• 한국재료학회지
• /
• 제25권8호
• /
• pp.403-409
• /
• 2015

Metastable phase characteristics of beta Ti alloys were investigated to consider the relationship of the microstructure and diffraction pattern in TEM. TEM analysis showed that the microstructure was mottled as a modulated structure, and the diffraction pattern was composed of spot streaks between the main spots of a stable beta phase with a specific lattice relationship. The modulated structure may be induced by short distance slip or atom movement during a very short interval of solution treated and quenched (STQ) materials. The athermal ${\omega}$ phase, which could be precipitated at low temperature aging, is also analysed by the metastable phase. The metastable phases including athermal ${\omega}$ phase had a common characteristic of hardened and brittle behavior because the dislocation slip was restricted by a super lattice effect due to short distance atom movement at the metastable state.

• 한국산학기술학회논문지
• /
• 제22권2호
• /
• pp.733-738
• /
• 2021

최근 국내 해양레저에 대한 국민들의 관심이 높아지고 있고, 해외 시장 개척을 위한 레저선박 건조 및 제조업체들의 연구개발이 활발한 실정이다. 기존 레저보트에 많이 사용되어 온 재료 중에서 FRP와 알루미늄합금은 각각 장기간 사용으로 인한 흡습성과 재활용이 불가능한 환경문제와, 높은 열전도도와 고열에 약해 화재에 취약하다는 단점을 가지고 있다. 따라서 본 연구에서는 높은 비강도와 내식성을 갖춘 티타늄합금을 선체 재료로 선택하였고, 선박의 구조설계를 위해 충격하중에 의한 설계하중을 4가지 규정으로부터 산정하고, 이 하중에 대응하는 선체 판두께를 추정하였다. 국제표준인 ISO 12215-5, 이탈리아선급인 RINA Pleasure Yacht, 영국선급인 LR Special Service Craft, 한국선급인 KR 고속경구조선규칙을 비교 분석한 결과, 최대 슬래밍하중은 ISO, KR, LR, RINA의 크기 순서로 높게 계산되었고, 요구되는 판 두께도 ISO, KR, LR, RINA의 크기 순서로 추정되었다. 레저보트는 국제 규정에 적합한 설계와 인증이 필수적이므로, 각 규정에 대한 사용자의 이해를 높이고 해외 수출 선박의 설계 및 승인 절차에 도움이 되리라 생각한다.

• 대한치과보철학회지
• /
• 제41권4호
• /
• pp.503-518
• /
• 2003

Statement of problem : There have been previous studies about considerable variations in machining accuracy and consistency in the implant-abutment-screw interfaces. Purpose : The purpose of this study was to evaluate the machining accuracy and consistency of implant/abutment/screw combinations on two randomly selected implants from each of four manufactures. Material and methods : In this study, screws were respectively used to secure a cemented abutment, to a hexlock implant fixture ; teflon coated titanium alloy screw(Torq-Tite) and titanium alloy screw in Steri--Oss system, gold-plated gold-palladium alloy screw(Gold-Tite) and titanium alloy screw in 3i system gild screw ana titanium screw in AVANA Dental Implant system, and titanium screws in Paragon System. The implants were perpendicularly mounted in polymethyl methacrylate autopolymerizing acrylic resin block(Orthodontic resin, Densply International Inc. USA) by use of dental surveyer. Each abutment screw was secured to the implant with recommended torque value using a digital torque controller. Each screw was again tightened after 10 minutes. All samples were cross sectioned with grinder-polisher unit(Omnilap 2000 SBT Inc) after embeded in liquid unsaturated polyester (Epovia, Cray Valley Inc) Results : There were the largest gaps in the neck areas of screws in hexagonal extension implants which were examined in this study. The leading edge of the abutment screw thread (superior surface) was in contact with the implant body thread, and the majority of the contacting surfaces were localized to the middle portion of the mating threads. Considerable variation in the contacting surfaces was noted in the samples evaluated. Amounts of contact in the abutment screw thread were larger for assemblies with Gold-Tite screw, gold alloy screw. Torq-Tite screw than those with titanium screws. The findings of intimate contact between the screw and screw seat were seen in all samples, regardless of manufacturers. However, microgap between the head and lateral neck surface of the screw and the abutment could be dectected in all samples. The findings of intimate contact between the platform of the implant and the bottom of the abutment were consistent in all samples, regardless of manufacturers. However, microgaps between the lateral surface of external hex of the fixture and the abutment could be dectected in all samples. Conclusion : Considerable variations in machining accuracy and consistency were noted in the samples and the implant-abutment-screw interfaces were incomplete. From the results of this study, further development of the system will be required, including improvements in pattern design.

• 한국재료학회지
• /
• 제14권12호
• /
• pp.857-862
• /
• 2004

Production of titanium powder directly from tantalum oxides ($TiO_2$) pellet through an electronically mediated reaction (EMR) by calciothermic reduction has been investigated. Feed material ($TiO_2\;pellet$) and reductant (Ca-Ni alloy) were charged into electronically isolated locations in a molten calcium chloride ($CaCl_2$) bath at $950^{\circ}C$. The current flow through an external circuit between the feed (cathode) and reductant (anode) locations was monitored during the reduction of $TiO_2$. The current approximately 3.2A was measured during the reaction in the external circuit connecting cathode and anode location. After the reduction experiment, pure titanium powder with low nickel content was obtained even though Ca-Ni alloy was used as a reductant. These results demonstrate that titanium powder can be produced without direct physical contact between the feed and reductant. In certain experimental conditions, pure titanium powder with approximately $99.5\;mass\%$ purity was successfully obtained.

• 연구논문집
• /
• 통권31호
• /
• pp.113-125
• /
• 2001

Silicon addition in titanium alloys generally results in solid solution hardening by silicon itself and precipitation hardening by titanium silicides. The morphology and distribution of the titanium silicides depend upon the alloy chemistry or the heat treatment condition, and play an important role in improving the mechanical properties of the alloys. In this study, the morphology and crystallographic characteristics of the titanium silicides in the Ti-Fe-Si alloy system were studied. Three types of silicides were found in the alloys; (1) interconnected chain-like silicides at grain boundary, (2) coarse silicides over im, (3) fine silicides smaller than 0.2m. Ti3Si was dominant in cast + HIP condition while Ti5Si3 was dominant in as-cast state. It is recognized that $Ti_5Si_3$$\rightarrow$$Ti_3Si$ transition occurred by the peritectoid reaction and it may be promoted by the pressure during HIP. However, in the case of the fine silicides, $Ti_3Si$ and $Ti_5Si_3$ were found simultaneously even after HIP. Such a fine silicide was found to have a crystallographic orientation relationship with matrix.

• 한국재료학회:학술대회논문집
• /
• 한국재료학회 2007년도 춘계학술발표대회 및 제12회 신소재 심포지엄
• /
• pp.37.1-37.1
• /
• 2007

• 한국표면공학회:학술대회논문집
• /
• 한국표면공학회 2003년도 춘계학술발표회 초록집
• /
• pp.76-77
• /
• 2003

• 한국자동차공학회논문집
• /
• 제13권3호
• /
• pp.117-122
• /
• 2005

Titanium alloy has widely been used as material for glasses frame parts because it has high specific strength. It is also light and harmless to human body. However, we have little design data about the mechanical properties such as the creep behaviors of the alloy. Therefore, in this study, creep tests under four constant stress conditions have been conducted with four different temperature conditions. A series of creep tests had been performed to get the basic design data and life prediction of titanium products and we have gotten the following results. First, the stress exponents decrease as the test temperatures increased. Secondly, the creep activation energy gradually decrease as the stresses became bigger. Thirdly, the constant of Larson-Miller parameter on this alloy was estimated as about 2.5. Finally, the fractographs at the creep rupture showed the ductile fracture due to the intergranullar rupture and some dimples.

• 한국자동차공학회논문집
• /
• 제13권1호
• /
• pp.153-158
• /
• 2005

Titanium alloy has widely been used as material for automotive parts because it has high specific strength. It is also light and harmless to human body. But, we have little design data about the creep behaviors of the alloy. Therefore, in this study, creep tests under four constant stress conditions have been conducted with low different temperature conditions. A series of creep tests had been performed to get the basic design data and life prediction of titanium products and we have gotten the fallowing results. First, the stress exponents decrease as the test temperatures increased. Secondly, the creep activation energy gradually decrease as the stresses became bigger. Thirdly, the constant of Larson-Miller parameter on this alloy was estimated as about 7.5. And for the last, the fractographs at the creep rupture showed the ductile fracture due to the intergranullar rupture.

• 한국기계가공학회지
• /
• 제21권6호
• /
• pp.81-88
• /
• 2022

Titanium alloy (Ti-6Al-4V) has excellent mechanical properties and high specific strength; therefore, it is widely used in aerospace, automobile, defense, engine parts, and bio fields. Particularly in the aerospace field, as it has a low specific gravity and rigidity, it is used for the purpose of increasing energy efficiency through weight reduction of parts, and most have a thin-walled structure. However, it is extremely difficult to machine thin-walled shapes owing to vibration and deformation. In the case of thin-walled structures, the cutting forces and vibrations rapidly increase depending on the cutting conditions, significantly affecting the surface integrity and tool life. In this study, machining experiments on thin-wall milling of a titanium alloy (Ti-6Al-4V) were conducted for each experimental condition with different axial depths of cut, radial depth of cut, and machining sequence. The machining characteristics were analyzed, and an effective machining method was derived by a comprehensive analysis of the machined surface conditions and cutting signals.