• Journal of Power System Engineering
• /
• v.3 no.3
• /
• pp.76-82
• /
• 1999

This study presents a methodology to predict the hardenability of quenched carbon steels. The equation of transient heat conduction is analyzed to formulate a cooling curve by a finite element method which incorperates coupled effects of temperature on physical properties, the metallic structures and also the latent heat by phase transformation. The volume traction of martensite and pearlite are the structural analysis for hardenability analysis. In order to demonstrate the feasibility of adopting a full quench model respectively. This procedure could be used as the database for optimal condition of heat treatment processes.

• Journal of the Korean institute of surface engineering
• /
• v.32 no.2
• /
• pp.100-108
• /
• 1999

The microstructure and corrosion properties of Al-Si diffusion coated PWA1426 alloy have been investigated. Experimental variables are included temperatures of heat-treatment and coating thickness. The microstructure of coated layer and corrosion properties were analysed by SEM, EDS and hot corrosion test. Two major processes have been found to contribute to microstructural changes in the coating. These are, firstly, the transformation of the NiAl to other $Ni_2Al_3$-based phase and secondly, the precipitation of Cr containing phases. Specimens heat treated at $1080^{\circ}C$ showed superior corrosion resistance to heat treated at $880^{\circ}C$. These increase in life was attributed to the transformation of NiAl and increased coating thickness of PWA1426 alloy.

• The Magazine of the Society of Air-Conditioning and Refrigerating Engineers of Korea
• /
• v.17 no.4
• /
• pp.473-488
• /
• 1988

This paper is concerned with the prediction of two dimensional turbulent flows in the parallel plate with the repeated cylindrical blockages. The purpose of this paper is to find the effect of the eccentricity and the pitch of the repeated cylindrical blockages on the flow field, heat transfer coefficients and friction factors. A special technique is developed for the solution of the fully developed turbulent recirculating flow, in which the flow field varies periodically. A non-othogonal coordinate transformation is employed to solve the momentum and the energy equations. The results show that the pitch ratio or the eccentricity of the repeated blockages become smaller, or the Reynolds number of the flow larger, friction factors and heat transfer coefficients increase.

• Journal of Ginseng Research
• /
• v.41 no.2
• /
• pp.180-187
• /
• 2017

Background: The incidence of halitosis has a prevalence of 22-50% throughout the world and is generally caused by anaerobic oral microorganisms, such as Fusobacterium nucleatum, Clostridium perfringens, and Porphyromonas gingivalis. Previous investigations on the structure-activity relationships of ginsenosides have led to contrasting results. Particularly, the antibacterial activity of less polar ginsenosides against halitosis-related bacteria has not been reported. Methods: Crude saponins extracted from the Panax quinquefolius leaf-stem (AGS) were treated at $130^{\circ}C$ for 3 h to obtain heat-transformed saponins (HTS). Five ginsenoside-enriched fractions (HTS-1, HTS-2, HTS-3, HTS-4, and HTS-5) and less polar ginsenosides were separated by HP-20 resin absorption and HPLC, and the antimicrobial activity and mechanism were investigated. Results: HPLC with diode-array detection analysis revealed that heat treatment induced an extensive conversion of polar ginsenosides (-Rg1/Re, -Rc, -Rb2, and -Rd) to less polar compounds (-Rg2, -Rg3, -Rg6, -F4, -Rg5, and -Rk1). The antimicrobial assays showed that HTS, HTS-3, and HTS-4 were effective at inhibiting the growth of F. nucleatum, C. perfringens, and P. gingivalis. Ginsenosides-Rg5 showed the best antimicrobial activity against the three bacteria, with the lowest values of minimum inhibitory concentration and minimum bactericidal concentration. One major reason for this result is that less polar ginsenosides can more easily damage membrane integrity. Conclusion: The results indicated that the less polar ginsenoside-enriched fraction from heat transformation can be used as an antibacterial agent to control halitosis.

• Progress in Superconductivity and Cryogenics
• /
• v.5 no.1
• /
• pp.40-43
• /
• 2003

The phase transformation, variation of secondary phase, and critical current density $(J_c) for (Bi,Pb)_2Sr_2Ca_2Cu_3O_10 (2223)$ tapes have been studied through the thermal slide heat treatment (TSHT) process. This process consists of a multiple variations of oxygen partial pressures and temperatures at the initial heat treatment During the initial heat treatment some secondary phase such as $(Ca,Sr)_2CuO_3(2/1 AEC), (Ca,Sr)_{14}Cu_{24}O_{41} (14/24 AEC), and (Bi,Pb)_2Sr_2CuO_y$(2201, amorphous phase) farm in Bi-2223 tapes, especially at the 2223 grain boundaries. These secondary phases are detrimental to the phase transformation and final properties. In order to control the secondary phase in Bi-2223 tapes the amount and size of secondary phases among the TSHT process were observed. The results indicate that the amount and particle size of AEC particles were smaller when the TSHT process was used than when the normal process at the initial heat treatment was used which results in the improved $J_c$ properties after the final process.

• Journal of the Korean Society for Heat Treatment
• /
• v.24 no.5
• /
• pp.262-270
• /
• 2011

Carbide precipitation and dissolution behavior at various temperatures during heat treatment has been studied in STD11 cold working die steel through confocal scanning laser microscopy; dilatometry; and X-ray diffraction analysis. The equilibrium phase diagram and phase fractions with temperature were calculated using a FactSage program. Confocal laser microscopic observation revealed that ${\alpha}$ to ${\gamma}$ transformation temperature is near $800^{\circ}C$; M7C3 carbides melt at $1245^{\circ}C$; and the melting temperature of STD11 is near $1370^{\circ}C$. XRD results indicated that the M23C6 carbides dissolve in the matrix if austenitized at over $1030^{\circ}C$; while the M7C3 carbides remain up to $1200^{\circ}C$ although their amount decreases. The calculated equilibrium phase diagram showed good agreement with experimental results on carbide dissolution and phase transformation temperatures.

• Journal of the Korean Society for Heat Treatment
• /
• v.29 no.1
• /
• pp.8-14
• /
• 2016

This article presents a study on the tensile properties of hypoeutectoid steels with different ferrite-pearlite microstructures. Nine kinds of hypoeutectoid steel specimens were fabricated by varying carbon content and isothermal transformation temperature. The microstructural factors such as ferrite & pearlite fraction, interlamellar spacing, and cementite thickness were quantitatively measured and then tensile tests were carried out on the specimens in order to investigate the correlation of the microstructural factors with strength and ductility. The pearlite volume fraction usually increased with decreasing transformation temperature, while the pearlite interlamellar spacing and cementite thickness decreased mostly with decreasing transformation temperature, irrespective of carbon content. The tensile test results showed that the yield and tensile strengths of all the steel specimens increased and their ductility was also improved as the transformation temperature decreased. For the steel specimens investigated, the difference in the transformation temperature dependence of strength and ductility could be explained by the fact that the variation in pearlite fraction with transformation temperature noticeably affected various microstructural factors such as pearlite interlamellar spacing and cementite thickness associated with pearlite fracture mechanism such as void initiation, cementite necking, and cracking.

• Journal of the Korean Society of Industry Convergence
• /
• v.25 no.6_2
• /
• pp.1055-1062
• /
• 2022

In this study, the mechanical properties of 80% cold-rolled austenitic 316L stainless steel were evaluated using specimens subjected to reverse transformation at 500-750℃ for 20 minutes and reverse transformation at 700℃ for 2-60 minutes. Also, for the elastic wave obtained from the tensile test, the dominant frequency according to the reverse transformation condition was investigated by time-frequency analysis. The SEM image of the 80% cold-rolled material was transformed into martensite and showed line and cross shapes. The TEM image showed that line shapes were shown at the grain, and grain boundary of martensite. The higher the heat treatment temperature and the longer time, the larger the grain. Tensile strength decreased as the heat treatment temperature and time increased, but elongation increased. Hardness was proportional to tensile strength. This is because the grain with different directions showed the same direction due to reverse transformation. The dominant frequency was decreased and then increased as the temperature and time increased. This is because the direction of the grain is different at a low temperature and the same direction is shown at a high temperature.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.16 no.12S
• /
• pp.1278-1285
• /
• 2003

This study investigated the phase transformation of the REBa$_2$Cu$_3$$O_{7-x}$ (RE=Nd, Gd, Dy) superconductor, and CCT (Continuous-Cooling-Transformation) along with the TTT (Time-Temperature-Transformation) diagrams are suggested according to the isothermal and continuous cooling heat-treatments. The peritectic temperature of the 123 phases decreased approximately 3$0^{\circ}C$ when the ionic radius of the rare-earth elements was reduced. The optimum cooling rate where BC and Cu-free phases do not exist was 0.001$^{\circ}C$/s. At this cooling late, the 123 phase grew with a c-axis Perpendicular to the surface and had a well-distributed 211 phase. When the oxygen partial pressure was reduced Outing isothermal heat-treatment, the formation temperature of the 211 phase decreased. In addition, the formation temperature of the 123 phases decreased from 100$0^{\circ}C$ (Nd-123) to 9$25^{\circ}C$ (Gd-123), and finally 875$^{\circ}C$ (Dy-123) according to the decrease in the ionic radius of the tare-earth elements. Compared to Nd-123, Gd- and Dy-123 had a better texture with a well-distributed 211 phase.e.

• Korean Journal of Plant Tissue Culture
• /
• v.28 no.2
• /
• pp.75-79
• /
• 2001

An experiment was carried out to introduce OsHSP17.9, a low molecular HSP gene isolated from rice plant to orchardgrass (Dactylis glomerata L.) using Agrobacterium. Mature seed-derived calli of orchardgrass were co-cultured with Agrobacterium tumefaciens EHA101 harboring the plasmid pIG-HSP17.9 for transformation. Calli selected by hygromycin were transferred to N$_{6}$ medium containing 1 mg/L NAA, 5 mg/L kinetin, 250 mg/L cefotaxime and 50 mg/L hygromycin and several hygromycin resistant plants were obtained. Stable incorporation of the introduced OsHSP17.9 to the genome of the hygromycin resistant plants was confirmed by PCR and Southern blot analysis. Transformation efficiency was variable between cultivars in which it was 16.5% in Potomac and 8.0% in Frontier. Constitutive expression of the transgene in the transformed orchardgrass tissues was identified by Northern blot analysis but transcript levels were different among individual plants.s.