• 폴리머
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• 제26권2호
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• pp.200-208
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• 2002

난연성분인 트리클로로벤조산(TBA)의 함량을 10, 20, 30 wt%로 변화시키면서 아디프산, 1,4-부탄디올 및 트리메틸올프로판과 축중합을 하여 트리클로로 락톤 변성폴리에스테르(TAPTs)를 합성한 후에, TAPT류와 이소시아네이트인 Desmodur IL을 블렌드하여 2성분계 폴리우레탄 난연 도료를 제조하였다. 제조된 난연도료의 도막물성을 측정한 결과, 결코 비난연도료보다 물성이 떨어지지 않음을 알았다. 또한 난연도료의 3종류 난연성 시험결과, 수직법에서 TBA 함량 20 wt% 이상에서 불꽃에 타지 않았고, LOI 연소성 시험에서 TBA 함량 20, 30 wt%시 25%와 27%의 LOI값을 나타내었으며, $45^{\circ}$ Meckel burner법에서는 탄화길이가 3.6-5.2 cm로서 난연 1급에 해당되었으므로 이를 미루어 난연효과가 좋은 난연도료임을 알 수 있었다.

• 한국식품과학회지
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• 제22권3호
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• pp.290-295
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• 1990

감마선 조사(0, 2, 4kGy)에 따른 튀긴 닭고기 patty의 미생물 및 TBA가의 변화를 조사하기 위하여 닭고기 patty를 각각 $3{\pm}1^{\circ}C$ 와 $-10{\pm}1^{\circ}C$에서 저장하였다. 방사선 조사에 의하여 $3{\pm}1^{\circ}C$에 저장된 닭고기 patty의 품길 수명은 증가하였다(p<0.05). 대조구 1g당 미생물 총균 log 수가 6.5에 다다르는데 걸리는 시간은 22일인 반면 방사선 조사구는 40일이 걸렸으며 4kGy로 조사된 patty에서는 초기에 미생물이 발견되지 않았다. 조사선량 증가에 따라 gram-positive cocci의 미생물은 감소한 반면 2kGy와 4kGy로 조사된 시료에서는 각각 yeasts와 gram-negative rod 미생물이 현저했다. TBA가는 조사량과 저장기간이 증가함에 따라 증가하였다.

• Journal of Korean Neurosurgical Society
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• 제49권3호
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• pp.157-162
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• 2011

Objective : Vasospasm of cerebral vessels remains a major source of morbidity and mortality after an aneurysmal subarachnoid hemorrhage (SAH). The purpose of this study was to evaluate the safety and efficacy of transluminal balloon angioplasty (TBA) for SAH-induced vasospasm. Methods : Eleven patients with an angiographically confirmed significant vasospasm (>50% vessel narrowing and clinical deterioration) were studied. A total of 54 vessel segments with significant vasospasm were treated by TBA. Digital subtraction angiography was used to confirm the presence of vasospasm, and TBA was performed to dilate vasospastic arteries. Medical and angiographic reports were reviewed to determine technical efficacy and for procedural complications. Results : TBA using Hyper-Glide or Hyper-Form balloons (MicroTherapeutics, Irvine, CA) was successfully accomplished in 88.9% vasospastic segments (48 of 54), namely, in the distal internal carotid artery (100%, n=7), the middle cerebral artery (100%), including the M1 (n=10), M2 (n=10), and M3 segments (n=4), in the vertebral artery (100%, n=2), basilar artery (100%, n=1), and in the anterior cerebral artery (ACA), including the A1 (66%), A2 (66%), and A3 segments (100%). Vessel diameters significantly increased after TBA. There were no cases of vessel rupture or thromboembolic complications. GCS at one day after TBA showed an improvement in all patients except one. Conclusion : This study suggests that TBA using Hyper-Glide or Hyper-Form balloons is a safe and effective treatment for subarachnoid hemorrhage-induced cerebral vasospasm.

• 한국식품조리과학회지
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• 제17권2호
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• pp.117-122
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• 2001

마쇄한 마늘과 50% ethanol의 마늘 추출액을 분쇄돈육에 첨가하여 4$^{\circ}C$에 저장하면서 pH, POV가와 TBA가의 변화를 조사하였다. 분쇄돈육은 가열하지 않은 생육과 10$0^{\circ}C$에서 10분간 가열한 가열육으로 나누어 실험하였다. 마쇄한 마늘과 마늘 추출액을 분쇄돈육에 첨가하였을 때 저장 중 과산화물가와 TBA가는 마늘첨가량이 많을수록 현저한 감소로 지질의 산화 억제 효과를 나타내었으며, 특히 10% 마늘 추출액은 마쇄 마늘을 20% 첨가하였을 때와 거의 비슷한 효과를 보였다. 효과는 저장 중 4-6일째까지 가장 컸고 그 후에는 점차적으로 감소하였다. pH는 전반적으로 6일까지는 대체적으로 감소하였다가 그 이후 증가하였다. 마쇄한 마늘과 ethanol 50%의 마늘 추출액을 분쇄돈육에 첨가했을 때 약간의 pH 증가를 보였다. 생육과 가열육 모두 pH, 과산화 물가와 TBA가에서 비슷한 영향을 주었으나 생육보다 가열육에서 더 많은 변화를 보였다.

• 대한한의학회지
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• 제35권1호
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• pp.50-57
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• 2014

Objectives: The purpose of this study was to examine whether Temporomandibular Joint Balance Appliance-Golf (TBA-G) can improve postural control ability of healthy adults. Methods: Twenty participants (10 male, 10 female) aged 20 to 39 years were involved. Postural control ability of all participants was assessed before and after applying TBA-G with Balance $Master^{(R)}$ system. Modified clinical test sensory interaction on balance (mCTSIB), unilateral stance, weight bearing and rhythmic weight shift were used to evaluate postural control ability. Results: After applying TBA-G, mCTSIB on a firm plate with eyes open increased from 0.2 to 0.23 (p<0.05) but directional control was improved in slow and moderate velocity of front/back rhythmic weight shift test (P<0.05). In two cases with postural imbalance, most of the postural control measures improved after applying TBA-G. Conclusions: The results suggest that TBA-G could improve balance control ability. A larger controlled trial is needed to determine more accurately the effect of TBA-G on balance control ability.

• 산업식품공학
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• 제15권3호
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• pp.209-213
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• 2011

대두에서 산패취를 발생시키는 lipoxygenase 효소를 비가열 전처리 방법인 초고압 처리 방법을 이용하여 효소의 활성도의 변화를 확인하였다. 연구 결과 초고압 처리에 의해 lipoxygenase 효소의 활성도가 감소하는 것을 확인하였다. 또한 lipoxygenase 효소의 활성도 감소에 의해 대두의 저장성에 미치는 영향을 확인하기 위해 국산 대두와 연해주대두를 이용하여 저장 실험을 실시하였다. 실험 결과 국산대두의 경우 초고압 처리에 의해 lipoxygenase 효소의 활성도가 감소하였으나 TBA가에 영향을 주는 자동산화등의 화학반응에 의해 TBA가가 지속적으로 증가함을 보여주었다. 그러나 연해주 대두의 경우에는 초고압 처리를 한 시료의 TBA가의 증가정도가 상대적으로 낮게 측정된 것을 확인하였다. 이는 연해주 대두가 항산화 성분을 국산콩에 비하여 많이 포함하고 있어 초고압 처리에 의한 lipoxygenase 효소의 불활성과 함께 항산화 성분의 영향으로 TBA가의 저장 중 증가 정도가 낮게 측정된 것으로 판단되어진다.

• 한국식품과학회지
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• 제24권5호
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• pp.497-503
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• 1992

영지 추출액의 항산화 활성을 thiocyanate method, TBA method, weighing method를 이용하여 검색한 결과 n-hexane 추출물, methanol 추출물에서 항산화활성이 나타났으며 그 중에서 n-hexane 추출물의 fraction V와 methanol 추출물의 methanol 불용성 fraction II에서 강한 활성을 나타내었다. 이들 항산화 활성을 나타내는 fraction 5와 fraction II를 rat의 간 균질액을 이용한 항산화 활성 검색에서 과산화 지질 생성억제를 TBA값으로 나타내어 inhibition ratio(I.R.)를 산출하였으며 그 결과 n-hexane 추출물의 fraction V는 l5%, methanol 추출물의 methanol 불용성 fraction II는 54.6%의 억제율을 나타내었다 이는 rat의 간 mitochondria에서 과산화지질 생성 억제율이 영지의 물 추출물은 16%, acetone 추출물은 23%인 것에 비하여 약간 높았으나, microsome에서 과산화지질 생성 억제율이 물 추출물은 44%, acetone 추출물은 75%인 것에 비하여 다소 낮은 활성을 보여주었다.

• 한국응용과학기술학회지
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• 제12권1호
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• pp.43-46
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• 1995

The antioxidative effect of ethanol extract of ginger on mackerel pike(Colorabis saira) flesh was investigated by periodically measuring TBA value and perioxide value(POV) during storage. The ethanol extract of ginger was added to minced mackerel pike flesh and the fish oil by concentration(2%, 4%, 6%, 8%). Then the minced flesh was storaged at $-5^{\circ}C$ and the fish oil was incubated at $40^{\circ}C$. The TBA values of minced flesh were approximately increased in inverse proportion to concentration of ginger extract. Peroxide values were attended with the same effect as TBA value in the aggregate. In addition, The relationship between $TBA_{37^{\circ}C-2hrs}$ of the minced flesh and their lipid oxidation during storage at -$5^{\circ}C$ for 4 weeks was observed(r=O.98). $TBA_{37^{\circ}C-2hrs}$ can be expressed as the susceptibility to lipid oxidation of minced mackerel pike flesh during storage. In the results, the antioxidative effect of alcohol extract of ginger on mackerel pike flesh was observed.

• 대한가정학회지
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• 제24권1호
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• pp.43-51
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• 1986

In order to study antioxidative acton of garlic, alliin, scordinin, garlic oil, ethanol fraction and non-kaolin fraction which have been discovered from garlic until now were extracted and isolated, and each fraction was utilized as the experimental materials. Antioxidative action of each fraction was compared through the in vitro and in vivo experiments. Electron donatingability on $\alpha$, $\alpha$-diphenyl-$\beta$picrylhydra-$\chi$yl, the inhibitory effect of lipoperoxide formation by TBA and peroxide value were measured and analyzed. RESULTS : 1. When observed antioxidative ability by EDA value, ethanol fraction of garlic components showed the strongest reaction as 15.25. 2. In vitro experiment with TBA value, garlic oil, alliin and ethanol fracton showed distinctive effect on inhibitory effect of lipoperoxide formation. 3. Comparing with the inhibitory effect of lipoperoxide formation with TBA value in vivo, the ethanol fraction was the most effective in the blood or liver by intraperitoneal administration, whereas the ethanol fraction in the blood and non-kaolin fraction in the liver was most effective each other by orally administration. 4. In vitro experiment with peroxide value, garlic oil was distinctive effect on the inhivitory effect of lipoperoxide formation, which was a similar to the trend of TBA value in vitro. 5. Examining the induction time for the first period of lipoperoxide formation in vitro, garlix oil, ethanol fraction and alliin were effective, which was a similar to the trend of TBA value and peroxide value in vitro.

• 한국재료학회지
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• 제26권2호
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• pp.61-66
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• 2016

In order to fabricate porous mullite ceramics with controlled pore structure and improved mechanical strength, a freeze casting route has been processed using camphene mixed with tertiary-butyl alcohol (TBA) and coal fly ash/alumina as the solvent and the ceramic material, respectively. After sintering, the solidification characteristics of camphene and TBA solvent were evident in the pore morphology, i.e., dendritic and straight pore channels formed along the solidification directions of camphene and TBA ice, respectively, after sublimation. Also, the presence of microcracks was observed in the bodies sintered at $1500^{\circ}C$, mainly due to the difference in solidification volume change between camphene and TBA. The compressive strength of the sintered bodies was found generally to be dependent, in an inverse manner, on the porosity, which was mainly determined by the processing conditions. After sintering at $1300{\sim}1500^{\circ}C$ with 30~50 wt% solid loading, the resulting mullite ceramics showed porosity and compressive strength values in ranges of 83.8~43.1% and 3.7~206.8 MPa, respectively.