Hihg-toughened ceria-stabilized tetragonal zirconia ceramics with irregular grain shape and undulated grain boundary was prepared by ceria doping. Irregularity of grain shapes was increased with the amount of doped ceria. But in case of the large amount of doped ceria grain boundary was migrated to the reverse direction of DIGM. Ceria-stabilized zirconia ceramics annealed at 1650$^{\circ}C$ for 2h after twice dippings into cerium nitrate solu-tion of 0.2M and sintering at 1500$^{\circ}C$ for 2h showed the highest grain boundary length with a value of 23.6$\mu\textrm{m}$ Ceria concentration difference between convex and concave sides in irregular grains was observed over 1 mol% but not observed in normal grains, Specimens with normal grain shape showed intergranular fracture mode whereas the specimens with irregular grain shape showed transgranular fracture mode.

• 한국세라믹학회지
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• 제26권6호
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• pp.789-794
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• 1989

The high-temperature strength of Ce-TZP was measured at 200, 650 and 100$0^{\circ}C$ by 4-point bending test. And its fracture behavior was observed by SEM. Below $650^{\circ}C$ of the temperature, where monoclinic fraction was almost zero, the decreasing rate of bending strength was relatively slow, but above this temperature, high temperature strength was largely decreased as a result of the decrease of stress-induced transformation of zirconia. The observation of fracture surface bended at 100$0^{\circ}C$ indicated that the fracture mode changed from intergranular-into transgranular-form with regardless of ceria contents.

• 한국세라믹학회지
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• 제34권8호
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• pp.877-885
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• 1997

The dependence of strength, crack growth, fracture mode and degree of domain rearrangement of PZT ceramics on poling strength were studied. The PZT [(Pb0.94Sr0.06)(Zr0.46Ti0.54)O3+Nb(trace)] specimens were poled at 0, 0.5, 1.0, 1.5, 2.0, 2.5, 3.0 kv/mm, and the strength of the specimens was measured by 3 point flexure system. The bending strength of the specimen decreased in different modes according to the bending directions; xz, zx and yz plane direction with x axis of the poling direction in Cartesian coordinate system. The strength differences between the directions increased as the poling strength increased. The fracture mode transferred to intergranular fracture mode from transgranular one as the poling strength increased. The mechanical breakdown occurred when the poling strength higher than 3 kV/mm was applied to the specimen. It was observed that the crack length increased in the normal direction to the poling direction, however, decreased in the parallel direction to the poling direction when the poled PZT specimen was indented by the Vickers indenter. However, the crack produced by indentation continuously was continuously increased little by little after indentation on the specimen. The domain rearrangement occurred as the poling strength increased and the domains were rearranged more effectively when the electric field was continuously increased little by little.

• 한국재료학회지
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• 제2권3호
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• pp.172-179
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• 1992

$Al_2O_3/ZrO_2$복합분말에 상릉분말을 침가하여 상압소결법으로 $Al_2O_3/ZrO_2$복합체를 제조한 후, 밀도, 강도, 경도 및 파괴인성등의 물성을 측정하였으며 미세구조 및 파괴단면도 관찰하였다. 상용분말의 침가량이 중량비로 50%이하인 경우에는 평균 꺽임 강도가 640 MPa정도로 거의 변화가 없었으며, 50%이상 첨가된 경우에는 강도가 저하되었는데, 이는 미세조직과 관계가 있는 것으로 생각된다. 또한 파괴인성(4.3-5.3 $Mpam^{1/2}$)값은 상용분말 첨가량에 비례하여 증가하였다. 파괴단면 관찰결과 파괴원인으로는 가공에서 생기는 표면 결함, $ZrO_2$ agglomeration에 의한 crack-like void 및 $Al_2O_3/ZrO_2$ nano복합체 분말과 상용분말간의 소결성 차이에서 생기는 계면 분리등이 관찰되었는데, nano 복합 분말만을 사용한 소결체에서는 가공에 의한 표면 결함만이 파괴원으로 작용하였다. 또한, 파괴형태는 주로 transgranular fracture이었다

• 한국세라믹학회지
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• 제33권7호
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• pp.785-792
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• 1996

Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN compo-site using oxides as a sintering aid at 185$0^{\circ}C$ and 195$0^{\circ}C$ Regardless of SiC/AlN ratio in composition most of sintered specimens showed he complex structure mixed with 2H solid solution and SiC particles. High sintering temperature and large AlN content in starting composition enhanced the formation of 2H solid solution in sintered specimen 2H solid solution showed the spherical shape and core-rim structure. AlN content in the core is higher than that in the rim but SiC content . The size of 2H solid solution on fracture showed the transgranular fracture mode compared with the dispersed SiC particles which showed the intergranular fracture mode.

• 열처리공학회지
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• 제10권3호
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• pp.172-180
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• 1997

The microstructure, tensile and impact properties of forgings of 7175 aluminium alloy have been studied as a function of intermediate thermo-mechanical treatment(ITMT) process. The ITMT process is consisted of warm working and recrystallization. In the case that the billet was warm-worked above 60% below $250^{\circ}C$ and recrystallized at $475^{\circ}C$, the grain size revealed about $17{\mu}m$ which corresponds to one third of that of conventional process. The refinement of grain size leaded to the improved ductility and impact energy without sacrifice of tensile strength. It was found that the ITMT processed specimen behaved isotropically due to the near equiaxed grains. It was observed that the ITMT processed specimen showed the mixed fracture mode of transgranular and intergranular, instead of intergranular mode. This change of fracture mode contributed to the improved ductility and impact property.

• 대한기계학회논문집A
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• 제40권6호
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• pp.565-571
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• 2016

본 논문은 Alloy 617 모재와 용접재에 대한 저사이클 피로 시험 후의 파괴 시험편에 대한 거시적 및 미시적 파면해석을 나타낸다. 용접재 시험편은 Alloy 617의 가스텅그스텐아크 용접 패드로부터 채취, 제작하였다. 본 연구의 목적은 Alloy 617의 모재와 용접재 시험편의 저사이클 파괴 모드 및 기구의 거시적 및 미시적 양상을 고찰하는 것이다. 전변형률 제어 피로시험이 상온에서 0.6, 0.9, 1.2 및 1.5%에 대하여 수행되었다. Alloy 617 모재의 거시적 파면은 피로하중 축에 수직인 평평한 형태의 양상을 보였으나, 용접재 시험편의 경우는 상대적으로 전단/별모양의 양상의 파괴를 나타내었다. 두 시험편 모두 피로균열전파 영역에서는 명확한 스트라이에이션이 관찰되었다. 한편, 모재의 피로균열은 피로 하중 축에 수직인 방향으로 결정입내를 따라 전파하였으나, 용접재 시험편의 경우 하중 축에 거의 $45^{\circ}$의 경사진 형태의 결정입내로 나타났다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1159-1160
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• 2006

For pure Molybdenum carburized in mixed gases of argon and carbon monoxide, microstructural observations were carried out. X-ray diffraction analysis for carburized specimens revealed that brittle ${\alpha}-Mo_2C$- layer hardly formed in the case of low carbon monoxide concentration. Fracture strength of the specimen carburized at 1673 K for 16 h is about 550 MPa higher than that of the un-carburized specimen. SEM observation revealed that with increasing carburizing temperature, the region demonstrating a transgranular fracture mode progressed towards the center of specimen. This result means that the grain boundaries were strengthened by the grain boundary diffusion of carbon and the strength of grain boundaries exceeded that of grain itself.

• 한국주조공학회지
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• 제21권6호
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• pp.336-342
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• 2001

This study was carried out to examine the effects of adding 0.3at.%Hf in Fe-30at.%Al-5at.%Cr alloy on the variation of microstructures and hot workability. The effect of hot rolling on mechanical properties was estimated by measuring the elongation and tensile strength after rolling at 800 and 1000 respectively. Microstructure of Fe-30at.%Al-5at.%Cr alloy was consisted of large equiaxed grains and it was changed to quasi-equiaxed or columnar structures by adding 0.3at.%Hf to Fe-30at.%Al-5at.%Cr alloy. Every specimens showed a decreased tensile strength after hot rolling compared to that of before rolling. The elongation was increased by hot rolling. Remarkable changes in elongation by hot rollong was observed such as from 1.4% to 4.5% elongation at the specimen of 0.3at.%Hf added to Fe-30at.%Al-5at.%Cr. Fe-30at.%Al-5at.%Cr alloy showed typical cleavage fracture on tensile failure and hot rolling has negligible effects on fracture mode in this alloy. However at the alloy containing Hf fracture mode was changed by hot rolling from intergranular to mixed intergranular and transgranular fracture mode.