• Journal of the Korean Electrochemical Society
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• v.20 no.1
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• pp.1-6
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• 2017

This study investigated the effect of surface pretreatment, which removes native Cu oxides on Cu seed layer, on subsequent Cu electro-/electroless deposition in Cu interconnection. The native Cu oxides were removed by using citric acid-based solution frequently used in Cu chemical mechanical polishing process and the selective Cu oxide removal was successfully achieved by controlling the solution composition. The characterization of electro-/electrolessly deposited Cu films after the oxide removal was then performed in terms of film resistivity, surface roughness, etc. It was observed that the lowest film resistivity and surface roughness were obtained from the substrate whose native Cu oxides were selectively removed.

• Proceedings of the KSME Conference
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• 2003.11a
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• pp.1121-1126
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• 2003

Strength evaluation was carried out for the fillet and oil hole of crankshaft of medium speed diesel HiMSEN engine to verify initial concept design. Alternating torque obtained from torsional vibration analysis and radial force due to firing pressure were applied. It was assumed that the maximum alternating torque and radial force occur simultaneously. Weak points in view of fatigue are proceeding fillet and crank pin fillet area and the minimum normalized fatigue safety factor is 1.17 at crank pin fillet. The fatigue strength of the oil hole was evaluated to verify the effect of the surface roughness of the oil hole. As results, the specific level of the inner surface roughness and the polishing depth of the oil hole for sufficient fatigue strength was suggested. The maximum stress value and stress distribution at the inner surface of the oil hole can be easily estimated at initial design stage by the newly developed method.

• Journal of the Korean Society for Precision Engineering
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• v.33 no.11
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• pp.905-910
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• 2016

Infrared (IR) optic lens can be fabricated by a single point diamond turning (SPDT) machine without subsequent polishing process. However, this machining process often leaves micro-cracks that deteriorate the surface quality. In this work, we propose an experimental design to remove micro-cracks on IR lens. The proposed design gathered data between cutting process condition and Rt surface roughness. This is of great importance because the scale of micro-cracks is a few micrometer. Rt surface roughness is suitable for analyzing maximum peak height signals of the profile. The experimental results indicate that feed per revolution variable is one of the most dominant variable, affecting the generation micro-cracks on IR lens surfaces.

• Journal of the Korean Society for Precision Engineering
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• v.22 no.7 s.172
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• pp.122-129
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• 2005

Shoe with leather upper such as safety and golf shoe requires a roughing process where the upper is roughed fur helping outsole to be cemented well. It is an important and basic process for production of leather shoe but is not automated yet. Thus, there are problems that the defect rate is high and the quality of roughed surface is not uniform. In order to solve such problems, the interest in automation of roughing process is being increased and this paper introduces CAM system for 5-axis automatic roughing machine as one part of automation of roughing process. The CAM system developed interpolates a B-spline curve using points measured from the Roughing Path Measurement System. The B-spline curve is used to generate the tool path and orientation data fer a roughing tool which has not only stiffness but also flexibility to rough the inclined surface efficiently. For productivity, the upper of shoe is machined by side of the roughing tool and tool offset is applied to the roughing tool for machining of inclined surface. The generated NC code was applied to 5-axis polishing machine for the test. The upper of shoe was roughed well along the roughing path data from CAM and the roughed surface was proper fur cementing of the outsole.

• International Journal of Precision Engineering and Manufacturing
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• v.5 no.1
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• pp.47-54
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• 2004

In this study, the electrorheological (ER) fluid was used as finishing agent. Since the apparent viscosity can be controlled by an electric field, the ER fluid can be one of efficient materials in finishing processes. To finish small 3-dimensional structures such as the aspherical surface in optical elements, the possible arrangement of a tool, part and auxiliary electrode was described. We examined the influence of the addition of a few abrasive particles on the performance of the ER fluid by measuring yield stress and observed the behavior of abrasive particles in the ER fluid by a CCD camera, which had been also theoretically predicted from the electromechanical principles of particles. On the basis of the above results, the steady flow analysis around the rotating micro tool was performed considering the non-uniform electric field. Finally, borosilicate glass was finished using the mixture of the ER fluid and abrasive particles and material removal with field strength and surface roughness were investigated.

• Journal of Welding and Joining
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• v.35 no.3
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• pp.28-34
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• 2017

The authors derived the criteria on the process parameters of laser depositions with metal powers(SUS316L & IN718) by evaluating the surface and cross-section properties of the deposition layers. The surface characteristics of the deposition layer are investigated through optical microscopy by controlling the process parameters of laser output, powder feeding rate and gas feeding rate. The cross-section characteristics were also analyzed after polishing and chemical etching process. As the gas feeding rate increased, the amount of powder loss increased and the difference in the dilution ratio and heat affected zone depending on laser outputs was observed. In addition, the powder feeding rate used in the experiment did not interfere with the energy absorption of the base material.

• Nuclear Engineering and Technology
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• v.51 no.3
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• pp.877-883
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• 2019

Superconducting multi-spoke cavities are outstanding alternative choice for acceleration of heavy ions in medium velocity regimes. Based on the scheme of China ADS, several researches on the superconducting double-spoke cavities were done and two prototype cavities have been developed. In this paper, the RF design, the mechanical design and fabrication considerations of the bare cavity will be described in detail. After Buffered Chemical Polishing and High Pressure Rinsing, one of the prototype cavities was installed into the Vertical Test Stand for high gradient RF testing at 4.2 K. The measurement results of the quality factor as a function of the accelerating field and the maximum surface field will be presented. An accelerating gradient of more than 15 MV/m is achieved during the test, with maximum surface electric field of 58 MV/m, and maximum surface magnetic field of 117 mT.

• Restorative Dentistry and Endodontics
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• v.45 no.4
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• pp.52.1-52.11
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• 2020

Objectives: Yttria-stabilized tetragonal phase zirconia has been used as a dental restorative material for over a decade. While it is still the strongest and toughest ceramic, its translucency remains as a significant drawback. To overcome this, stabilizing the translucency zirconia to a significant cubic crystalline phase by increasing the yttria content to more than 8 mol% (8YTZP). However, the biocompatibility of a high amount of yttria is still an important topic that needs to be investigated. Materials and Methods: Commercially available 8YTZP plates were used. To enhance cell adhesion, proliferation, and differentiation, the surface of the 8YTZP is sequentially polished with a SiC-coated abrasive paper and surface coating with type I collagen. Fibroblast-like cells L929 used for cell adherence and cell proliferation analysis, and mouse bone marrow-derived mesenchymal stem cells (BMSC) used for cell differentiation analysis. Results: The results revealed that all samples, regardless of the surface treatment, are hydrophilic and showed a strong affinity for water. Even the cell culture results indicate that simple surface polishing and coating can affect cellular behavior by enhancing cell adhesion and proliferation. Both L929 cells and BMSC were nicely adhered to and proliferated in all conditions. Conclusions: The results demonstrate the biocompatibility of the cubic phase zirconia with 8 mol% yttria and suggest that yttria with a higher zirconia content are not toxic to the cells, support a strong adhesion of cells on their surfaces, and promote cell proliferation and differentiation. All these confirm its potential use in tissue engineering.

• The korean journal of orthodontics
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• v.27 no.5 s.64
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• pp.791-800
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• 1997

Sixty premolars extracted for orthodontic treatment were divided into four groups, and the residual resin was removed with four different rotary finishing instruments at a fixed speed of $18,500{\pm}300 rpm$ on the low speed handpiece. The instruments were G1; No.169L carbide fissure bur, G2: No.2 round bur, G3; No.4 round bur, G4: No.8 round bur. Then, the enamel received a S-second polishing with a rubber cup and a pumice. To find the extent of loss on the enamel at this point, prophylaxis was done with the rubber cup and pumice prior to bonding of the bracket(P1) and removal of residual resin by means of appropriate procedure applicable to each respective group(P2) followed. The final polishing was done with the rubber cup and pumice(P3), and the enamel surface roughness was measured each by the surface measuring instrument. The whole process was observed under a scanning electron microscope to gain the following results: At P2, the enamel surface roughness in G1 showed most smoothly with $2.60{\pm}0.55{\mu}m;\;in\;G2,\;3.24{\pm}0.80{\mu}m;\;in\;G3,\;3.44{\pm}0.94{\mu}m;\;in\;G4,\;3.89{\pm}0.54{\mu}m$, the roughest. G2 and G3 showed no statistical significance(P>0.05). At P3, the enamel surface roughness in G1 showed most smoothly with $2.29{\pm}0.47{\mu}m;\;in\;G2,\;2.44{\pm}0.56{\mu}m;\;in\;G3,\;2.44{\pm}0.56{\mu}m;\;in\;G4,\;2.92{\pm}0.43{\mu}m$, the roughest. G1 vs G2, G3, and G2 vs G3 had no statistical significances(p>0.05). In all groups, P2 and P3 showed rougher in surface roughness than P1, and P2 rougher than P3(p<0.01). In a case of 5-second prophylaxis with the rubber cup and the pumice on a virgin, normal enamel, fine scratches were found under the scanning electron microscope. In all four groups, unremovable gouges remained even after polishing with the ubber and pumice; residual resin was not observed with naked eye when finished with the rubber and pumice, but the resin debris was observed under the scanning electron microscope.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2016.11a
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• pp.153-153
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• 2016

Aluminum alloys have poor corrosion resistance compared to the pure aluminum due to the additive elements. Thus, anodizing technology artificially generating thick oxide films are widely applied nowadays in order to improve corrosion resistance. Anodizing is one of the surface modification techniques, which is commercially applicable to a large surface at a low price. However, most studies up to now have focused on its commercialization with hardly any research on the assessment and improvement of the physical characteristics of the anodized films. Therefore, this study aims to select the optimum temperature of sulfuric electrolyte to perform excellent corrosion resistance in the harsh marine environment through electrochemical experiment in the sea water upon generating porous films by variating the temperatures of sulfuric electrolyte. To fabricate uniform porous film of 5083 aluminum alloy, we conducted electro-polishing under the 25 V at $5^{\circ}C$ condition for three minutes using mixed solution of ethanol (95 %) and perchloric (70 %) acid with volume ratio of 4:1. Afterward, the first step surface modification was performed using sulfuric acid as an electrolyte where the electrolyte concentration was maintained at 10 vol.% by using a jacketed beaker. For anode, 5083 aluminum alloy with thickness of 5 mm and size of $2cm{\times}2cm$ was used, while platinum electrode was used for cathode. The distance between the two was maintained at 3 cm. Afterward, the irregular oxide film that was created in the first step surface modification was removed. For the second step surface modification process (identical to the step 1), etching was performed using mixture of chromic acid (1.8 wt.%) and phosphoric acid (6 wt.%) at $60^{\circ}C$ temperature for 30 minutes. Anodic polarization test was performed at scan rate of 2 mV/s up to +3.0 V vs open circuit potential in natural seawater. Surface morphology was compared using 3D analysis microscope to observe the damage behavior. As a result, the case of surface modification presented a significantly lower corrosion current density than that without modification, indicating excellent corrosion resistance.