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검색결과 917건 처리시간 0.03초

Part-Per-Trillion level determination of Alkylphenols, Chlorophenols and Bisphenol A using GC/MS-SIM in Tap Water

  • Kim, Hyub
    • 한국환경독성학회:학술대회논문집
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    • 한국환경독성학회 2003년도 추계국제학술대회
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    • pp.149-149
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    • 2003
  • A new technique is proposed for the determination of alkylphenols, chlorophenols and bisphenol A in tap water. The sample preparation consists of a solid phase extraction (SPE) of alkylphenols, chlorophenols and bisphenol A from a water sample with XAD-4 and subsequent conversion to isobutyloxycarbonyl (isoBOC) derivatives or tert.-butyldimethylsilyl (TBDMS) derivatives for sensitive analysis with the GC/MS-SIM mode. The recoveries were 86.6∼105.2 % (isoBOC derivatization) and 97.6∼484.5 % (TBDMS derivatization), respectively. The limit of quantitation of alkylphenols, chlorophenols and bisphenol A for SIM were 0.001∼0.050 $\mu\textrm{g}$/l (isoBOC derivatization) and 0.003∼0.050 $\mu\textrm{g}$/l (TBDMS derivatization). The SIM responses were linear with the correlation coefficient varying 0.9755∼0.9981 (isoBOC derivatization), and 0.9908∼0.9996 (TBDMS derivatization). The derivative methods and their application to tap water samples will be disscussed.

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High Performance De-interlacing Algorithm Based on Region Adaptive Interpolation Filter

  • Yang, Yang;Chen, Xiangdong;Wang, Jin;Jeong, Jechang
    • 한국방송∙미디어공학회:학술대회논문집
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    • 한국방송공학회 2011년도 추계학술대회
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    • pp.200-203
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    • 2011
  • In order to convert interlaced video into progressive scanning format, this paper proposed a high performance de-interlacing algorithm based on region adaptive interpolation filter design. Specifically, usage of the 6-tap filter is only for the most complex region, but for the smooth and regular edge region, much more correlated filter such as 2-tap or 4-tap filter should be used instead. According to the experimental results, the proposed algorithm has achieved noticeably good performance.

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청량음료의 미생물 오염에 대하여 (On the Microbial Contamination in Softdrink Manufacturing Process)

  • 김용배;이병국;유건희;조남선
    • 미생물학회지
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    • 제11권3호
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    • pp.129-133
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    • 1973
  • The authors have investigated about the microbial contamination of goods which is a criterion of hygienic control. Conducting on investigation, a special attention has been paid on the rate of microbial contamination in the goods, especially in manufacturing process of the softdrink. The authors also made an experiment on total microbes which is the criterion of contamination in each step of the process and in raw materials together with materials to be used for subdividing. Results obtained were as follows : 1) The orgin of microbial contamination was found in bottle cap and in tap water, that is, there appeared 9 colony per ml in bottle cap and 31-74 colony per ml in tap water, respectively. 2) It was found that microbial contamination are 4 colony per ml in average through year. However, it appeared 1 colony per ml in winter and 8 colony per ml in summer. 3) Coliform groups are not detected in goods through a year. 4) There was no variation in number of total microbes after ion exchange resin passage in purification process of tap water. 5) The number of microbes in goods are decreased when the raw materials are treated in high temperature short time (HTST) sterilization.

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입자간 Stacking이 자기기록용 Ba-ferrite 분말의 물성과 분산성에 미치는 영향 (Particle Stacking Dependence of Properties and Dispersitility of Ba-ferrite Powder for Magnetic Recording)

  • 홍양기;정홍식;박상준
    • 한국자기학회지
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    • 제6권2호
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    • pp.117-121
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    • 1996
  • 육각판상 Ba-ferrite의 stacking 현상은 자성도료의 도포 후 자장배향를 행할 때 일어나는 것으로 알려져 있으나 분말의 건식분쇄시에도 일어났다. Edge mill을 사용하여 건식분쇄할 때 치환형 Ba-ferrite 분말의 보자력과 tap density는 거의 비례적으로 증가하였고, 분쇄시간보다는 가해지는 압력에 크게 의존하였다. 이 때 보자력의 증가원인은 분쇄시 생성되는 입자간의 stacking 현상에 기인된 것임을 투과전자현미경 관찰로부터 확인하였다. 분말의 tap density가 증가함에 따라 tape에서 분산초기의 광택도가 크게 감소되어 분산성은 떨어졌으나, 배향도는 tap density 1.3 g/$cm^{3}$에서 최대를 나타내었다. 과도한 건식분쇄에 의해 생성된 강고한 stacked cluster는 자성도료 제조시 분산성과 배향도를 동시에 떨어뜨리는 역할을 함을 알 수 있었다.

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The Study on Nonlinear Compensation Characteristics of Multi-tap Update Algorithm in Broadband PCS Channel

  • 이승대
    • 한국컴퓨터산업학회논문지
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    • 제9권2호
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    • pp.77-82
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    • 2008
  • The diversity reception and the equal gain combining technique are applied to the compensation of the distortion of channel, which occurs in transmission of data at rapid speed. DSSS BPSK system which has the receiving structure with the compensation algorithm is formed on the diversity branch, and the characteristics of the system are evaluated at the view point of the average bit error rate due to the SNR. In addition, the multi-tap update algorithm which is superior for the data compensation is suggested. Moreover, using the American Joint Technical Committee PCS RF channel characterization and system deployment model standard, the suggested multi-tap update algorithm is compared and analyzed with the view-point of the average bit error rate and convergence speed for evaluating the realistic efficiency of the system.

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수중음향통신을 위한 결정궤환 등화기의 실험적 연구 (Experimental Study of a Decision Feedback Equalizer for Underwater Acoustic Communications)

  • 최영철;박종원;임용곤
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2008년도 추계종합학술대회 B
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    • pp.565-568
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    • 2008
  • 본 논문에서는 2007년 11월 거제 연안에서 실해역 실험을 통하여 취득한 데이터를 이용하여 수중음향통신을 위한 적응 결정궤환 등화기의 비트 오율 성능 분석 결과에 대해서 논한다. 전방먹임 필터 탭수, 되먹임 필터 탭 수, 훈련신호열 길이, 시간 지연 등의 변수를 변화시키면서 비트 오율을 분석한 결과, 전달 거리 9.7km, 4km에서 각각 $4{\times}10^{-2}\;and\;1.5{\times}10^{-2}$ 비트 오율을 얻었다.

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GC/MS-SIM 방법에 의한 수돗물 중 알킬페놀, 플로로페놀과 비스페놀 A의 ppt 정량 (Part-Per-Trillion Level Determination of Alkylphenols, Chlorophenols and Bisphenol A using GC/MS-SIM in Tap Water Samples)

  • 김협
    • Environmental Analysis Health and Toxicology
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    • 제18권3호
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    • pp.199-208
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    • 2003
  • A new technique was proposed for the determination of alkylphenols, chlorophenols and bisphenol A in tap water samples. The sample preparation consists of a solid phase extraction (SPE) of alkylphenols, chlorophenols and bisphenol A from a water sample with XAD-4 and subsequent conversion to isobutyloxycarbonyl (isoBOC) derivatives or tert-butyldimethylsilyl (TBDMS) derivatives for sensitive analysis with the CC/MS SIM mode. The recoveries were 86.6 ∼ 105.2% (isoBOC derivatization) and 97.6∼484.5% (TBDMS derivatization), respectively. The limit of quantitation of alkylphenols, chlorophenols and bisphenol h for SIM were 0.001∼0.050 $\mu\textrm{g}$/1 (isoBOC derivatization) and 0.003∼0.050 $\mu\textrm{g}$/1 (TBDMS derivatization). The SIM responses were linear with the correlation coefficient varying 0.9755∼0.9981 (isoBOC derivatization), and 0.9908∼0.9996 (TBDMS derivatization). When these methods were applied to tap water samples, the range of concentrations were 22.8∼31.3 ng/1 in 2,4-dichlorophenol, 28.6∼70.3 ng/1 in pentachlorophenol, 15.2∼17.4 ng/1 in t-butylphenol, 10.8∼13.2 ng/1 in t-octylphenol and 17.6∼36.3 ng/l in bisphenol A, respectively.

물사용 인식 및 실천에 관한 조사 연구-대구광역시 초${\cdot}$중등교사를 대상으로- (A Research on Understanding about Water Usage, Recognition and Application among Primary and Secondary School Teachers in Daegu)

  • 곽홍탁;전은정;이옥희
    • 한국환경교육학회지:환경교육
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    • 제17권2호
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    • pp.60-78
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    • 2004
  • A survey performed on property of water usage, a recognition and stand on water, and awareness of practice related to water saving among primary and secondary teachers in Daegu metropolitan city leads to the following result. First, regarding the actual condition of water usage, boiled tap water was most preferred, followed by purified tap water, mineral water, and water from a mineral spring respectively. Second, the result of a survey regarding a recognition and stand on water presents that the quality of purified water and mineral water is generally trusted, not including tap water. A majority of teachers barely had any ideas on the process of tap water supplies and sewage disposal system. Third, another survey was performed to determine whether there's a gender difference on a general recognition of and stand on water usage, actual practice of water saving and love for water. As a result, 7 out of 25 questions showed the difference of significance by p<.05. As for tap water service and sewage disposal system, there were differences on 5 out of 6 questions, indicating that male teachers are more knowledgable than their female counterparts. Fourth, the result of the research about the recognition and attitudes about water and water saving of the teachers who were categorized by the age group showed that 14 questions of the 25 questions had differences in p<.05 level. Teachers in their twenties and thirties had less interest than those in their forties and fifties.

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수경재배시 양액 조성 처리가 몇가지 엽채류의 내적 품질에 미치는 영향 (Effect of Nutrient Solution Composition Modification on the Internal Quality of Some Leaf Vegetables in Hydroponics)

  • 강호민;김일섭
    • 생물환경조절학회지
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    • 제16권4호
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    • pp.348-351
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    • 2007
  • 본 실험은 양액조성 및 단비 처리에 의한 엽채류의 질산염과 비타민 C와 같은 내적품질 변화를 알아보고자 하였다. 2주일간 정상적인 배양액에서 재배한 후 다시 2주일간 서로 다른조건의 양액에서 재배한 청경채, 청치마상추, 로메인상추는 단비처리구를 제외하고는 생육에 큰 차이를 보이지 않았다. 내적 품질로 질산염은 야마자키 상추 1배 양액 처리구에서 가장 높았으며 다음으로 $+NH_4$ 처리구 순서였고 $-NO_3$와 단비 처리구에서 가장 낮았다. 비타민 C 함량은 대체로 질산염과 반대의 결과를 나타내어 청치마, 로메인상추에서는 단비처리구에서 청경채는 $-NO_3$처리구에서 가장 높았다. 이들 질산염과 비타민 C 함량간의 상관계수는 청경채는 -0.614, 로메인상추는 -0.651이었으며 특히 청치마상추는 -0.804를 나타내었다.