• Journal of Periodontal and Implant Science
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• v.26 no.1
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• pp.143-160
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• 1996

The purpose of this study was to evaluate the response in aspect of attachment and growth rate of osteoblasts and growth rate of osteoblasts and human gingival fibroblasts to the commercially pure titanium(CP titanium)and titanium alloy(Ti-6AI-4V) that are used widely as implant materials, and to obtain the basic information to ideal implant materials. In the studly, commercially pure titanium in first test group, titanium alloy(Ti-6AI-4V) in second test group, cobalt-chrome-molybdenum alloy(Co-Cr-Mo alloy) in positive control group, and tissue culture polystyrene plate in negative control group were used. The results of this study were as follows. 1. Bone marrow cells cultured on CP titanium and Ti-6Al-4V showed significantly greater attachment and growth rate(p(0.05) compared to Co-Cr-Mo alloy in each time. 2. There were no significant differences(p>0.05) in attachment and growth rate of bone marrow cells cultured on CP titanium and Ti-6AI-4V or tissue culture plate. 3. Most bone marrow cells cultured on CP titanium, Ti-6Al-4V and tissue culture plate were attached well to each substratum in first 2days, and then, grew at higher growth rate. On the other hand, some cells cultured on Co-Cr-Mo alloy failed to attach in first 2 days, and then, attached cells grew at lower growth rate than other groups. 4. Attachment and growth rates of gingival fibroblasts cultured on CP titanium and Ti-6Al-4V showed no significant differences(p>0.05) compared to Co-Cr-Mo alloy in 2 days, but significantly greater increase(p<0.05) in 5 and 9 days. 5. There were no significantly differences(p>0.05) between growth rates on gingival fibroblasts cultured on CP titanium, Ti-6Al-4V and tissue culture plate in 2 and 5days, but a significant lower growth rate(p<0.05) on CP titanium and Ti-6Al-4V versus tissue culture plate. 6. Some gingival fibroblasts cultured on all specimen groups failed to attach, but attached cells grew well, especially on CP titanium, Ti-GAl-4V and tissue culture plate. 7. There were no significant differences(P>0.05) between growth rates of both bone marrow cells and gingival fibroblasts cultured on CP titanium and Ti-6AI-4V. As a result of this study, both commercially pure titanium and Ti-6AI-4V showed excellent biocompatibility and there was no significant difference in the cellular response to the both metals. Bone marrow cells cultured on each substratum showed significantly greater growth rate and responded sensitively to cytotoxic effects of metal surfaces compared to gingival fibroblasts. Considering cell response to the substrate, it was likely that the composition itself of titanium metals have no significant effect on the biocompatibility. Further study need to be done to evaluate the influence of surface characteristics on cellular responses.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2009.10a
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• pp.507-508
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• 2009

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.299-302
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• 2003

The interface heat transfer coefficient was measured for non-isothermal bulk forming of Ti-6Al-4V. FE analysis and experiments were conducted. Equipment consisting of AISI H13 die was instrumented with thermocouples located at sub-surface of the bottom die. Die temperature changes were investigated in related to the process variables such as reduction, lubricant and initial die temperature. The calibration approach based on heat conduction and FE analysis using an inverse algorithm were used to evaluate the interface heat transfer between graphite-lubricated die and glass-coated workpiece. The coefficients determined determined were affected mainly by the contact pressure. The validation of the coefficients was made by the comparison between experimental data and FE analysis results.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.347-350
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• 2003

The metal forming behavior and defect formation in Ti-6Al-4V tube during hot backward extrusion were investigated. To predict the forming-defects such as shear band, inner cracks or surface cracks, dynamic material model(DMM) including Ziegler's instability criterion and modified Cockcroft-Latham fracture criterion(C-L model) were used. These models were coupled to the internal variables generated from FE analysis. The chilling effect and friction indicated a great influence on the deformation mode of the tube and the formation of surface cracks. The simulation results for the backward extrusion were compared with the experimental observations.

• Korean Journal of Materials Research
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• v.12 no.8
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• pp.669-675
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• 2002

CrN film coated by AIP method, improved the mechanical properties (Hardness, Roughness, wear and fatigue) of Ti-6Al-4V alloy. The properties were studied using GXRD, XPS, Hardness, Roughness, wear and fatigue testers. CrN thin film thickness was about 7.5$\mu\textrm{m}$ and grew with (111) orientation. Hardness of CrN thin film was very high (Hv 1390) and roughness of the surface layer was greatly improved (Ra=0.063$\mu\textrm{m}$) compared with matrix alloy (Ra=0.321$\mu\textrm{m}$). Such changes of hardness and roughness could be contributed to improving the wear resistance and fatigue life. Striation like pattern with dimples and voids, a typical fatigue fracture mode, was observed throughout the specimen.

• Journal of the Korea Institute of Military Science and Technology
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• v.3 no.1
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• pp.231-236
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• 2000

The wall thickness of the Ti-6Al-4V Large-Diameter Seamless Tube, which is supposed to be a very important parameter in a system design, was measured during $360^{\circ}$ cold bending processes. The factors or processes affecting the wall thickness include 1) primary bending, 2)secondary or finishing step of the $360^{\circ}$ bending, 3)cleaning processes in CERO TRUTM(CT)process. But thinning effects of the wall thickness during the cleaning processes are negligible compared to those during the formers. The variations in the percentages of the change in wall thickness were found to be from -14% to +16%.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.03a
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• pp.175-178
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• 1997

A modified Mukerjee's model considering the microstructural evolution was developed to study the superplastic bulge forming process of Ti-6Al-4V alloy. Through the microstructual observation after deformation, it was found that the grain growth rate of uniaxially tested specimens was different from that of biaxially deformed specimens. From this result, bulge forming experiments with and without back pressure were performed to examine the grain growth behavior and to compare the results of biaxial test with those of triaxial test. Good agreement between the prediction by a modified Mukerjee's model and the experimental measurements was obtained for bulge profile and thickness distribution.

• Journal of Powder Materials
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• v.14 no.1 s.60
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• pp.32-37
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• 2007

Using spark plasma sintering process (SPS), Ti-6Al-4V alloy powders were successfully consolidated without any contamination happened due to reaction between the alloy powders and graphite mold. Variation of microstructure and mechanical properties were investigated as a function of SPS temperature and time. Compared with hot isostatic pressing (HIP), the sintering time and temperature could be lowered to be 10 min. and $900^{\circ}C$, respectively. At the SPS condition, UTS and elongation were about 890 MPa and 24%, respectively. Considering the density of 98.5% and elongation of 24%, further improving the tensile strength would obtain by increasing the SPS pressure.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1997.10a
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• pp.202-209
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• 1997

The mechanical properties of Ti-6Al-4V greatly vary for changes of microstructures. Therefore, when manufacturing components with this material, it is important to understand the influence of process parameters to the resulting microstructures. In the present investgation, it was attempted to relate the process parameters with the microstructures in a hot forged Ti-6Al-4V disk. The investigation was carried out by a rigid thermo-viscoplastic FEM analysis, flow stress measurements and microstructure studies. It was found that the dynamic recrystallization would hardly occur in this material and that variations of strain, strain rate and temperature of several locations in the disk were below the assumed dynamic recrystallization zone. These findings confirmed the experimental obervations that the microstructures in the disk were only deformed without being recrystallized.

• Journal of Advanced Marine Engineering and Technology
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• v.24 no.6
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• pp.70-77
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• 2000

In this paper, the effect of solution and age heat treatment to the corrosion behavior for the Ti-6Al-4V alloy were studied by cyclic polarization methods. Ti-6Al-4V was solution heat treated at $1,066^{\circ}C$ and $966^{\circ}C$ for 5 hours, and followed by age heat treated at $650^{\circ}C$, $600^{\circ}C$ and $550^{\circ}C$ with 1, 2, 4, 8 and 16 hours under vacuum environment. Test solution was 3.5% NaCl with temperature $25^{\circ}C$. The obtained results were as follows: 1. Base metal was exhibited higher electrical charge than that of solution and aged material. With decrease of solution-treatment temperature from 1066 to $966^{\circ}C$, the electrical charge was increased due to softening of micro structure. 2. The corrosion resistance of specimen that solution treated at $966^{\circ}C$ for 5 hours and age heat treated at 650, 660 and $550^{\circ}C$ were increased with increase of aging time to 4, 8 and 16 hours respectively, and then decreased. 3. In case of 316L stainless steel, measured charge and corrosion potential was 0.0627 coulomb and -614 mV respectively. Corrosion resistance of Ti-6Al-4V was higher than that of 316L.