• 한국공작기계학회논문집
• /
• 제16권2호
• /
• pp.106-111
• /
• 2007

In this research work attempts were made to study the bonding of thermo-plastics with adhesives using solar radiation. In order to study the curing behaviour necessary experiments were conducted under varying conditions of temperature, exposure time and power of solar energy. The cured samples were then studied under the optical microscope before subjecting to tensile testing in order to study their mechanical properties of thermo-plastics. The fracture surfaces were further studied under the Scanning Electron Microscopy(SEM) in order to research the microstructural changes that are taken place during curing. In order to measure the performance of solar energy cured joints the parameters such as; bond strength, surface morphology, the microstructual changes, variation in properties of adhesives bonded joints are compared to that of specimen cured at ambient conditions and specimen cured using microwave techniques.

• Tribology and Lubricants
• /
• 제8권1호
• /
• pp.48-55
• /
• 1992

The friction characteristic of plastics (PTFE, Nylon, Acetal and phenolic) was studied on the lubricated condition with a pin on disk machine. Mineral oil without additive (base oil) and water were used as liquid lubricants at the controlled temperature. From the experimental work, it was found out that the coefficient of friction of plastics was controlled by the mechanical properities of plastic more than that of liquid for various load and temperature. Viscosity of liquid has affected on the friction only at low temperature under lighb load. Among the tested plastics, the coefficient of friction of PTFE was the lowest under light load and at low temperature while Nylon at medium load and temperature, and Acetal at heavy load and high temperature. The coefficient of friction of soft plastics like PTFE and Nylon were increased as the load and temperature were increased, while that of hard plastic (Acetal) was decreased and that of thermo setting plastic (phenolic) was mixed. Also for soft plastics, the coefficient of friction under heavy load was always higher than that under light load, while hard plastic was vice versa.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2003년도 추계학술대회 논문집 Vol.16
• /
• pp.235-238
• /
• 2003

Thermo-plastic has generally bad electrical characteristics at high temperature comparing to thermoset-plastics when the plastic apply to electrical power apparatus as an electrical insulator. To solve the problem, we study engineering plastics such as Polyamide and Polyphthalamide as a base resin. And filler of the engineering plastics is glass fiber. Electrical characteristics studied are permittivity, loss factor and breakdown strength according to temperature and frequency of measuring signal. Electrical characteristics of Polyphthalamide has good temperature and frequency dependency comparing to those of Polyamide.

• 한국정밀공학회지
• /
• 제26권7호
• /
• pp.99-104
• /
• 2009

Creep characteristic is an important failure mechanism when evaluating engineering materials that are soft as polymers or used as mechanical elements at high temperatures. One of the popular thermo-elastic plastics, Polyethylene(PE) which is used broadly for engineering purposes, as it has good properties and merits compared to other plastics, was studied for creep characteristic at various level of stresses and temperatures. From the experimental results, the creep limit of PE at room temperature is 75% of tensile strength. Also the creep limits decreased exponentially as the temperatures increased, up to 50% of the melting point. Also the secondary stage among the three creep stages was nonexistent nor was there any rupture failure which occurred for many metals.

• 한국정밀공학회지
• /
• 제26권6호
• /
• pp.42-49
• /
• 2009

The optical elements made of plastics are normally produced by mass production such as injection molding with use of precision dies and molds. It costs to prepare the dies and molds, and it is only justified to prepare such expensive dies and molds when the parts are massively produced. On the other hand, it is too expensive and inefficient when precision plastic parts are needed only in small quantities, such as a case of trial manufacturing of new products. An ultra-precision diamond cutting is one of promising processes to produce the precision plastic parts in such cases. But it is commonly believed that an ultra-precision cutting of plastics for optical components is very difficult, because they are thermo-plastic material. In the present research, an ultra-precision diamond cutting of polycarbonate (PC), that is one of typical optical materials, was tried by using elliptical vibration cutting method. It is experimentally proved that good optical surfaces were obtained by using elliptical vibration cutting in cases of grooving and flat surfaces. The maximum surface roughness of less than 60 nm in peak to valley value is acquired.

• 비파괴검사학회지
• /
• 제10권2호
• /
• pp.50-55
• /
• 1990

Flaws in GFRP(Glass Fiber Reinforced Plastics) were thermally detected using cholesteric liquid crystals. Presence of flaws changes the thermal conductivity of GFRP, and disturbs heat flow. When a uniform heat source is applied, the surface temperature of flawed region is different from that of sound region. The surface temperature distributions were measured by thermo-optic properties of liquid crystal. Since the colors of liquid crystal indicate temperature distribution of GFRP surface, the thermal disturbance by flaws could be detected. The locations of flaws in GFRP could be determined from the distribution of liquid crystal colors.

• 한국자원리싸이클링학회:학술대회논문집
• /
• 한국자원리싸이클링학회 2006년도 고분자리싸이클링 심포지엄
• /
• pp.39-54
• /
• 2006

폐플라스틱으로부터 만든 재생연료유의 연료특성 향상을 위하여 수첨 열분해 실험을 수행하였다. 주요 실험인자로 반응온도($300^{\circ}C{\sim}700^{\circ}C$), 촉매(알루미나-실리카, 활성탄, 제올라이트)를 선정하였고 이들이 액상 생성물의 인화점, 동점도, 고형물 함량에 미치는 영향을 조사하였다. $300^{\circ}C{\sim}400^{\circ}C$ 온도에서 수첨 열분해는 재생연료유의 연료특성을 개선하는 효과가 있었다. $500^{\circ}C$ 이상 온도에서는 열분해반응이 활발하게 진행되어 생성물의 인화점이 급격히 낮아졌다. 촉매를 도입하여 생성물의 인화점을 높일 수 있었는데 이는 촉매가 수첨반응을 활성화하였기 때문으로 사료된다. 동점도는 무촉매 반응에서 가장 낮은 값을, 제올라이트 촉매 반응에서 가장 높은 값을 보였다. 고형물 제거율은 모든 반응조건에서 70 % 이상이었다. 조사한 촉매들 중에서 활성탄이 재생연료유의 수첨 열분해 반응에 가장 안정적이며 높은 활성을 보였다.

• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2004년도 추계학술대회 논문집
• /
• pp.34-37
• /
• 2004

In the present research, a ultra-precision diamond cutting of thermo-plastic materials, polycarbonate (PC) and cyclic olefin polymer (COC), is carried out by applying a method named ultrasonic elliptical vibration cutting developed by the authors. It is experimentally proved that good optical surfaces are obtained by applying the elliptical vibration cutting in cases of machining of flat surfaces and grooves as compared with the conventional diamond cutting. The maximum surface roughness in peak to valley value obtained is less than 60 nm and 20 nm for PC and ZEONEX, respectively.

• Carbon letters
• /
• 제7권2호
• /
• pp.87-96
• /
• 2006

This paper describes the physical properties of filled Nylon6 composites resin with nano-sized carbon black particle and graphite nanofibers prepared by melt extrusion method. In improving adhesions between resin and fillers, the surface of the carbon filler materials were chemically modified by thermo-oxidative treatments and followed by treatments of silane coupling agent. Crystallization temperature and rate of crystallization increased with increases in filler concentration which would act as nuclei for crystallization. The silane treatments on the filler materials showed effect of reduction in crystallization temperature, possibly from enhancement in wetting property of the surface of the filler materials. Percolation transition phenomenon at which the volume resistivity was sharply decreased was observed above 9 wt% of carbon black and above 6 wt% of graphite nanofiber. The graphite nanofibers contributed to more effectively in an increase in electrical conductivity than carbon black did, on the other hand, the silane coupling agent negatively affected to the electrical conductivity due to the insulating property of the silane. Positive temperature coefficient (PTC) phenomenon, was observed as usual in other composites, that is, temperature increase results conductivity increase. The dispersity of the fillers were excellently approached by melt extrusion of co-rotational twin screw type and it could be illustrated by X-ray diffraction and SEM.

• Advanced Composite Materials
• /
• 제16권4호
• /
• pp.335-347
• /
• 2007

Green composites composed of long maize fibers and poly $\varepsilon$-caprolactone (PCL) biodegradable polyester matrix were manufactured by the thermo-mechanical processing termed as 'Sequential Molding and Forming Process' that was developed previously by the authors' research group. A variety of processing parameters such as fiber area fraction, molding temperature and forming pressure were systematically controlled and their influence on the tensile properties was investigated. It was revealed that both tensile strength and elastic modulus of the composites increase steadily depending on the increase in fiber area fraction, suggesting a general conformity to the rule of mixtures (ROM), particularly up to 55% fiber area fraction. The improvement in tensile properties was found to be closely related to the good interfacial adhesion between the fiber and polymer matrix, and was observed to be more pronounced under the optimum processing condition of $130^{\circ}C$ molding temperature and 10 MPa forming pressure. However, processing out of the optimum condition results in a deterioration in properties, mostly fiber and/or matrix degradation together with their interfacial defect as a consequence of the thermal or mechanical damages. On the basis of microstructural observation, the cause of strength degradation and its countermeasure to provide a feasible composite design are discussed in relation to the optimized process conditions.