• Title/Summary/Keyword: Surface leakage

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THE CHARACTERISTICS OF RESIN INFILTRATED INCIPIENT CARIOUS LESIONS (Resin infiltration을 시행한 법랑질 초기 우식 병소의 특성)

  • Kim, Eun-Young;Kwon, Min-Seok;Kim, Shin;Jeong, Tae-Sung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.39 no.1
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    • pp.1-10
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    • 2012
  • The concept of resin infiltration which was born in an innovative philosophy to arrest the incipient caries. However, the structural changes of resin infiltrated lesions have not yet explained completely. The liquid resin might contribute not only to maximizing the penetration but to deteriorating physical stability. This study was performed to examine some physical and histological features of resin infiltrated incipient carious lesions. With the specimen of resin infiltrated lesions, microhardness by nanoindentation in depth profile, morphology of resin tags were revealed after HCl dissolution, and degree of microleakage were assessed. The percentage of microhardness of surface layer and lesion body of untreated specimen to sound enamel was 64.6% and 24.6% respectively, while that of resin-infiltrated lesions was 72.1%, showing significant difference (p<0.05). The resin tags observed under SEM had relatively homogeneous length of 433(282~501) ${\mu}m$ on the average. Among 20 specimens for microleakage assessment, 13 specimens showed no leakage while 5 and 2 showed leakage into outer and inner half of lesion respectively. It was thought the infiltrant resin penetrates deeply and homogeneously into lesion body and improves its hardness with relatively good physical stability.

Preparation of CeO$_2$ Thin Films as an Insulation Layer and Electrical Properties of Pt/$SrBi_2$$Ta_2$$O_9$/$CeO_24/Si MFISFET (절연층인 CeO$_2$박막의 제조 및 Pt/$SrBi_2$$Ta_2$$O_9$/$CeO_24/Si MFISFET 구조의 전기적 특성)

  • Park, Sang-Sik
    • Korean Journal of Materials Research
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    • v.10 no.12
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    • pp.807-811
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    • 2000
  • CeO$_2$ and SrBi$_2$Ta$_2$O$_{9}$ (SBT) thin films for MFISFET (Metal-ferroelectric-insulator-semiconductor-field effect transistor) were deposited by r.f. sputtering and pulsed laser ablation method, respectively. The effects of sputtering gas ratio(Ar:O$_2$) during deposition for CeO$_2$ films were investigated. The CeO$_2$ thin films deposited on Si(100) substrate at $600^{\circ}C$ exhibited (200) preferred orientation. The preferred orientation, Brain size and surface roughness of films decreased with increasing oxygen to argon gas ratio. The films deposited under the condition of Ar:O$_2$= 1 : 1 showed the best C- V characteristics. The leakage current of films showed the order of 10$^{-7}$ ~10$^{-8}$ A at 100kV/cm. The SBT thin films on CeO$_2$/Si substrate showed dense microstructure of polycrystalline phase. From the C-V characteristics of MFIS structure with SBT film annealed at 80$0^{\circ}C$, the memory window width was 0.9V at 5V The leakage current density of Pt/SBT/CeO$_2$/Si structure annealed at 80$0^{\circ}C$ was 4$\times$10$^{-7}$ /$\textrm{cm}^2$ at 5V.

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Degradation from Polishing Damage in Ferroelectric Characteristics of BLT Capacitor Fabricated by Chemical Mechanical Polishing Process (화학적기계적연마 공정으로 제조한 BLT Capacitor의 Polishing Damage에 의한 강유전 특성 열화)

  • Na, Han-Yong;Park, Ju-Sun;Jung, Pan-Gum;Ko, Pil-Ju;Kim, Nam-Hoon;Lee, Woo-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.236-236
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    • 2008
  • (Bi,La)$Ti_3O_{12}$(BLT) thin film is one of the most attractive materials for ferroelectric random access memory (FRAM) applications due to its some excellent properties such as high fatigue endurance, low processing temperature, and large remanent polarization [1-2]. The authors firstly investigated and reported the damascene process of chemical mechanical polishing (CMP) for BLT thin film capacitor on behalf of plasma etching process for fabrication of FRAM [3]. CMP process could prepare the BLT capacitors with the superior process efficiency to the plasma etching process without the well-known problems such as plasma damages and sloped sidewall, which was enough to apply to the fabrication of FRAM [2]. BLT-CMP characteristics showed the typical oxide-CMP characteristics which were related in both pressure and velocity according to Preston's equation and Hernandez's power law [2-4]. Good surface roughness was also obtained for the densification of multilevel memory structure by CMP process [3]. The well prepared BLT capacitors fabricated by CMP process should have the sufficient ferroelectric properties for FRAM; therefore, in this study the electrical properties of the BLT capacitor fabricated by CMP process were analyzed with the process parameters. Especially, the effects of CMP pressure, which had mainly affected the removal rate of BLT thin films [2], on the electrical properties were investigated. In order to check the influences of the pressure in eMP process on the ferroelectric properties of BLT thin films, the electrical test of the BLT capacitors was performed. The polarization-voltage (P-V) characteristics show a decreased the remanent polarization (Pr) value when CMP process was performed with the high pressure. The shape of the hysteresis loop is close to typical loop of BLT thin films in case of the specimen after CMP process with the pressures of 4.9 kPa; however, the shape of the hysteresis loop is not saturated due to high leakage current caused by structural and/or chemical damages in case of the specimen after CMP process with the pressures of 29.4 kPa. The leakage current density obtained with positive bias is one order lower than that with negative bias in case of 29.4 kPa, which was one or two order higher than in case of 4.9 kPa. The high pressure condition was not suitable for the damascene process of BLT thin films due to the defects in electrical properties although the better efficiency of process. by higher removal rate of BLT thin films was obtained with the high pressure of 29.4 kPa in the previous study [2].

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The Contamination Characteristics of BTEX and TPH Components in Silty Soils with the Oil Leakage Event from Point Source (점오염원 형태의 유류누출 사건에 의한 실트질 토양층에서 BTEX와 TPH 성분의 오염도 연구)

  • Kang, Dong-Hwan;Chung, Sang-Yong;Go, Dong-Ho
    • The Journal of Engineering Geology
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    • v.16 no.4 s.50
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    • pp.393-402
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    • 2006
  • The contamination characteristics of BTEX and TPH components in silty soils with the oil leakage event from point source were studied. The over ratios of three soil pollution standard for TPH component were $1.5{\sim}1.7$ times higher than that of BTEX component. The mean and maximum values of BTEX and TPH components with sample points were B-zone > A-zone > C-zone, and the highest concentrations were measured at $1{\sim}2m$ depth below surface. BTEX and TPH components were increased with linear distance in zone within 120 m and 80 m from point source. For the zone more than 120 m, BTEX and TPH concentrations were under soil pollution standard. The cutoff values of indicator kriging using BTEX and TPH components were defined as confirmative limit, warn- ing limit and counterplan limit. The variograms of indicator-transformed data were selected linear model. The contamination ranges of BTEX and TPH components using confirmative limit and warning limit were estimated similar, but the contamination range of those using counterplan limit was much reduced. The maximum contamination probabilities were estimated by probability maps usinB confirmative limit, warning limit and counterplan limit. The maximum contamination probabilities with three soil pollution standard were estimated 26%, 26% and 13% for BTEX component, and 44%, 38% and 26% for TPH component.

Transgastric Endoscopic Cholecystectomy in a Dog : Natural Orifice Transluminal Endoscopic Surgery (개에서 내시경을 이용한 경위장관 담낭절제술 1예 : 자연개구부 내시경수술)

  • Jeong, Seong-Mok;Kim, Young-Ill;Lee, Jae-Yeon;Jee, Hyun-Chul;Park, Ji-Young;Park, Jong-Heon;Kim, Ji-Yeon;Lee, Sang-Il;Kim, Myung-Cheol;Shin, Sang-Tae;Lee, Young-Won
    • Journal of Veterinary Clinics
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    • v.24 no.3
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    • pp.315-319
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    • 2007
  • Transgastric endoscopic cholecystectomy was successfully accomplished in a 1-year-old, 15 kg, female, mongrel dog. Single-working channel flexible gastric endoscope was used with the aid of one abdominal laparoscopic port. Gastrotomy was performed using endoscopic needle knife at the ventral antral region. Through the gastric incision endoscope was advanced and retroflexed for the visualization of gallbladder. For the better exposure of surgical field, gentle traction was applied at the fundus of the gallbladder using laparoscopic grasping forceps. Cystic duct and artery was ligated using endoclips. After transecting the duct and artery, gallbladder was dissected using endoscopic coagulating grasping forceps and needle knife. Resected gallbladder was retrieved through the mouth and gastric incision site was sutured using endoclips. There was no evidence of bile leakage or stomach leakage on postoperative day (POD) 3. On POD 16, gastric endoscopy and laparoscopy was performed. Gastric endoscopy revealed complete adhesion of incision site. The content of the peritoneum appeared healthy, with no sign of infection, bile staining, or organ injury. The omentum was adhered over resected gallbladder fossa and the serosal surface of gastrotomy site. This is the first report of NOTES cholecystectomy in the dog and provides new concept of cholecystectomy of the dog.

Geomechanical Stability of Underground Lined Rock Caverns (LRC) for Compressed Air Energy Storage (CAES) using Coupled Thermal-Hydraulic-Mechanical Analysis (열-수리-역학적 연계해석을 이용한 복공식 지하 압축공기에너지 저장공동의 역학적 안정성 평가)

  • Kim, Hyung-Mok;Rutqvist, Jonny;Ryu, Dong-Woo;Synn, Joong-Ho;Song, Won-Kyong
    • Tunnel and Underground Space
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    • v.21 no.5
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    • pp.394-405
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    • 2011
  • In this paper, we applied coupled non-isothermal, multiphase fluid flow and geomechanical numerical modeling using TOUGH-FLAC coupled analysis to study the complex thermodynamic and geomechanical performance of underground lined rock caverns (LRC) for compressed air energy storage (CAES). Mechanical stress in concrete linings as well as pressure and temperature within a storage cavern were examined during initial and long-term operation of the storage cavern for CAES. Our geomechanical analysis showed that effective stresses could decrease due to air penetration pressure, and tangential tensile stress could develop in the linings as a result of the air pressure exerted on the inner surface of the lining, which would result in tensile fracturing. According to the simulation in which the tensile tangential stresses resulted in radial cracks, increment of linings' permeability and air leakage though the linings, tensile fracturing occurred at the top and at the side wall of the cavern, and the permeability could increase to $5.0{\times}10^{-13}m^2$ from initially prescribed $10{\times}10^{-20}m^2$. However, this air leakage was minor (about 0.02% of the daily air injection rate) and did not significantly impact the overall storage pressure that was kept constant thanks to sufficiently air tight surrounding rocks, which supports the validity of the concrete-lined underground caverns for CAES.

Applicability of Composite Polyurea Method Considering the Required Performance in Underground Parking Lot Upper Slab (공동주택 지하주차장 상부슬래브의 요구성능을 고려한 복합형 폴리우레아 공법의 적용성 검토)

  • Lee, Jung-Hun;Choi, Eun-Kyu;Song, Je-Young;Kim, Soo-Yeon;Oh, Sang-Keun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.3
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    • pp.243-254
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    • 2019
  • In this study, problems of the waterproofing methods in which water leakage occurs in the upper slab of the underground parking lot of apartment houses and the requirements considering the characteristics of the upper slab, and selected the appropriate performance(proposal) for the composite polyurea process are reviewed. As a result of the study, it is necessary to review performance such as responsiveness to upper slab of the multi-unit underground parking lot that is comprised of (1) crack and behavior responsiveness, (2) surface integrity, (3) vertical watertight stability, (4) pressure layer construction, (5) impact and pressure response and (6) vehicle moving load. As a result of evaluating 5 items corresponding to the requirements for the soft and hard complex polyurea, all of them were found to meet the conditions, and each materials were improved by compounding the materials that had problems when applying a single-ply method, thereby clarifying the advantages and disadvantages of the material property. However, in order to apply to the actual site, additional evaluation on site applicability such as mock-up evaluation should be conducted, and subsequent studies on the applicability of the market through review of economic feasibility and maintenance is required.

Study on safety performance evaluation of stationary SOFC stack (건물용 고체산화물연료전지 스택 안전성능평가 연구)

  • Park, Tae Seong;Lee, Eun Kyung;Lee, Seung Kuk
    • Journal of Energy Engineering
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    • v.27 no.4
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    • pp.1-12
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    • 2018
  • The code and standards related to fuel cells were analyzed to derive the SOFC(Solid Oxide Fuel Cell) stack safety performance evaluation items and evaluation methode. Safety performance evluation of the SOFC stack was tested by quoting derived test items. The stack used in the test is an anode-supported type 2 Cell stack (Active surface area : 220cm) manufactured by MICO Inc, and SOFC stack safety performance evaluation system used for the test is self-manufactured. We conducted a leakage test, current voltage characteristic test, rated output test, and power response characteristics test. In the safety performance evaluation test, the stack showed no gas leakage, the maximum output and rated output was recorded to 65.6 W(1.41 V, 46.5 A, $422mA/cm^2$), 62.3 W(1.57 V, 40 A, $363mA/cm^2$). In the power response characteristics test verified that the output is kept stable within two seconds. At the maximum load (40 A) and the minimum load (8 A), the output was recorded 62 W and 16W in $750^{\circ}C$. This study will contribute to the universalization and to provide much safe environment of operating the solid oxide fuel cell system.

Evaluation of the Pull-out Resistance of the SMA Wire Connector (SMA 와이어를 이용한 연결재의 인발저항성능 평가)

  • Jung, Chi-Young;Woo, Tae-Ryeon;Lee, Jong-Han;Cheung, Jin-Hwan
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.1
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    • pp.130-137
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    • 2019
  • Precast concrete (PC) structure is one of the type of the structures which is made in a facility prior to installing it to a construction field. The contact surfaces between two PC structures should be treated for obtaining enough binding force by inducing prestressing force. However, in the many cases, the contact surface causes the crack and leakage of water. These cracks and water leakage can cause the corrosion of the rebar, and the corrosion of the rebar can severely reduce the long-term durability. In this study, the SMA wire connector is suggested to solve the problem with the contact surfaces between two PC structures. The pull-out resistance of the suggested SMA wire connector is evaluated by conducting the tests to find the effect of the number of wires, shape of connector part, and shape memory effect. As a result of this study, the empirical formula is suggested to estimate the pull-out resistance related with the effects of the shape of the connector, shape memory effect, and the adhesive force. The validity between the estimated pull-out resistance and the measured value is confirmed.

The Study on Thermal Shock Test Characteristics of Solar Cell for Long-term Reliability Test (장기 신뢰성 평가를 위한 태양전지의 열충격 시험 특성에 관한 연구)

  • Kang, Min-Soo;Kim, Do-Seok;Jeon, Yu-Jae;Shin, Young-Eui
    • Journal of Energy Engineering
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    • v.21 no.1
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    • pp.26-32
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    • 2012
  • This study has been performed Thermal Shock test for analyze the cause of Power drop in PV(Photovoltaic) Module. Thermal Shock test condition was performed with temperature range from $-40^{\circ}C{\sim}85^{\circ}C$. One cycle time is 30min. which are consist of low and high temperature 15min. each other. The test was performed with total 500cycles. EL, I-V were conducted every 100cycle up to 500cycles. Mono Cell resulted in 8% Power drop rates in Bare Cell and 9% in Solar Cell. In the case of Multi Cell resulted in 6% Power drop rates in Bare Cell and 13% in Solar Cell. After Thermal Shock test, Solar Cell's Power drop resulted from surface damages, but in the case of Bare Cell's Power drop had no surface damages. Therefore, Bare Cell's Power drop was confirmed as according to leakage current increase by analysis of Fill Factor after Thermal Shock test. Also, Solar Cell's Power drop rates are higher than that of Bare Cell because of surface damages and consuming electric power increase. From now on, it should be considered that analyzed the reasons of Fill Factor decrease and irregular Power drop in PV module and Cell level using cross section, various conditions and test methods.