• Korean Chemical Engineering Research
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• v.50 no.1
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• pp.118-127
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• 2012

TiN or Ti/TiN was coated on stainless steel as bipolar plate in polymer electrolyte membrane fuel cells (PEMFCs) to improve their corrosion resistance and electric conductivity, and their properties were examined under fuel cell operating condition. After 200 hours operation, the behaviors for the corrosion, crack and dissolution of coating layer were investigated by various techniques. The corrosion and exfoliation of coating layer were considerably generated except for SUS316L-Ti/TiN after fuel cell operation even if the electric conductivity and corrosion resistance of coated stainless steel bipolar plates were improved. The adoption of Ti layer between TiN layer and the surface of stainless steel enhanced the adhesion of TiN layer and decreased the possibility of corrosion by the increase of coating layer.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.3
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• pp.1253-1258
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• 2014

The tribological properties of TiC, TiN and TiC/TiN coatings on steels prepared by the cathodic-arc (CA) ion plating technique were investigated. Experiments were carried out on a tribo-test machine using a Falex journal V block system. The friction and wear characteristics of the coatings were determined by varying the applied load and sliding speed. The TiC, TiN and TiC/TiN coatings markedly increased the tribological characteristics of the surface. As far as a single layer coating was concerned, TiN goes better results than TiC. However, the TiC/TiN multilayer coating performed better than either single layer coating. The major factor in the improved performance of the multilayer coating was the role of TiC in improving the adhesion between the external TiN layer and the substrate steel.

• Journal of the Korean Society for Nondestructive Testing
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• v.26 no.1
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• pp.7-11
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• 2006

Since ceramic layers coated on machinery components inevitably experience the changes in their properties it is necessary to evaluate the characteristics of ceramic coating layers nondestructively for a reliable use of coated components and 4heir remaining life prediction. To address such a need, in the present study, an ultrasonic backward radiation technique is applied to investigate the characteristics of leaky Rayleigh surface waves propagating through the very thin TiN ceramic layers coated on AISI 1045 steel or austenitic 304 steel substrate with three different conditions of surface roughness, coating layer thickness and wear condition. In the experiments performed in the present work, the peak angle and the peak amplitude of ultrasonic backward radiation profile varied sensitively according to three specimen preparation renditions. in fact, this result demonstrates a high possibility of the ultrasonic backward radiation as an effective tool for the nondestructive characterization of the resting layers even in such a thin regime.

• Journal of Ocean Engineering and Technology
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• v.11 no.4
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• pp.49-60
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• 1997

This paper deals with the effect of coating layer on the fatigue strength of TiN coated 1Cr-1Mo-0.25V steel prepared by using the arc ion plating (AIP) process, in which it was characterized by the presence of extractor grid (ion filter). The rotary bending fatigue tests were carried out under room air conditions, and the fatigue crack initiation and growth bwhavior were observed by using plastic replica method. As experimental results, it was found that the obvious improvement of fatigue life at lower stress region was confirmed in TiN coated specimen processed with ion filter. It was also exlained that the increase of fatigue life in the case of an improved AIP process with ion filter was attributed to the retardation of crack initiation of the substrate surface due to hard coating layer, more densly formed with the reduced size and density of droplets.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.10a
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• pp.178-181
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• 2005

Quaternary Ti-Si-C-N coatings were deposited on WC-Co substrates by a hybrid coating system of arc ion plating (AIP) and sputtering techniques using Ti and Si targets, in an $Ar/N_2/CH_4$ gaseous mixture. The crystallinity, bending status, and microstructure of the Ti-Si-C-N coatings were measured by X-ray diffractometer (XRD) and X-ray photoelectron spectroscope (XPS), The micro-hardness of Ti(C,N) and Ti-Si-N coatings were about 30 and 40 GPa, respectively. As the Si was incorporated into Ti(C,N) coatings, the Ti-Si-C-N coatings having Si content of $8.9\;at.\%$ showed the maximum hardness value of about 55 GPa. In this work, the microstructure and mechanical properties of Ti-Si-C-N coatings were systematically investigated.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.9 no.2
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• pp.40-46
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• 2010

The purpose of this study is to show the friction and wear characteristics on the vapor deposited coating layers on the SCM415 steel. In this research, frictional wear characteristic of coating materials such as TiAlN+WC/C Multilayer Coating was investigated under room temperature, normal air pressure and nothing lubricating condition. Therefore this study carried out research on the friction coefficient, micro hardness(Hv), roughness, EPMA on the vapor deposited coating layers on the SCM415 steel. As the wear experimental result, the coefficient of friction decreased according to experimental load increases.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2015.05a
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• pp.170-170
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• 2015

아크이온플레이팅(AIP)을 이용하여 SKD61강에 TiN 및 TiAlN을 증착함으로써 내산화성 및 아연증기와의 반응을 억제할 수 있었으며, 도금두께 제어를 위한 에어나이프의 수명개선 및 생산성향상에 매우 중요한 요인으로 판단되었다.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2003.10a
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• pp.89-94
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• 2003

Hard coatings are known to improve the performance of cutting tools in aggressive machining applications, such as high speed machining. New superhard Ti-Al-Si-W films, characterized by a nanocomposite nano-sized (Ti,Al,Si)N crystallites embedded in amorphous $Si_3 N_4$ matrix, could be successfully synthesized on WC-Co substrates by a hybrid coating system of arc ion plating(AIP) and sputtering method. The hardness of Ti-Al-Si-N film increased with incorporation of Si, and had the maximum value ~50 GPa at the Si content of 9 at.%, respectively. And the X-ray diffraction patterns of Ti-Al-Si-N films with various Si content is investigated. In this study, Ti-Al-Si-N coatings were applied to end-mill tools made of WC-Co material by a hybrid coating system. Cutting tests fir the high-hardened material (STD11,$H_R$)C62 and their performances in high speed cutting conditions were studied. Also, the tool wear and tool lift of Ti-Al-Si-N with various si(6, 9, 19) contents were measured.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.10a
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• pp.50-50
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• 2003

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2007.04a
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• pp.136-138
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• 2007

최근 기계가공기술의 발달에 따라 내마모용 TiN 박막의 수요가 증가하였고, TiN박막은 내마모용으로 높은 경도 및 밀착력을 필요로 한다. TiN박막을 증착시키는 방법은 PVD, CVD 등 여러 가지가 있으나 본 연구에서 공구강 SKD 61기판 표면과 Radical Nitriding(RN) 처리된 SKD 61 기판에 arc ion plating(AIP)를 이용하여 TiN 박막을 증착시켜 표면경도를 향상시키고, 이 코팅층의 미세구조가 기계적 특성에 미치는 영향을 연구하였다. 그 결과 RN처리된 SKD61에서 코팅 두께가 많이 나왔고, 스크래치테스트 결과 접착력이 향상되었음을 알 수 있었다.