• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1997.04a
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• pp.150-155
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• 1997

Rapid Prototyping(RP) is the technique which is used to make prototypes or functional parts directly using the 3-D solid data. Before building the prototype, several processes such as transfering 3D data from CAD system(STL) determination of build-direction, adding support structure and slicing are required. Among the above processes. determination of build-direction is the target of this study. The build direction is determined by many factors according to the objective of the user, like part accuracy, number of support structure, build time, amount of trapped volume, etc, But it is not easy to determine the build-direction because there are many factors and some factors have dependent properties with one another. So, in this study the part accuracy, the number of support structures and build time are considered as the main factor to determine the optimal build-direction. To determine the optimal build-direction for increasing part accuracy, sum of projected area which caused stairstepping effect was considered. The less the projected area is the better part accuracy is About the optimal build-direction to minimize the amount of support structure, sum of projected area of facets that require support structures was considered. About the build time, we considered the minimum height of part we intended. About the build time, we considered the minimun height of part we intended to make.

• Bulletin of the Korean Chemical Society
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• v.32 no.2
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• pp.673-680
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• 2011

The compound 3-(2-Mercaptopyridine)phthalonitrile has been synthesized and characterized by IR, UV-vis, and X-ray single-crystal determination. The molecular geometry from X-ray determination of the title compound in the ground state has been compared using the Hartree-Fock (HF) and density functional theory (DFT) with the 6-31G(d) basis set. The calculated results show that the DFT and HF can well reproduce the structure of the title compound. The energetic behavior of the title compound in solvent media was examined using the B3LYP method with the 6-31G(d) basis set by applying the Onsager and polarizable continuum model. Using the TD-DFT and TD-HF methods, electronic absorption spectra of the title compound have been predicted and good agreement with the TD-DFT method and the experimental determination was found. The predicted nonlinear optical properties of the title compound are much greater than those of urea. Besides, molecular electrostatic potential of the title compound were investigated by theoretical calculations. The thermodynamic properties of the compound at different temperatures have been calculated and corresponding relations between the properties and temperature have also been obtained.

• Journal of the Korean Wood Science and Technology
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• v.42 no.2
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• pp.183-192
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• 2014

For the structure determination of D-(+)-sucrose, which consists of ${\alpha}$-D-(+)-glucose and ${\beta}$-D-(+)-fructose, it was acetylated with acetic anhydride and triethyl amine, pyridine, zinc chloride, and sodium acetate as catalysts. The acetylated D-(+)-sucrose was acid-hydrolyzed using sulfuric acid and sodium chloride in methanolic solution. The structures of the reaction products were determined by $^1H$-NMR and $^{13}C$-NMR spectra. The yield of the acetylation indicated the high value in zinc chloride as 70% in zinc chloride catalyst. The acid-hydrolyzed product of the acetylated D-(+)-sucrose, 2,3,4,6,1',3',4',6'-octa-O-acetyl-D-(+)-sucrose, gave 2,3,4,6-tetra-O-acetyl-${\beta}$-D-(+)-glucose and it suggests that the acetylated D-(+)-sucrose was rearranged through the formation of oxonium ion by mutarotation in the 2,3,4,6-tetra-O-acetyl-${\alpha}$-D-(+)-glucose moiety and through the ring opening in the 1',3',4',6'-tetra-O-acetyl-${\beta}$-D-(+)-fructose moiety.

• Composites Research
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• v.17 no.1
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• pp.1-9
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• 2004

A new non-destructive evaluation method using tapping sound is proposed. This method, named Tapping Sound Analysis, is using the difference between tapping sound data of healthy structure and defective structure as the criteria of determination of internal defect of composite structure. For the characterization of tapping sound, a feature extraction method based on wavelet packet transform is proposed. And a feature index is defined for the decision of existence of internal defects. To prove the possibility of proposed method as a non-destructive evaluation method, experimental study is performed. The tapping sound data of healthy structure and defective structure are measured and compared based on the proposed decision method. The experimental results showed that the feature index is a good indicator for the determination of internal defects.

• International journal of advanced smart convergence
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• v.11 no.3
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• pp.119-131
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• 2022

The purpose of this study is to analyze the difference in the degree of self-determination between the criteria that general high school students consider important when selecting subjects (hereinafter referred to as 'importance') and the criteria that are actually applied when selecting subjects (hereinafter referred to as 'implementation'), based on the existing motivation type discrimination scale and subject selection criteria scale. As a result of analysis based on the data of a total of 786 high school students, the degree of self-determination was found to be different for all 34 questions and 8 factors in importance and implementation. In general, the questions and factors showed a simple structure with the motivation types and showed the lowest correlation with the motivations at both ends of the self-determination continuum. Among the factors that students consider important when selecting subjects and the factors that are actually applied, the 'SAT' factor showed the highest positive correlation with identification control. In addition, it was found that autonomous subject selection was more preferred than subject selection based on extrinsic motivation. These results are not only meaningful as the first study to analyze the degree of self-determination in the subject selection of high school students, but also can be used as useful data for customized subject selection guidance according to the degree of self-determination. The implications of this study and suggestions for follow-up studies were discussed.

• Journal of Microbiology and Biotechnology
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• v.18 no.10
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• pp.1655-1658
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• 2008

Cyanobacteria, blue-green algae, are a rich source of bioactive secondary metabolites with many potential applications. The ubiquitin-proteasome proteolytic system plays an important role in selective protein degradation and regulates cellular events including apoptosis. Cancer cells are more sensitive to the proapoptotic effects of proteasome inhibition than normal cells. Thus, proteasome inhibitors can be potential anticancer agents. Cyanobacteria have been shown to be a rich source of highly effective inhibitors of proteases. A proteasome inhibitor was screened from an extract of the culture of Scytonema hofmanni on the basis of its inhibitory activity, which led to the isolation of nostodione A with an $IC_{50}$ value of 50${\mu}M$. Its structure was determined by spectroscopic methods such as $^{1}H$-NMR and ESI-MS spectral analyses.

• Bulletin of the Korean Chemical Society
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• v.32 no.11
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• pp.4021-4026
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• 2011

Functions of the luteinizing hormone releasing hormone (LHRH) and its induced release by divalent metal ions have received great attention because this neurotransmitter subsequently regulates the secretion of luteinizing hormone (LH). Metal-LHRH complexes were synthesized by addition of various Cu(II),Ni(II),Zn(II) ions into LHRH in order to understand how the induced release of LHRH is possible. The degree of complexation was monitored by $^1H$, $^{13}C$-NMR chemical shifts, and final products were identified by Mass spectrometry. Solutionstate structure determination of Zn(II)-LHRH out of metal-complexes was accomplished by using NMR and NMR-based distance geometry (DG). Interproton distance information from nuclear Overhauser effect spectroscopy was utilized for structure determination. Structure obtained in this study has a cyclic conformation exhibiting a specific ${\alpha}$-helical turn with residue numbers His[2]-Leu[7] out of 10 amino acids. Comparison of chemical shifts and EPR studies of Ni(II),Cu(II)-LHRH complexes exhibit that these metal complexes have 4-coordination geometry.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.8
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• pp.88-101
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• 1998

In this paper, module of a product is determined by the characteristics of a product itself and art assembly process. To analyze the characteristics o( the product, assembly function, structure of subassembly and parts could be considered. Based on the analysis of characteristics of product structure, assembly process and product function, determination criteria of a module could be proposed. For the assembly process, assembly methods, assembly equipment and workers could be considered. For the product structure, constituent object and structural feature could also be considered. To obtain the interrelationship between the product and the assembly process, the matrix table could be used to find the influencing factors that affected the module.

• 한국생물공학회:학술대회논문집
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• 2005.04a
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• pp.518-518
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• 2005

• Proceedings of the Microbiological Society of Korea Conference
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• 2004.05a
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• pp.55-58
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• 2004