• Title/Summary/Keyword: TDU

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Geographical origin discrimination of Korean variety, Angelica gigas Nakai by using TDU (Thermal Desorption Unit)-GC/MS (TDU-GC/MS를 이용한 한국품종 참당귀 국산 판별 기법)

  • Lee, Mi-Na;Kim, Yoon-Suk;Kim, Won-Il;Kim, Jeong-Gyu;Kwon, Oh-Kyung
    • Journal of Applied Biological Chemistry
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    • v.63 no.1
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    • pp.29-33
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    • 2020
  • The objective of this study was to develop a fast and accurate method of variety discrimination and geographical discrimination origin of Korean angelica (Korean variety, Angelica gigas Nakai) by using TDU-GC/MS. Two peaks of decursin and decursinol, which are coumarin derivatives were identified in the range of Total Ion Chromatogram (TIC) RT 26.9-27.2 of the Korean angelica by GC/MS analysis at the time of condensation in a refrigerated condensation system after thermal desorption of sample extracts. In case of Chinese angelica (Chinese variety), ligustilide peak was detected at the RT 17.2. In order to investigate the difference of volatile components according to the geographical origin of Korean variety, the mass spectra were measured by TDU-GC/MS at the range of m/z 40-400 amu. The TIC of domestic cultivation and Chinese cultivation of the Korean variety, Angelica gigas Nakai showed the same tendency as a whole. However, in partial scans of TIC, two peaks detected at 15.54 and 16.05 of RT showed different peak patterns between Korean angelica (Korean variety) cultivated in Korea and in China. The ratio of Peak A (RT 15.54) and B (RT 16.05) was 0.0-0.2 for domestic cultivation and 0.5-2.8 for Chinese cultivation, confirming the possibility of discriminating origin by comparing the TIC peak pattern of TDU-GC/MS.

Accelerated Life Test and Analysis of Track Drive Unit for an Excavator (주행 구동 유니트의 가속 수명 시험 및 분석)

  • Lee Y.B.;Park J.H.
    • Transactions of The Korea Fluid Power Systems Society
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    • v.2 no.2
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    • pp.1-7
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    • 2005
  • For the reliability evaluation of the track drive unit(TDU), firstly, we analyzed the major failure modes through FMEA(failure mode & effects analysis), FTA(failure tree analysis), and 2-stage QFD(quality function deployment), and then quantitatively determined the priority order of test items. The Minitab analysis was also performed for prediction of life distribution and parameters of TDU by use of field failure data collected from 430 excavators for two years. In addition, we converted the fluctuation load in field conditions into the equivalent load, and for evaluation of the accelerated lift by the cumulative fatigues, the equivalent load is again divided into the fluctuation load by reference of test time. And then, by use of the test method in this paper, the acceleration factor(AF) of needle bearing inside planetary gear which is the most weakly designed part of TDU is achieved as 5.3. This paper presents the quantitative selection method of test items for reliability evaluation, the determination method of the accelerated life test time, and the method of non-failure test time based on a few of samples. And, we proved the propriety of the proposed methods by experiments using a TDU for a 30 ton excavator.

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High accuracy online 3D-reconstruction by multiple cameras

  • Oota, Yoshikazu;Pan, Yaodong;Furuta, Katuhisa
    • 제어로봇시스템학회:학술대회논문집
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    • 2005.06a
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    • pp.1749-1752
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    • 2005
  • For online high accurate reconstruction of an object from an visual information, a linear reconstruction method for multiple images is popular. Basically this method needs many cameras or many different screen shots from different view points. This method, however, has the benefit of less calculation and is adequate for a real time application by comparing other popular method. In this paper, online reconstruction system using more than three cameras is treated. An evaluation method of cameras' position, and of the number is derived for the linear reconstruction method. To decrease errors that are caused from skew of lens, positional error between corresponding points is taken into consideration on the evaluation. The proposed evaluation method enables estimation of the adequate number of cameras and then of feasible view locations. Additionally, repeating search of epipolar lines enables estimation of the hidden point. Comparing with result of an average error analysis, it was confirmed that the proposed methods works effectively.

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Overview of Human Adaptive Mechatronics and Assist-control to Enhance Human's Proficiency

  • Suzuki, Satoshi;Furuta, Katsuhisa;Harashima, Fumio
    • 제어로봇시스템학회:학술대회논문집
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    • 2005.06a
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    • pp.1759-1764
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    • 2005
  • Human Adaptive Mechatronics(HAM) is a new concept which was proposed in our university's research project sponsored by Japanese Ministry of Education, Sports, Culture, Science and Technology(MEXT), and is defined as "intelligent mechanical systems that adapt themselves to the user's skill under various environments, assist to improve the user's skill, and assist the human-machine system to achieve best performance". In this paper, the concept and key-items of HAM are mentioned. And the control strategy to realize a HAM human-machine system is explained in the case of physical-interface system, i.e. haptic system. The proposed assist-control of a force-feedback type haptic system includes online estimation of a operator's control characteristics, and a `force assist' function implemented as a change in the support ratio according to the identified skill level. We developed a HAM-haptic device test system, executed evaluation experiments with this apparatus, and analyzed the measured data. It was confirmed that the operator's skill could be estimated and that operator's performance was enhanced by the assist-control.

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Calibration Methods for the Gas Chromatographic Analysis of ppt-level Hydrogen Sulfide (H2) in Air (환경 대기 중 ppt 수준의 황화수소 분석을 위한 GC 방식의 검량 기법에 대한 연구)

  • 김기현;오상인;최여진;최규훈;주도원
    • Journal of Korean Society for Atmospheric Environment
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    • v.19 no.6
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    • pp.679-687
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    • 2003
  • In this study, we investigated the analytical techniques to quantify the ambient concentration of hydrogen sulfide (H$_2$S) in air at ppt concentration level. For this purpose, an on-line GC analytical system equipped with both pulsed-flame photometric detector (PFPD) and thermal desorption unit (TDU) was investigated by collecting ambient air samples. The results of our study generally indicated that calibration conditions of GC system is highly sensitive to affect the accuracy of the analytical technique. Most importantly. we found that the use of different matrices in the the preparation stage of working standards was sensitive to control the overall performance of this technique. The calibration of our analytical system was tested by the two types of working standard (prepared by mixing either with high purity $N_2$ or with the ambient air). According to this test, the latter represented more efficiently the detecting conditions of actual air samples. The peak occurrence patterns of both air samples and standards (prepared by mixing with ambient air) were altered in a similar manner as the function of the loaded volume; however, it was not the case for the $N_2$-mixed standards. Results of our study suggest that detection of H$_2$S is highly different from other sulfides and that its quantification requires minimiaing interfering effects of non -pure substance (like water vapor) and (either sorptive or destructive) loss effects.

Near-infrared Spectroscopy and an Example of HAM Study;Brain Activation in the Development of Drawing Skills

  • Kobayashi, Harumi;Yasuda, Tetsuya;Suzuki, Satoshi;Takase, Hiroki
    • 제어로봇시스템학회:학술대회논문집
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    • 2005.06a
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    • pp.1745-1748
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    • 2005
  • Near-infrared spectroscopy (NIRS) can be used to monitor brain activation by measuring changes in the concentration of oxy- and deoxy-hemoglobin (Hb) by their different spectra in the near-infrared range. Because NIRS is a noninvasive, highly flexible and portable device, it is very suitable to study brain activation when a human repeatedly performs a manipulative task, and possibly provides useful information to construct human adaptive mechatronics (HAM). There is some evidence that the dorsolateral prefrontal cortex (DLPFC) plays a major role in working memory and it is proposed that the use of working memory decreases as a human develops manipulative skills. In the present study, we investigated the activation of the dorsolateral prefrontal cortex (DLPFC) of the brain in Brodmann's areas 9 and 46 in drawing tasks to examine whether NIRS can measure the changes of DLPFC activation as a human develops manipulative skills. Subjects performed a mirror image drawing task and a square drawing task by ones' left hands. In the mirror image task the subject drew following a star shape based on a mirror image of it, but square drawing did not involve mirror image and was estimated to be simpler. The changes of the concentration of oxy-Hb was higher in the mirror image drawing than the square drawing in most subjects. The changes of oxy-Hb decreased as the subject repeated the drawing task in most subjects. In conclusion, The activation of DLPFC measured by NIRS can reflect the brain activity in the development of manipulative skills.

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Changes in the gas chromatographic sensitivity with its analytical setting: Comparison of TDU and loop-injection system for the analysis of sulfur compounds (GC 분석 시스템의 설정과 그에 따른 감도의 차이: 열탈착 방식 대비 루프주입방식에 의한 황성분의 분석)

  • Kim, Ki-Hyun;Choi, Y.J.;Kim, S.C.
    • Analytical Science and Technology
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    • v.18 no.1
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    • pp.66-73
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    • 2005
  • In this study, we investigated the gas chromatography (GC) and pulsed flame photometric detection (PFPD) system for the analysis of four major reduced S compounds including hydrogen sulfide ($H_2S$); methyl mercaptan ($CH_3SH$); dimethyl sulfide (DMS); and dimethyl disulfide (DMDS) contained in environmental samples. To analyze these compounds in high concentration range (above ppb level), we developed a high mode analytical setting with the loop-injection system. By contrast, we also established a low mode setting for the analysis of low concentration samples (ppt-level samples from ambient air) by the combination with thermal desorption unit (TDU). Comparative analysis of both settings revealed that relative detection properties of four S compounds are systematic enough. The results of high mode analysis indicated that the patterns were systematic among S compounds: $H_2S$ exhibited the lowest sensitivity, while DMDS showed the strongest one. The results were also compared in terms of sensitivity reductions for all compounds by dividing slope ratios between low and high mode system. Although low mode system exhibited significant reductions on the order of a few tens times, their detection characteristics were highly consistent as it was shown in the high mode setting. To learn more about absolute and relative relations between two different modes of S analysis, future studies may have to be directed to cover more complicated nature of GC/PFPD performance.

Continuous Measurements of Reduced Sulfur Gases in Urban Air (연속측정방법을 이용한 도심권 대기질 내 저농도 황화합물의 관측에 대한 연구)

  • Choi Ye-Jin;Kim Ki-Hyun;Oh Sang-In;Shon Zang-Ho
    • Journal of Korean Society for Atmospheric Environment
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    • v.20 no.2
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    • pp.195-204
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    • 2004
  • In this study, the concentrations of major reduced sulfur compounds (H$_2$S, $CH_3$SH, DMS, and DMDS) were determined from ambient air in a monitoring station located in the mid-eastern area of Seoul. Measurements of sulfur species were conducted by the combination of on -line air sampling, thermal desorption, and capillary GC/PFPD analysis. A total number of 143 hourly samples were collected in the two time periods set between June and July 2003. The mean concentrations of four sulfur species measured in the whole study period were found on the order: DMS (535$\pm$183) > H$_2$S (47$\pm$10) > DMDS (35$\pm$22) > $CH_3$SH (6.19$\pm$29.4 pptv). The results of this study show that the concentrations of DMS at the study area are generally higher than those reported previously in the oceanic environments, while those of other sulfur species are not easy to compare with due to the lack of data. The H$_2$S concentrations were generally higher during the daytime than the nighttime, whereas those of others generally exhibited a reversed diurnal pattern. The overall results of our study suggest that the distribution of major reduced S compounds should be controlled by diverse processes in the urban area.

Continuous Measurements of Aromatic VOCs in a Mid-eastern Region of Seoul during Winter 2002/2003 (방향족 휘발성 유기화합물의 겨울철 연속 관측 연구)

  • 최여진;오상인;김기현
    • Journal of Korean Society for Atmospheric Environment
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    • v.19 no.5
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    • pp.491-502
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    • 2003
  • In the present work, the distribution characteristics of ambient volatile organic compounds (VOCs) were investigated at high temporal resolution from a monitoring station located in a mid-eastern area of Seoul. A total number of 587 samples were collected during December 2002 to January 2003. The measurements of VOC were conducted by a combination of on-line air sampling and thermal desorption unit (TDU) coupled with capillary GC/FID analysis. A total of five aromatic compounds (BTEX: benzene, toluene, ethylbenzene, m, p-xylene, and o-xylene) were measured routinely at hourly intervals during the whole study period. The mean concentrations of BTEX measured in our study period were found in the order: toluene (8.99 $\pm$5.38 ppb) > benzene (0.92$\pm$0.52 ppb) > m, p-xylene (0.51$\pm$0.34 ppb) > 0- xylene (0.48$\pm$0.35 ppb) > ethyl benzene (0.43$\pm$ 0.32 ppb). The BTEX concentrations were generally higher during the daytime than the nighttime, exhibiting certain patterns on a weekly basis. Results of our analysis indicate that the unusually high concentrations of toluene, while showing good correlations with other VOCs, can be a good indicator of air pollution in the study area.