• Title/Summary/Keyword: Three-step Pressure

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Effects of pressure during the synthesis of petroleum pitch precursors in open and closed systems

  • Choi, Jong-Eun;Ko, Seunghyun;Kim, Jong Gu;Jeon, Young-Pyo
    • Carbon letters
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    • v.25
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    • pp.95-102
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    • 2018
  • We examined the pressure effects on petroleum pitch synthesis by using open and closed reaction systems. The pressure effects that occur during the pitch synthesis were investigated in three pressure systems: a closed system of high pressure and two open systems under either an atmosphere or vacuum. A thermal reaction in the closed system led to the high product yield of a pitch by suppressing the release of light components in pyrolysis fuel oil. Atmospheric treatment mainly enhanced the polymerization degree of the pitch via condensation and a polymerization reaction. Vacuum treatment results in a softening point increase due to the removal of components with low molecular weights. To utilize such characteristic effects of system pressure during pitch preparations, we proposed a method for synthesizing cost-competitive pitch precursors for carbon materials. The first step is to increase product yield by using a closed system; the second step is to increase the degree of polymerization toward the desired molecular distribution, followed by the use of vacuum treatment to adjust softening points. Thus, we obtained an experimental quinoline insolubles-free pitch of product yield over 45% with softening points of approximately $130^{\circ}C$. The proposed method shows the possibility to prepare cost-competitive pitch precursors for carbon materials by enhancing product yield and other properties.

Effective Porosity Variation of Cement Samples According to Vacuum Pressure and Time (진공의 압력과 시간을 달리할 때 시멘트시험편의 유효공극률 변화)

  • Lee, Sang Kyu;Lee, Tae Jong;Kim, Hyoung Chan
    • Geophysics and Geophysical Exploration
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    • v.15 no.4
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    • pp.163-176
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    • 2012
  • Effective porosity has been measured for cement specimen as a function of vacuum time and pressure in the vacuum saturation process. Six cement specimen are used; three of them are made of the same ratio of cement and sand, the other three are 100% cement mortar, of which average porosity is about 25% and 40%, respectively. Using the 6 samples, measured effective porosities are compared and examined with 5 different vacuum pressures (2, 4, 6, 8, 10 torr) and times (20, 40, 60, 80, 100 minute), respectively. Comparing measured effective porosity from experiments when vacuum time varies from 100 minute to 20 minute with 20 minute step and vacuum pressure is fixed to 10, 6, and 2 torr, average deviation decreases as 0.6, 0.5, and 0.2% respectively. Comparing measured effective porosity from experiments when vacuum pressure varies from 2 torr to 10 torr with 2 torr step and vacuum time is fixed to 100, 60, and 20 minute, average deviation increases as vacuum time decreases. These results can be a background of suggested method of ISRM that describes the vacuum time longer than 60 minute and vacuum pressure higher than 6 torr. In this study, only qualitative discussion can be possible for the effects on the effective porosity by decreasing 20 minute vacuuming time at the same pressure or by decreasing 2 torr of vacuum pressure at the same vacuum time. This is because the sample could not reached to perfectly dried condition even though the sample were dried at $105^{\circ}C$ and following the ISRM suggested method, so that initial water content could not be the same at each experiment.

Preliminary Design Program Development for Aircraft Gas Turbine Combustors : Part 1 - Combustor Sizing (항공용 가스터빈 연소기 기본 설계 프로그램 개발 : Part 1 - 연소기 크기 결정)

  • Kim, Daesik;Ryu, Gyong Won;Hwang, Ki Young;Min, Seong Ki
    • Journal of the Korean Society of Combustion
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    • v.18 no.3
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    • pp.54-60
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    • 2013
  • This paper shows a general development process for aircraft gas turbine combustors. As a first step for developing the preliminary combustor design program, several combustor sizing methodologies using reference area concepts are reviewed. There are three ways to determine the reference area; 1) combustion efficiency approach, 2) pressure loss approach, 3) velocity assumption approach. The current study shows the comparisons of the calculated results of combustor reference values from the pressure loss and velocity assumption approaches. Further works are required to add iterative steps in the program using more reasonable values of pressure loss and velocities, and to evaluate the sizing results using data for actual combustor performance and sizes.

Hydrodynamic Pressure and Shear Stress in Chemical Mechanical Polishing (화학기계적연마 공정의 윤활역학적 압력 및 전단응력 분포 해석)

  • 조철호;박상신;안유민
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.1
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    • pp.179-184
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    • 2000
  • Chemical Mechanical Polishing (CMP) refers to a material removal process done by rubbing a work piece against a polishing pad under load in the presence of chemically active and abrasive containing slurry. CMP process is a combination of chemical dissolution and mechanical action. The mechanical action of CMP involves hydrodynamic behavior. The liquid slurry is trapped between the work piece and pad forming a hydrodynamic film. For the first step to understand material removal mechanism of the CMP process, the hydrodynamic analysis is done with semiconductor wafer. Three-dimensional Reynolds equation is applied to get pressure distribution of the slurry film. Shear stress distributions on the wafer surface are also analyzed

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Numerical Simulation of Wave Deformation due to a Submerged Structure with a Second-order VOF Method (2차 정확도 VOF기법을 활용한 수중구조물에 의한 파랑변화 예측)

  • Ha, Tae-Min;Cho, Yong-Sik
    • Journal of the Korean Society of Hazard Mitigation
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    • v.10 no.1
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    • pp.111-117
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    • 2010
  • A three-dimensional numerical model is employed to investigate wave deformation due to a submerged structure. The three-dimensional numerical model solves the spatially averaged Navier-Stokes equations for two-phase flows. The LES(large-eddy-simulation) approach is adopted to model the turbulence effect by using the Smagorinsky SGS(sub-grid scale) closure model. The two-step projection method is employed in the numerical solutions, aided by the Bi-CGSTAB technique to solve the pressure Poisson equation for the filtered pressure field. The second-order accurate VOF(volume-of-fluid) method is used to track the distorted and broken free surface. A simple linear wave is generated on a constant depth and compared with analytical solutions. The model is then applied to study wave deformation due to a submerged structure and the predicted results are compared with available laboratory measurements.

The study on the influence of contact pressure distribution on brake squeal analysis (브레이크 스퀼 해석에서 접촉압력분포의 영향에 관한 연구)

  • Lee, Ho-Gun;Son, Min-Hyuk;Seo, Young-Uk;Boo, Kwang-Seok;Kim, Heung-Seob
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2007.11a
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    • pp.1120-1124
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    • 2007
  • Recently in the automotive brake industry brake squeal noise has become one of the top automotive quality warranty issues. The contact pressure is used to predict friction coupling in the brake squeal analysis. The formulation of friction coupling has performed by nonlinear static analysis prior to the complex eigenvalue analysis. This paper proposes a validation methodology of squeal analysis using modal testing and contact analysis and examines the effect of predicted contact pressure that leads to the discrepancy between unstable complex mode and squeal frequency. This studies compose a three step validation process : examining the modal characteristics of component and assembly loaded contact pressure using modal testing and FEM analysis and verifying the contact pressure distribution using nonlinear static analysis and experiment. Finally, the unstable modes from complex eigenvalue analysis and realistic squeal frequency from the noise dynamometer are investigated.

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An Empirical Study on the Characteristics of Pore Water Pressure Reaction in Colluvium Model (붕적층내의 간극수압 반응에 관한 실험적 연구)

  • 정두영;최길렬
    • Geotechnical Engineering
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    • v.8 no.2
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    • pp.59-70
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    • 1992
  • This work is to study experimentally the measurment of pore air pressure according to rainfall in colluvium model and the characteristics of pore water pressure according to increasement of artesian ground water head. After modeling a geological feature of the Tertiary formation, the experiment was performed about sixty times on three kinds of soil. This experimental results showed the variation of pore water and pore air pressures with time, the change of void ratio and appling pressure head in the nonsaturated soil. It can be also expressed by the final pore water and the air reaction ratios and then formularizing the relationship between the permeability coefficient and the void ratio. In the results of this experiment, the patterns of the pore water pressure reaction are classified by the step-type and the wave-type, and the time-lag to reach final point of pore water pressure is in order sand, sandy silt and clayey sand.

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Three-Dimensional Numerical Analysis for Detonation Propagating in Circular Tube

  • Sugiyama, Yuta;Matsuo, Akiko
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.03a
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    • pp.364-370
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    • 2008
  • Spinning detonations propagating in a circular tube were numerically investigated with a one-step irreversible reaction model governed by Arrhenius kinetics. The time evolution of the simulation results was utilized to reveal the propagation mechanism of single-headed spinning detonation. The track angle of soot record on the tube wall was numerically reproduced with various levels of activation energy, and the simulated unique angle was the same as that of the previous reports. The maximum pressure histories of the shock front on the tube wall showed stable and unstable pitch modes for the lower and higher activation energies, respectively. The shock front shapes and the pressure profiles on the tube wall clarified the mechanisms of two modes. The maximum pressure history in the stable pitch remained nearly constant, and the single Mach leg existing on the shock front rotated at a constant speed. The high and low frequency pressure oscillations appeared in the unstable pitch due to the generation and decay of complex Mach interaction on the shock front shape. The high frequency oscillation was self-induced because the intensity of the transverse wave was changed during propagation in one cycle. The high frequency behavior was not always the same for each cycle, and therefore the low frequency oscillation was also induced in the pressure history.

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Stabilized finite element technique and its application for turbulent flow with high Reynolds number

  • Huang, Cheng;Yan, Bao;Zhou, Dai;Xu, Jinquan
    • Wind and Structures
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    • v.14 no.5
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    • pp.465-480
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    • 2011
  • In this paper, a stabilized large eddy simulation technique is developed to predict turbulent flow with high Reynolds number. Streamline Upwind Petrov-Galerkin (SUPG) stabilized method and three-step technique are both implemented for the finite element formulation of Smagorinsky sub-grid scale (SGS) model. Temporal discretization is performed using three-step technique with viscous term treated implicitly. And the pressure is computed from Poisson equation derived from the incompressible condition. Then two numerical examples of turbulent flow with high Reynolds number are discussed. One is lid driven flow at Re = $10^5$ in a triangular cavity, the other is turbulent flow past a square cylinder at Re = 22000. Results show that the present technique can effectively suppress the instabilities of turbulent flow caused by traditional FEM and well predict the unsteady flow even with coarse mesh.

A study on the performance improvement of the quality prediction neural network of injection molded products reflecting the process conditions and quality characteristics of molded products by process step based on multi-tasking learning structure (다중 작업 학습 구조 기반 공정단계별 공정조건 및 성형품의 품질 특성을 반영한 사출성형품 품질 예측 신경망의 성능 개선에 대한 연구)

  • Hyo-Eun Lee;Jun-Han Lee;Jong-Sun Kim;Gu-Young Cho
    • Design & Manufacturing
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    • v.17 no.4
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    • pp.72-78
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    • 2023
  • Injection molding is a process widely used in various industries because of its high production speed and ease of mass production during the plastic manufacturing process, and the product is molded by injecting molten plastic into the mold at high speed and pressure. Since process conditions such as resin and mold temperature mutually affect the process and the quality of the molded product, it is difficult to accurately predict quality through mathematical or statistical methods. Recently, studies to predict the quality of injection molded products by applying artificial neural networks, which are known to be very useful for analyzing nonlinear types of problems, are actively underway. In this study, structural optimization of neural networks was conducted by applying multi-task learning techniques according to the characteristics of the input and output parameters of the artificial neural network. A structure reflecting the characteristics of each process step was applied to the input parameters, and a structure reflecting the quality characteristics of the injection molded part was applied to the output parameters using multi-tasking learning. Building an artificial neural network to predict the three qualities (mass, diameter, height) of injection-molded product under six process conditions (melt temperature, mold temperature, injection speed, packing pressure, pacing time, cooling time) and comparing its performance with the existing neural network, we observed enhancements in prediction accuracy for mass, diameter, and height by approximately 69.38%, 24.87%, and 39.87%, respectively.