• 한국결정성장학회지
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• 제13권1호
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• pp.24-30
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• 2003

The preparation of $PbTiO_3$ powder was carried out using the oxide starting material by hydrothermal method. The powder of a crystalline phase with perovskite structure was synthesized. The optimum conditions for the preparation of powder were as follows; hydrothermal solvent; 8M-KOH or 8M-NaOH, reaction temperature; 250~$270^{\circ}C$, run time; 10 h. The ,shape of synthesized powders were well developed crystalline faces with specific surface area of about 2.3 $\textrm m^2$/g in KOH solution and about 5.0 $\textrm m^2$/g in NaOH solution. The cell parameters of powder were a = 3.90$\AA$, c = 4.14 $\AA$ and cell volume was 57.30 $\AA^3$. The cell ratio (c/a) of powder was the same as the theoretical ratio with c/a = 1.06 and the phase transition temperature(Tc) of the powders was about $470^{\circ}C$.

• Carbon letters
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• 제14권2호
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• pp.99-104
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• 2013

We investigated the effects of parametric synthesis conditions of catalysts such as sintering temperature, sorts of supports and compositions of catalysts on alignment and length-control of carbon nanotubes (CNTs) using catalyst powders. To obtain aligned CNTs, several parameters were changed such as amount of citric acid, calcination temperature of catalysts, and the sorts of supports using the combustion method as well as to prepare catalyst. CNTs with different lengths were synthesized as portions of molybdenum and iron using a chemical vapor deposition reactor. In this work, the mechanisms of alignment of CNTs and of the length-control of CNTs are discussed.

• Carbon letters
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• 제12권1호
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• pp.39-43
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• 2011

Synthesis of carbon fibers from cotton fiber by pyrolysis process has been described. Synthesis parameters are optimized using Taguchi optimization technique. Synthesized carbon fibers are used for studying hydrogen adsorption capacity using Seivert's apparatus. Transmission electron microscopy analysis and X-ray diffraction of carbon fiber from cotton suggested it to be very transparent type material possessing graphitic nature. Carbon synthesized from cotton fibers under the conditions predicted by Taguchi optimization methodology (no treatment of cotton fiber prior to pyrolysis, temperature of pyrolysis $800^{\circ}C$, Argon as carrier gas and paralyzing time for 2 h) exhibited 7.32 wt% hydrogen adsorption capacity.

• 한국농업기계학회:학술대회논문집
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• 한국농업기계학회 1993년도 Proceedings of International Conference for Agricultural Machinery and Process Engineering
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• pp.284-290
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• 1993

In order to improve the adaptability of rice transplanter to seeding with different length when transplanting multicropping rice in south China. The seedling separating planting mechanism is resynthesized in the paper. According to the agronomy requirements of seedling's transplanting, optimum motional path of the tip point of planting needle is obtained. by applying the established kinematic model of the separating planting mechanism, the relevant software is compiled. On the basis of the features of the problem, the constrained optimization method is utilized to solve the problem with 24 restrictions. Thus, the optimum structure parameters are obtained to satisfy the path points accurately.

• 한국자동차공학회논문집
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• 제2권3호
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• pp.62-74
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• 1994

This paper addresses on the model synthesis and performance analysis of an engine mount featuring electro-rheological(ER) fluids which undergo a phase change when subjected to electric fields. A novel type of ER fluid-filled engine mount is devised and its hydraulic model is constructed. An equivalent mechanical model is subsequently obtained from the governing equation of the hydraulic model. The model parameters associated with the ER fluids are distilled from experimental investigations on the Bingham properties of the fluids. The distilled data are then incorporated into the governing model to undertake feasible work through computer simulations,. It is shown that the proposed engine mount has an inherent capability of controlling both the damping force and the resonance frequency. Other superior performance characteristics accrued from the proposed methodology are also evaluated.

• 한국응용과학기술학회지
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• 제26권4호
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• pp.385-393
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• 2009

Different types magnesium hydroxide groups have been obtained using the hydrothermal precipitation technique from magnesium sulfate and calcium carbonate solution. The Mg atom coordinated around O atom of ${SO_4}^{2-}$ in another layer to form a multi-layer structure crystal. The influence of synthesis parameters on the morphological characteristics and size of magnesium hydroxide groups precipitated in aqueous were investigated such as different of additive and pH. Magnesium hydroxide groups were decomposed gradually and converted finally to MgO particles after heated in air temperature up to $1050^{\circ}C$. The particle size and it's distribution morphology, crystal phase and thermal behavior of the samples were characterized through XRD, SEM, EDS, and TG/DTA.

• 한국전기전자재료학회논문지
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• 제18권10호
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• pp.929-935
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• 2005

In this paper, synthetic conditions of titania nanparticle was investigated to enhance its uniformity of the particle size as a child particle on organic mother particle of liquid powder type electronic paper. The physical properties are very important to improve the uniformity of electrical charging properties Concentration of titania raw material ($C_9H_{19}NO_4Ti$) in the ethanol solvent, pH, and concentration of the solution in the D.I. water were selected as parameters. As a result, ultrafine and well crystallized titania nanoparticle with good uniformity could be synthesized as the concentration of the $C_9H_{19}NO_4Ti$ in the ethanol solvent, pH of the solution, and the amount of the D.I. water were increased. Using the optimized conditions, the titania nanparoticle with uniformly ultrafime size of 10 nm could be synthesized.

• 한국결정성장학회지
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• 제11권4호
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• pp.176-179
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• 2001

Iron oxide powders were prepared under high temperature (up to $175^{\circ}C$) and pressure conditions( up to 129 pasi) by precipitation from metal nitrates with aqueous potassium hydroxide. Various types of iron oxide powders were obtained at different conditions. The size and the shape of the particles can be controlled as afunction of starting solution pH. The average particles size of the synthesized iron oxide powders increased, the particle shapes of the powders became fibrous, and the crystalline phase of the powder changes from iron oxide to iron hydroxide with increasing solution pH. The effects of synthesis parameters are discussed.

• The Korean Journal of Ceramics
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• 제5권4호
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• pp.348-352
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• 1999

Barium uranium sulfides, $BaUS_3$ and $BaU_2B_5$, were synthesized in a single phase by the reactin of $(Ba, UO_2)(NO_3)_2$ at Ba/U=1 and 0.5 with carbon disulfide at 1273 K for 6 h. They crystallized in orthorhombic structure with space group, Pnma. The lattice parameters a, b and c are 7.493, 10.38 and 7.238$\AA$ for $BaUS_3$ and 7.525, 8.475 and 11.858$\AA$ for $BaU_2S_5$, respectively. The electrical conductivity of these compunds increased with increasing temperature above 200K, below which however, it was nearly temperature independent. The Hall coefficient suggested that they are n-type semiconductors.

• Bulletin of the Korean Chemical Society
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• 제32권7호
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• pp.2316-2318
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• 2011

A novel technology has been developed for the synthesis of thioglycolic acid (TGA)-capped CdSe quantum dots (QDs) in aqueous medium. The reaction was carried out in air atmosphere with one-pot by using $SeO_2$ to replace Se or $Na_2Se$. The technological parameters including refluxing time, pH values and molar ratios of selenium to cadmium had significant influence on the luminescence properties of CdSe QDs. Furthermore, the obtained QDs were characterized by fluorescent spectroscopy, X-ray powder diffraction (XRD) and transmission electron microscopy (TEM), respectively. The results demonstrated that the CdSe QDs were of zinc-blended crystal structure in a sphere-like shape.