• Title/Summary/Keyword: Tensile bond strength

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Effect of adhesive hydrophobicity on microtensile bond strength of low-shrinkage silorane resin to dentin (접착시스템의 소수성이 Low-shrinkage silorane resin과 상아질의 미세인장강도에 미치는 영향)

  • Cho, So-Yeun;Kang, Hyun-Young;Kim, Kyoung-A;Yu, Mi-Kyung;Lee, Kwang-Won
    • Restorative Dentistry and Endodontics
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    • v.36 no.4
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    • pp.280-289
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    • 2011
  • Objectives: The purpose of this study was to evaluate ${\mu}TBS$ (microtensile bond strength) of current dentin bonding adhesives which have different hydrophobicity with low-shrinkage silorane resin. Materials and Methods: Thirty-six human third molars were used. Middle dentin was exposed. The teeth were randomly assigned to nine experimental groups: Silorane self-etch adhesives (SS), SS + phosphoric acid etching (SS + pa), Adper easy bond (AE), AE + Silorane system bonding (AE + SSb), Clearfil SE bond (CSE), CSE + SSb, All-Bond 2 (AB2), AB2 + SSb, All-Bond 3 (AB3). After adhesive's were applied, the clinical crowns were restored with Filtek LS (3M ESPE). The 0.8 mm ${\times}$ 0.8 mm sticks were submitted to a tensile load using a Micro Tensile Tester (Bisco Inc.). Water sorption was measured to estimate hydrophobicity adhesives. Results: ${\mu}TBS$ of silorane resin to 5 adhesives: SS, 23.2 MPa; CSE, 19.4 MPa; AB3, 30.3 MPa; AB2 and AE, no bond. Additional layering of SSb: CSE + SSb, 26.2 MPa; AB2 + SSb, 33.9 MPa; AE + SSb, no bond. High value of ${\mu}TBS$ was related to cohesive failure. SS showed the lowest water sorption. AE showed the highest solubility. Conclusions: The hydrophobicity of adhesive increased, and silorane resin bond-strength was also increased. Additional hydrophobic adhesive layer did not increase the bond-strength to silorane resin except AB2 + SSb. All-Bond 3 showed similar ${\mu}TBS$ & water sorption with SS. By these facts, we could reach a conclusion that All-Bond 3 is a competitive adhesive which can replace the Silorane adhesive system.

Control of Tensile Behavior of Ultra-High Performance Concrete Through Artificial Flaws and Fiber Hybridization

  • Kang, Su-Tae;Lee, Kang-Seok;Choi, Jeong-Il;Lee, Yun;Felekoglu, Burak;Lee, Bang Yeon
    • International Journal of Concrete Structures and Materials
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    • v.10 no.sup3
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    • pp.33-41
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    • 2016
  • Ultra-high performance concrete (UHPC) is one of the most promising construction materials because it exhibits high performance, such as through high strength, high durability, and proper rheological properties. However, it has low tensile ductility compared with other normal strength grade high ductile fiber-reinforced cementitious composites. This paper presents an experimental study on the tensile behavior, including tensile ductility and crack patterns, of UHPC reinforced by hybrid steel and polyethylene fibers and incorporating plastic beads which have a very weak bond with a cementitious matrix. These beads behave as an artificial flaw under tensile loading. A series of experiments including density, compressive strength, and uniaxial tension tests were performed. Test results showed that the tensile behavior including tensile strain capacity and cracking pattern of UHPC investigated in this study can be controlled by fiber hybridization and artificial flaws.

THE EFFECTS OF SURFACE TREATMENT OF DENIAL NICKEL-CHROMIUM ALLOY ON TENSILE BOND STRENGTH (치과용 니켈-크롬합금에 대한 표면 처리가 인장접착강도에 미치는 영향)

  • Lee, Eun-Suk;Kwon, Oh-Won
    • The korean journal of orthodontics
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    • v.27 no.3 s.62
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    • pp.493-502
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    • 1997
  • This study was conducted to evaluate the tensile bond strength by bonding the dental bracket with Super-bond after treating the surface of dental Nickel-Chromium alloy with sandblasting, sandblasting & tin-plating, respectively, and tin-plating. 10 pieces of Nickel-Chromium alloys with brackets bonded with Super-bond without their surface treatment were sampled as a control group, 20 pieces of Nickel-Chromium alloy brackets bonded with Super-bond after treating them with sandblasting as group I, 20 pieces of Nickel-Chromium alloys tin-plated and bonded with Super-bond after sandblasting as group II, and then 20 pieces of alloys with brackets bonded with Super-bond after tin-plating as group III. The result of those examination and comparison is summarized as follows: 1. Group I showed the mean tensile bond strength of $14.41{\pm}2.24MPa$ which was highest among 4 groups, followed by group III($13.59{\pm}.51MPa$), group II($12.27{\pm}.45MPa$), and control group($10.50{\pm}1.57MPa$), respectively. However, it was shown that there was no statistically significant difference between group I and III, group III and II, and group II and control group(p>0.05). 2. The main failure pattern of those brackets showed that $70\%$ of the control group had an adhesive failure at the bracket-Superbond interface, and $30\%$ at the Nickel-Chromium alloy-Superbond interface, while other groups did the adhesive failure at the bracket-Superbond interface. 3. When examined under SEM, it was shown that adhesives were mostly attached to the surface of the Nickel-Chromium alloy for all groups while a considerable quantity of adhesives were attached to the bracket base. Then, those samples treated only with sandblasting showed the most even and remarkable roughness of their surface.

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EFFECT OF TEMPORARY CEMENT ON TENSILE BOND STRENGTH OF DENTIN BONDING AGENT (Temporary Cement가 상아질 접착제의 접착성능에 미치는 영향)

  • Chang, Heon-Soo;Cho, Kyeu-Zeung
    • Restorative Dentistry and Endodontics
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    • v.20 no.2
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    • pp.685-698
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    • 1995
  • This study was conducted to the effect of temporary cement on the adhesiveness of dentin bonding agent to dentin surface. One hundred freshly extracted bovine mandibular incisors were grinded to expose flat labial dentin surface. The dentin surfaces were temporarized with either eugenol-containing temporary cement(TemBond and Zinc Oxide Eugenol cement) or non-eugenol temporary cement(Nogenol and TempBond NE) for 7days, and then the temporarization was removed with surgical currette and the exposed dentin surfaces were water-rinsed. Bonding specimens were made by use of All-Bond 2 and Super-Bond C&B dentin bonding agent, and stored in $37^{\circ}C$ distilled water for 24hours. The tensile bond strenth and the cohesive failure rate were measured, and then the pretreated dentin surfaces which the temporary cement had been applied to and removed from and the fractured dentin surfaces after bonding test were examined under scanning electron microscope. The results were as follows : In case of bonding with All-Bond 2, tensile bond strength of each experimental group was lower than that of the control group(p<0.05), but there was no significant difference between the bond strengths of the control group and each experimental group in case of bonding with Super-Bond C&B(p>0.05). No significant difference between tensile bond strength of experimental group, whether temporary cement contains eugenol or not, was seen(p>0.05). In case of bonding with All-Bond 2, the control group showed cohesive-adhesive mixed failure mode and the experimental groups mainly showed adhesive failure mode, but in case of bonding with Super-Bond C&B, almost of the control and the experimental groups mainly showed cohesive failure mode. On SEM examination, all of the dentin specimens pretreated with either 10 % phosphoric acid or 10% citric acid after application of the temporary cements demonstrated remnants of temporary cement attached to dentin surface.

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Comparative Studies on Physical and Mechanical Properties of Domestic Wood-Based Panels (국산목질판상재료(國産木質板狀材料)의 물리적(物理的) 및 기술적성질(機械的性質)에 관(關)한 비교연구(比較硏究))

  • Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.18 no.2
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    • pp.67-78
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    • 1990
  • This study was performed to determine the characteristics of physical and mechanical properties of domestic wood based materials; plywood, particleboard, medium density fiberboard. Main items of tested properties were panel size, moisture content, water absorption, linear expansion and thickness swelling, glue bond shear strength, bending properties(stress at proportional limit, modulus of rupture. modulus of elasticity), tensile strength, screw holding strength, and internal bond as neccessary. the results were discussed mainly with Korean Standards. The obtained conclusions are as follows; 1. Length and width of 3mm thin plywood(3-ply) and 12mm thick plywood(7-ply) were satished with KS-standard, but thicknesses of these panels were not- passed tolerance limit except one of eight makers. 2. Length and width of particleboard and medium density fiberboard were greater than the tolerance limit value of KS standard, but the thicknesses of these panels were passed this value. 3. Moisture contents of 12mm thick and 3mm thin plywood were satisfied with KS-standard except one mill made 3mm thin plywood. 4. Moisture absortion of plywood was not passed tolerance limit of KS-standard but particleboard was satisfied with this standard value. 5. Dry and wet shear strengths in glue bond of 3mm thin plywood were not reached to KS-standard, but those of 12mm thick plywood were sufficiently satisfied with KS standrad. 6. Modulus of ruptures, parallel to grain and perpendicular to grain of plywood, and particleboard and medium density fiberboard were satisfied with KS-standard. 7. Tensile strengths, parallel to grain and perpendicular to grain of plywood were satisfied with allowance stress of US product standard PS 1-74. 8. Screw holding strength of particleboard was not reached to KS standard, but internal bond was satisfied with KS standard.

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Analytical model for flexural and shear strength of normal and high-strength concrete beams

  • Campione, Giuseppe
    • Structural Engineering and Mechanics
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    • v.78 no.2
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    • pp.199-207
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    • 2021
  • In the present paper, an analytical model is proposed to determine the flexural and shear strength of normal and high-strength reinforced concrete beams with longitudinal bars, in the presence of transverse stirrups. The model is based on evaluation of the resistance contribution due to beam and arch actions including interaction with stirrups. For the resistance contribution of the main bars in tension the residual bond adherence of steel bars, including the effect of stirrups and the crack spacing of R.C. beams, is considered. The compressive strength of the compressed arch is also verified by taking into account the biaxial state of stresses. The model was verified on the basis of experimental data available in the literature and it is able to include the following variables in the resistance provision: - geometrical percentage of steel bars; - depth-to-shear span ratio; - resistance of materials; - crack spacing; - tensile stress in main bars; - residual bond resistance including the presence of stirrups;- size effects. Finally, some of the more recent analytical expressions able to predict shear and flexural resistance of concrete beams are mentioned and a comparison is made with experimental data.

COMPARATIVE STUDY ON THE BOND STRENGTH OF CEMENTS BETWEEN PFM COPING AND VARIOUS CORES (도재전장관용 Coping과 수종 Core간의 시멘트 결합력에 관한 비교 연구)

  • Paik, Sung-Ki;Chang, Wan-Shik
    • The Journal of Korean Academy of Prosthodontics
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    • v.20 no.1
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    • pp.25-32
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    • 1982
  • An in vitro study was conducted to compare the bond strength of cements between Verabond coping and various cores. Fifty-four idential cores simulating maxillary central incisor prepared for PFM crowns were made. Eighteen samples were made with 20K cast gold, eighteen with Verabond, and eighteen with Adaptic. Samples were randomly divided into three groups, each consisting of six 20K cast gold, six verabond, and six Adaptic samples. The first group was cemented with zinc phosphate cement, the second group with poly-carboxylate cement, and the third group with glass ionomer cement. Constant finger pressure was applied for cementation. The sample were then stored at $37^{\circ}C$ in distilled water bath for 24 hours. The tensile strength test was performed on an Instron Universal test machine with crosshead speed of 0.05cm/min and the results compared statistically. Results of the study showed that: 1. A significant difference of bond strength was observed with different types of dental cements and core materials. 2. With gold core, zinc phosphate cement was stronger than both the polycarboxylate cement and glass ionomer cement, which did not differ in bond strength. 3. With base-metal core, zinc phosphate cement showed the highest bond strength and was followed by polycarboxylate cement and glass ionomer cement. 4. With composite resin core, zinc phosphate cement showed the highest bond strength and was followed by glass ionomer cement and polycarboxylate cement. 5. The base-metal core (Verabond core) privided the highest retention of all core materials.

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Fundamental Study on Development of Sealants used for WIM Sensor Installation (WIM 센서 설치에 적합한 실런트 개발을 위한 기초적인 연구)

  • Lim, Chisoo;Kim, Du-Byung;Kim, Yongjoo;Lee, Kanghun;Lee, Jaejun
    • International Journal of Highway Engineering
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    • v.19 no.2
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    • pp.17-24
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    • 2017
  • PURPOSES : This study aims to develop a sealant for use in the installation of Weigh-In-Motion (WIM) sensor for asphalt concrete or cement concrete pavements. METHODS : In order to investigate the properties of various sealants that were mixed with latex and carbon fiber, various test methods were adopted, such as bituminous bond strength test, softening point test, and cone penetration test. To evaluate moisture susceptibility, the BBS test was conducted under moist condition. The bond strength ratio (BSR) was calculated based on tensile strength ratio method. RESULTS : The sealant's properties significantly varied according to the amount of latex or carbon fiber. The usage of latex marginally enhanced the cone penetration test result, notwithstanding reduced asphalt content. This implies that the sealant will be proper cold temperature reason. Moreover, the addition of latex and carbon fiber evidently increased the softening point. This indicates that the tendency of the material to flow at elevated temperatures is encountered during service. With the addition of latex and carbon fiber, the moisture susceptibility measured with BSR improved marginally, while the bond strength under dry condition decreased marginally. Sealant F displays the highest bond strength and BSR under limited test conditions. CONCLUSIONS : According to the proportion of latex and carbon fiber mixed, properties of sealant, such as softening point, cone penetration, and BSR varied marginally. This indicates that the sealant has to be applied considering the environmental condition, to improve service life.

Analysis for Strength Estimation of Adhesive Joints (접착이음의 강도평가에 대한 해석)

  • 박성완;이장규
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2004.10a
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    • pp.98-107
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    • 2004
  • The objectives of this research are to establish the criteria of peel occurrence considering the shape of bond terminus and to compare the strength properties of some adhesive joints. The criteria of feel occurrence at the bond terminus was suggested. Peel loads of some adhesive joint(butt joint, T -shape specimen, single lap joint) were determined from tensile tests. Principal stress distributions of these joints were determined from finite element method analysis. Then, peel occurrence was estimated with intensity of stress singularity ' $K_{prin.}$' when the terminus shape was square, with average principal stress when the terminus shape was rounded. The conclusions are summarized as follows; (1) In the non-filleted model(e.g., butt joint, T-shape specimen), principal stress shows singularity at the bond terminus, intensity of stress(principal stress) singularity ' $K_{prin.}$&apso; can use as the criteria of peel occurrence at the bond terminus. (2) In the filleted model(e.g., single lap joint), principal stress doesn't show singularity at the bond terminus. Average principal stress can use as the criteria of peel occurrence at the bond terminus.'t show singularity at the bond terminus. Average principal stress can use as the criteria of peel occurrence at the bond terminus.

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Mechanical and durability properties of fluoropolymer modified cement mortar

  • Bansal, Prem Pal;Sidhu, Ramandeep
    • Structural Engineering and Mechanics
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    • v.63 no.3
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    • pp.317-327
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    • 2017
  • The addition of different types of polymers such as SBR, VAE, Acrylic, etc. in concrete and mortar leads to an increase in compressive, tensile and bond strength and decrease in permeability of polymer modified mortar (PMM) and concrete (PMC). The improvement in properties such as bond strength and impermeability makes PMM/PMC suitable for use as repair/retrofitting and water proofing material. In the present study effect of addition of fluoropolymer on the strength and permeability properties of mortar has been studied. In the cement mortar different percentages viz. 10, 20 and 30 percent of fluoropolymer by weight of cement was added. It has been observed that on addition of fluoropolymer in mortar the workability of mortar increases. In the present study all specimens were cast keeping the workability constant, i.e., flow value $105{\pm}5mm$, by changing the amount of water content in the mortar suitably. The specimens were cured for two different curing conditions. Firstly, these were cured wet for one day and then cured dry for 27 days. Secondly, specimens were cured wet for 7 days and then cured dry for 21 days. It has been observed that compressive strength and split tensile strength of specimens cured wet for 7 days and then cured dry for 21 days is 7-13 percent and 12-15 percent, respectively, higher than specimens cured one day dry and 27 days wet. The sorptivity of fluoropolymer modified mortar decreases by 88.56% and 91% for curing condtion one and two, respectively. However, It has been observed that on addition of 10 percent fluoropolymer both compressive and tensile strength decreases, but with the increase in percentage addition from 10 to 20 and 30 percent both the strengths starts increasing and becomes equal to that of the control specimen at 30 percent for both the curing conditions. It is further observed that percentage decrease in strength for second curing condition is relatively less as compared to the first curing condition. However, for both the curing conditions chloride ion permeability of polymer modified mortar becomes very low.