• Journal of Technologic Dentistry
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• v.44 no.4
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• pp.111-117
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• 2022

Purpose: This study was conducted to compare the Vickers hardness on the denture acrylic resins using the glaze color system. Methods: The specimens (20×2 mm) were prepared by mixing according to the manufacturer's protocols through thermal polymerization and self-polymerization. The surface roughness was measured using a testing machine after water-soaking for 48 hours. For the Vickers hardness measurement, the completed specimen was soaked in water for 48 hours and then applied at 200 gf for 30 seconds. Was the specimen immersed after being soaked in water for 48 hours at temperatures of 5℃ and 55℃, respectively, for 30 seconds for the thermos-cycling treatment, and it was carried out 5,000 times. Results: Surface roughness was higher in the more glazing group than in the control group. A significant difference was observed in all groups, except for the Retec Don 2000 and Luciton 199 groups (p<0.05). As a result of measuring the Vickers hardness, the treatment by glaze color showed slightly lower but the thermo-cycling treatment group appeared higher than control group in all. Conclusion: Therefore, the glaze color was found to affect the surface roughness and showed a significant difference. The surface glaze color showed a very high Vickers hardness after the thermo-cycling treatment, indicating that the surface-strengthening effect is greater in the oral environment.

• Restorative Dentistry and Endodontics
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• v.14 no.1
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• pp.179-188
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• 1989

The purpose of this study was to measure Micro vicker's hardness of 4 kinds of anterior Composite resins (Pyrofil light bond anterior, Lite-fil anterior, Photo clear fil anterior, Silux) and 6 kinds of posterior Composite resin (Pyrofil light bond posterior. Lite-fil posterior, Photo clear fil posterior, Occlusin posterior, Palfique light posterior, P-30, posterior) according to deference of depth and distance of light tip from surface of composite resin. Each composite resin was filled into Teflon tube of 5mm in diameter and 5mm in depth, celluloid matrix was covered and the light in accordance with each composite resin was irradiated in distance of zero millimeter and 1 cm from light tip to surface of composite resin for 30 seconds. Specimens were sectioned longitudinally with cutting device. Microvicker's hardness measurements ware made at the depth of surface, 1mm, 2mm, 3mm, 4mm and 5mm from the surface to deep portion. Vicker's hardness numbers were taken on each depth under 200gm load for 30 seconds with MVK-E. The following results were: 1. The highest hardness value was measured at 1 mm depth. Then the deeper the depth, the lesser the hardness was observed. 2. The hardness value of anterior composite resins is lower than one of posterior composite resins. 3. Hardness number of composite resin irradiated in distance of zero millimeter from surface of composite resin was higher than one of 1 cm from surface of composite resin. 4. The pattern of hardness change at varying depth was similar to all the experimental material with no relation to distance of light from specimen.

• The Journal of Korean Academy of Prosthodontics
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• v.33 no.3
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• pp.569-583
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• 1995

Disinfection of dental impressions are necessary due to contamination with patient’s saliva and blood, which is a potential for cross-infection. The purpose of this study was to evaluate the effects of disinfection of four hydrophilic rubber impression materials with three disinfecting solutions, on the dimensional stability and surface hardness of improved stone casts. Three hydrophilic vinyl polysiloxane impression materials(Express, Reprosil, Exafine) and one polyether impression material(Impregum-F) were mixed according to the manufacturer’s directions and impressions were made on a ADA specification No. 19 stainless-steeldie. On removal of the impressions, each impression was immersed in one of the disinfectants(Banicide, Potadine, Clorox) for 10 minutes. After disinfection, type IV improved stone. casts were poured. On this cast, the linear dimension and surface hardness were measuredusing a Measurescope(Nikon, Japan) and a Barcol hardness tester(Barber, Colman Co U. S. A). The results were as follows : 1. The improved stone casts from disinfected Reprosil and Impregum-F impression material did not show dimensional changes(P>0.01). Those from disinfected Express and Exafine impression material showed dimensional changes(P<0.01). The amount of shrinkage was not clinically significant. 2. The improved stone casts from disinfected Express impression material did not exhibit changes in surface hardness(P>0.01), but those from disinfected Reprosil, Exafine, Imp regnum-F impression material showed changes in surface hardness(P<0.01). 3. The dimensinal stability and surface hardness of the improved stone casts were satisfactory using Banicide on Express, all disinfectants used in this study on Reprosil, Potadin and Clorox on Exafine, Banicide and Clorox on Impregum-F. According to these results, immersion disinfection of hydrophilic rubber impression mate rials did not adversely affect the resultant casts. Nevertheless compatibility tests of impression materials and disinfectants should be done when disinfecting impressions.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.24 no.6
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• pp.625-631
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• 2015

The hardness of surface treated magnesium alloy was evaluated using laser induced breakdown spectroscopy. The surface of the specimen was hardened mechanically, and the hardness profiles were measured using a traditional measurement technique. A laser beam was irradiated to generate a plasma, and the peaks of the components of the specimen were analyzed. A wavelength of 333.66 nm and 293.65 nm were selected as the atomic and ionic peaks, respectively. The ratios of the ionic peak to the atomic peak were obtained so as to compare the hardness profile. As the depth increased, the ratio decreased. These results are in good agreement with the previous hardness measurement results. It can be considered that this technique could be applied for remote and time-efficient hardness measurement.

• Transactions of the Korean Society of Mechanical Engineers
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• v.11 no.6
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• pp.935-944
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• 1987

The surface rolling, one of the plastic working processes, provides good surface roughness with the reduction of diameter and the increase of surface hardness. In this study three Nachi 6000ZZ bearing were used for surface rolling on ductile cast iron. The results obtained are as follows; (1) The good surface roughness can be obtained with roller surface radius of curvature of 24mm after the 2nd rolling. (2) The surface roughness of ductile cast iron was 0.48.mu.mRmax by the contact pressure of 140kgf/mm$^{2}$ and surface hardness was Hv 395 with roller surface radius of curvature of 24mm after the 2nd rolling. (3) The reduction of specimen diameter of ductile cast iron were -12.8.mu.m due to rolling. (4) Within the diameter variation of -11.mu.m, surface roughness and surface hardness were increased, but at the range of exceeding -14.mu.m of the diameter variation the surface roughness became worse and the surface roughness became worse and the surface hardness was increased. (5) Dynamic contact area was about 25% to 30% of static contact area. The calculated contact pressure showed a good agreement with the experimental contact pressure.

• Tribology and Lubricants
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• v.34 no.6
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• pp.262-269
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• 2018

In this work the friction and wear characteristics of the gray cast iron surface processed by broaching method, which is widely used in the machinery industry, were investigated. The broaching process is mainly used for mass production because it has high dimensional accuracy and processing speed, but the defects on surface can be easily generated. In order to improve the tribological characteristics, the approach was to reduce the roughness and hardness of the surface by adding a machining process to the broaching specimen. The secondary machining process using abrasive grains produces low roughness and hardness than broaching because it has high tool accuracy and removes the work hardened surface. The friction coefficient and the wear rate were assessed using a reciprocating-type tribotester to analyze the effects of surface finishing on the tribological properties. The friction tests were conducted under dry and lubricated conditions. The test results showed that the reduction of surface roughness and hardness through secondary machining process in lubricated condition improved the friction and wear characteristics. The reason why the same results did not appear in a dry condition was that wear occurred more rapidly than in lubricated condition. Thus, the positive effect of roughness and hardness of the surface obtained through the secondary machining process was not observed.

• Journal of the Korean Society of Safety
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• v.2 no.1
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• pp.31-41
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• 1987

The surface rolling method which is one of the plastic deformation processes increases the surface roughness with reduction of diameter and hardness. In this study, three NACHI 6000 ZZ bearing were used for surface rolling tool on a mild steel. The following results have been obtained with the mild steel. 1) The load is major factor in getting fine surface roughness of roller fininshing after grinding. The optimal surface roughness of SS40 steel can be obtained at the contact pressure of $210kgf/cm^2$. But, Better surface roughness can not be expected, Due to flaking phenomena at more than 300 kgf/cm of contact pressure. 2) At the contact pressure range of $200kgf/cm^2{\sim}210kgf/cm^2$ for optimal surface roughness, The surface hardness increased to Hv 200~Hv 240 from Hv 125 before surface rolling. 3) Within the diameter variation of $13{\mu}m$ the surface roughness and the surface hardness were increased, but out of variation of $14{\mu}m$. The surface roughness become worse and the surface hardness was increased.

• Journal of the Korean institute of surface engineering
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• v.36 no.2
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• pp.206-213
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• 2003

Effects of plasma nitriding on the surface characteristics of tool steels have been investigated using wear tester, micro-hardness tester and scanning electron microscope (SEM) Commercial SKD 11 and SM45 alloy were used as specimens and were plasma nitrided using a plasma nitriding equipment for 5 hr and 10hr at $500^{\circ}C$. Microstructure and phase analysis were performed using SEM and XRD. It was found that plasma nitriding for lour at $500^{\circ}C$, compared with plasma nitriding for 10hr at $500^{\circ}C$, had a thick nitrided layer and produced a layer with good wear resistance and hardness as nitriding time increased. SKD11 alloy showed that wear resistance and hardness decreased, whereas surface roughness increased, compared with SM45 alloy.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2002.10b
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• pp.157-158
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• 2002

A surface hardenable low alloy carbon steel was implanted with medium energy (20 - 50KeV) $N_2^+$ ions to produced a modified hardened surface. The implantation conditions were varied and are given in several doses. The surface hardness of treated and untreated steels were measured using depth sensing ultra micro indentation system (UMIS). It is shown that the hardness of nitrogen ion implanted steels varied from 20 to 50GPa depending on the implantation conditions and the doses of implantation. The structure of the modified surfaces was examined by X-ray photoelectron spectroscopy (XPS). It was found that the high hardness on the implanted surfaces was as a result of formation of non-equilibrium nitrides. High-resolution XPS studies indicated that the nitride formers were essentially C and Si from the alloy steel. The result suggests that the ion implantation provided the conditions for a preferential formation of C and Si nitrides. The combination of evidences from nano-indentation and XPS, provided a strong evidence for the existence of $sp^3$ type of bonding in a suspected $(C,Si)_xN_y$ stoichiometry. The formation of ultra hard surface from relatively cheap low alloy steel has significant implication for wear resistance implanted low alloy steels.

• Journal of Technologic Dentistry
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• v.27 no.1
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• pp.73-78
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• 2005

The surface-reacted layer of titanium castings greatly affects their mechanical properties. This study analyzed the interfacial zone of Ti-20%Zr-5%Cr alloy castings obtained from phosphate bonded investment and examined the relationship between the surface-reacted layer and hardness. The Vickers hardness of cast disks were tested at 20$\mu m$ intervals from the surface to 120$\mu m$ in depth. The cross-section was observed metallurgically, and line profile of the reacted layer was conducted under the EDX. The surface-reacted layer of Ti-20%Zr-5%Cr alloy is showed a similar tendency to Ti-6%Al-4%V alloy in thickness, and also Si diffusion in multiple reacted layer of Ti-20%Zr-5%Cr alloy is less than cp Ti and similar to Ti-6%Al-4%V alloy. The Vickers hardness in the surface layer was greater than in the inner part, and the Vickers hardness of Ti-20%Zr-5%Cr alloy ranged 650 to 390 and cp Ti ranged 810 to 160, Ti-6%Al-4%V alloy ranged 710 to 530 respectively.