• Journal of the Korean Wood Science and Technology
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• v.49 no.1
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• pp.1-13
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• 2021

This study was conducted to investigate the effects of the synthesis method, melamine content, and GPC parameters (such as flow rate, column-detector temperature, and sample injection temperature) on the molecular weight of melamine-urea-formaldehyde (MUF) resins. Two different synthesis methods were employed. In the first method, MUF-A resins were synthesized by simultaneously reacting urea, formaldehyde, and melamine (5%, 10%, and 20%) using the reaction of alkaline-acid-alkaline steps under controlled temperature and viscosity. In the second method, MUF-B resins were synthesized by first reacting melamine at the same levels with formaldehyde and then by adding urea. The highest weight average molecular weight (Mw) of MUF-A resins was found at 10% melamine content when the flow rate was 0.3 and 0.8 ml/min; Mw decreased slightly at 20% melamine content. The results showed that Mw increased with an increase in the melamine content when the flow rate was 0.5 and 1.0 ml/min. In addition, Mw was the highest when the flow rate, column-detector temperature, and injection temperature were 0.3 ml/min, 50℃, and 25℃, respectively. On the contrary, MUF-B resins had greater Mw and number average molecular weight (Mn) than MUF-A resins. Overall, Mw and Mn increased as the melamine content increased. The optimal GPC parameter for MUF resins was determined as follows: a flow rate of 0.5 ml/min, a column-detector temperature of 50℃, and a sample injection temperature of 50℃.

• The Bulletin of The Korean Astronomical Society
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• v.38 no.2
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• pp.35.2-35.2
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• 2013

I will present a new approach to constrain galaxy physical parameters from the combined interpretation of stellar and nebular emission in wide ranges of observations. This approach relies on a comprehensive library of synthetic spectra, assembled using state-of-the-art models of star formation and chemical enrichment histories, stellar population synthesis, nebular emission and attenuation by dust. We focus on the constraints set by 5-band photometry and low- and medium-resolution spectroscopy at optical rest wavelengths on a few physical parameters characterizing the stars and interstellar medium. Since these parameters cannot be known a priori for any galaxy sample, we assess the accuracy to which they can be retrieved by simulating 'pseudo-observations' using models with known parameters. We find that the combined analysis of stellar and nebular emission in low-resolution (50A FWHM) galaxy spectra provides valuable constraints on all physical parameters. The approach can be extended to the analysis of any type of observation and during this talk i will present some applications to observed galaxies up to redshift 1.5.

• 제어로봇시스템학회:학술대회논문집
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• 1996.10a
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• pp.376-379
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• 1996

Synthesis for qualitative analysis in connection with quantitative analysis from the pinch design method, EVOP and Operations Research is proposed for the optimal synthesis of heat exchanger networks, that is through of the transportation model of the linear programming for synthesizing chemical processing systems, to determine the location of pinch points, the stream matches and the corresponding heat flowrate exchanged at each match. In the second place, according to the optimization, the optimal design of heat transfer enhancement is carried on a fixed optimum heat exchanger network structure, in which this design determines optimal operational parameters and the chosen type of heat exchangers as well. Finally, the method of this paper is applied to the study of the optimal synthetic design of heat exchanger network of constant-decompress distillation plants.

• Proceedings of the IEEK Conference
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• 2005.11a
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• pp.435-438
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• 2005

In this paper, we implemented a system that is called sound engine in musical synthesizer and synthesized a sound of Gayageum using TMS320C6713 DSK. Sound engine consists of two parts: synthesis algorithm and processor. We improved physical modeling using digital waveguide as a synthesis algorithm and we used TMS320C6713 as a processor. The excitation signals that make timbre are stored in memory. When we input parameters, sound engine synthesizes sound of Gayageum. The experimental result shows that synthesized sounds are very similar to real sounds.

• Journal of the Korean Ceramic Society
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• v.32 no.3
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• pp.341-348
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• 1995

An analysis of the use of temperature profiles in the determination of the kinetic parameters of combustion synthesis of Ti5Si3 were investigated. From profile analysis, an apparent activation energy of 12KJ/mol was calculated. The Maximum heating rate achieved during 10wt% Ti5Si3 reaction by the product dilution method was approximately $1.5\times$104 K/s. Coupling this value with the measured wave velocity of 7.02 cm/s yields a maximum thermal gradient of 2.14$\times$103 K/cm. The value of tr (=t*) was calculated to be 1.2$\times$10-1 s and the value of td (=tx) was calculated to be 32.89 s. Using the definition of t* and the measured wave velocity, the effective thermal diffusivity, $\alpha$, was calculated to be 0.59$\times$10 $\textrm{cm}^2$/s. From these analysis, the power function, G, was also calculated.

• Journal of the Korean Society of Laryngology, Phoniatrics and Logopedics
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• v.12 no.2
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• pp.115-120
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• 2001

In this paper, we synthesized vowel /ae/ with voice synthesis program of Dr. Speech Science, and we also synthesized pathologic vowel /ae/ by some parameters such as high frequency gain (HFG), low frequency gain(LFG), pitch flutter(PF) which represents jitter value and flutter of amplitude(FA) which represents shimmer value, and grade ranked as mild, moderate and severe respectively. And then we analysed all pathologic voice by analysis program of Dr. Speech Science. We expect that this synthesized pathologic voices are useful for understanding the parameter such as noise, jitter and shimmer and feedback effect to patient with voice disorder.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.12
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• pp.120-127
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• 1998

The finite element method has been used to model and analyze the heat transfer phenomena during manufacturing process of $MoSi_2$ by SHS(Self-propagating High-temperature Synthesis). For this purpose nonlinear transient heat transfer analyses by using ANSYS have been performed to estimate the temperature distributions and the peak temperature in the test specimen. The effects of manufacturing process parameters such as pre-heating temperatures, the velocity of reaction zone have been investigated. The results of the analysis have been compared with the experimental results.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2000.11a
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• pp.11-12
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• 2000

Non-stoichiometric ceramics of $Ni_{x}ZnO_{1-x}Fe_{2}O_{4}$ were prepared by self-propagating high temperature synthesis reaction with various processing conditions and their stoichometric numbers were determined by neutron diffraction. The neutron diffraction patterns were measured at room temperature using monochromatic neutrons with a wave length of 0.18339 nm from a Ge(331) mocochromator at a 90 degree take off angle. The Rietveld refinement of each pattern converged to good agreement (x2=1.88-2.24). The neutron diffraction analysis revealed the final stoichiometries of the ferrites were $Ni_{0.38}Zn_{0.62}Fe_{2}O_{4}$ and $Ni_{0.33}Zn_{0.67}Fe_{2}O_{4]$, respectively. This supports that final stoichiometric number of the self-propagating high temperature synthesis product can be controlled by the processing parameters during the combustion reaction.

• The Journal of the Acoustical Society of Korea
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• v.16 no.3
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• pp.5-12
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• 1997

In this paper, the 3 operator FM synthesis method has been devised on the basis of the analysis of Gayageum sounds. The parameters for the proposed synthesis algorithm has been implemented by C language. It is subjectively and objectively confirmed that the sounds synthesized by C language are very similar to the original sounds. The synthesis algorithm is also implemented by DSP, and the sounds from this experiment are close to the original ones.

• Proceedings of the KAIS Fall Conference
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• 2012.05a
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• pp.431-435
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• 2012

Aluminum containing mesoporous molecular sieves Al-SBA-1 ($n_{Si}/n_{Al}$= 2, 5, 10, 15) was synthesized with a one-step method, and the catalyst was characterized with powder X-ray diffraction (XRD), nitrogen adsorption-desorption, thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). Finally, we studied the catalytic activities of Al-SBA-1 molecular sieves in Pechmann reaction of 3-methoxyphenol and Ethyl acetoacetate to get 7-methoxy-4-methyl coumarin. Four parameters reaction temperature, time, catalyst weight and reactants ratio were optimized.