• Title/Summary/Keyword: Steam heat treatment

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마도1호선에서 출수된 죽찰의 보존처리 (Conservation of Bamboo Slips excavated from Mado Shipwreck No.1)

  • 윤용희;김응호;차미영
    • 보존과학연구
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    • 통권37호
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    • pp.17-26
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    • 2016
  • 태안 해역의 마도1호선에서는 해양에서 처음으로 총 57점의 죽찰이 출수되었다. 죽찰의 수량이 많아 세척과정 중 유물 상태를 관찰하여 부후정도에 따라 그룹화한 후 순차처리하였다. 또한 치수안정화과정에서 부후가 많이 진행된 죽찰은 PEG 4000, 부후가 많이 진행되지 않은 죽찰은 PEG 2000으로 처리하였다. 진공동결건조 후 PEG 4000으로 처리한 죽찰은 공업용 열풍기를 이용해 표면처리를 실시하였는데 일부는 재색이 많이 어두워졌다. 이를 보완하고자 스팀다리미를 이용하여 표면처리를 실시하였다. 스팀다리미로 표면처리한 죽찰은 재색을 잘 유지하였다. 처리 완료 후 일부 죽찰은 두께에 비해 길이가 긴 편이라 처리 후 무게를 지지해주는 견고성이 많이 떨어졌다. 이런 경우 유물의 이동과정이나 전시 중 유물이 더 손상되는 결과를 가져올 수 있어서 견고성을 더 높여주며 형태유지를 할 수 있는 방법을 찾고자 하였다. 따라서 묵서가 없는 면인 최외층에 100% PEG 2000 용액을 접착제로 사용하여 레이온지를 배접하는 방식을 취하였다. 이는 견고성을 높이면서 형태유지에도 좋은 효과를 보였다.

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Life cycle impact assessment of the environmental infrastructures in operation phase: Case of an industrial waste incineration plant

  • Kim, Hyeong-Woo;Kim, Kyeong-Ho;Park, Hung-Suck
    • Environmental Engineering Research
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    • 제22권3호
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    • pp.266-276
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    • 2017
  • A life cycle impact assessment was applied in an industrial waste incineration plant to evaluate the direct and indirect environmental impacts based on toxicity and non-toxicity categories. The detailed life cycle inventory of material and energy inputs and emission outputs was compiled based on the realistic data collected from a local industrial waste incineration plant, and the Korean life cycle inventory and ecoinvent database. The functional unit was the treatment of 1 tonne of industrial waste by incineration and the system boundary included the incineration plant and landfilling of ash. The result on the variation of the impact by the unit processes showed that the direct impact was decreased by 79.3, 71.6, and 90.1% for the processes in a semi dry reactor, bag filter, and wet scrubber, respectively. Considering the final impact produced from stack, the toxicity categories comprised 91.7% of the total impact. Among the toxicity impact categories, the impact in the eco-toxicity category was most significant. A separate estimation of the impact due to direct and indirect emissions showed that the direct impact was 97.7% of the total impact. The steam recovered from the waste heat of the incineration plant resulted in a negative environmental burden.

증발식 해수담수화설비의 에너지 소모량에 관한 연구 (A study on the required energy of a thermal type desalination plant)

  • 송치성
    • Journal of Advanced Marine Engineering and Technology
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    • 제38권9호
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    • pp.1094-1100
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    • 2014
  • 오폐수처리, 해수담수화 및 식품산업의 경우 증발과정은 필수공정이며, 이는 기본적으로 용액으로부터 용매인 순수한 물성분을 추출하여 점차 용액의 농도를 증가시키는 방식이다. 농축을 위한 방식은 전기투석, 증발식, 막방식 등의 다양한 방법이 사용되고 있으나, 본 연구에서는 여러 산업분야에서 적용되고 있는 증발식을 대상으로 운전방식에 따른 가열열원의 소모량을 이론적으로 분석하고, 이에 근거하여 다단증발식 해수담수화설비의 운전특성을 파악하였다. 본 연구의 결과에 따르면 시스템에서 이용할 수 있는 전체 온도차, 즉 인입해수의 온도와 1단 증발부로 유입되는 해수온도와의 차를 기준으로 증발단의 수를 증가시킬수록 에너지효율이 상승함을 알 수 있었다.

2.25% Cr-1%Mo 합금계 열연강판 제조기술 (Manufacturing 2.25Cr-1Mo Steel In Hot Rolling Strip Mill)

  • 노태훈
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1999년도 제3회 압연심포지엄 논문집 압연기술의 미래개척 (Exploitation of Future Rolling Technologies)
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    • pp.390-398
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    • 1999
  • The thermomechanical control process(in hot rolling strip mill) was employed to produce 2.25Cr-1Mo steel, which is to be construction material for the steam generator for power plant. Although the Conventional processes has been the primary means of producing the 2.25Cr-1Mo steel, an alternative method was used to meet the specification of ASTM heat treatment for A387-22-Classl using autotempering after coiling in hot rolling strip mill. The microstructures, tensile properties at various temperatures, and creep-rupture properties have been investigated to compare the properties with those of materials produced by the conventional process and to certify the application of the thermomechanical control process to an actual process of manufacturing 2.25-Cr-1Mo steel, this in turn, will reduce the cost of the process. About 14 to 34% glanular bainite (remainder proetectoid ferrite) formed in a coil, and this variety of volume fraction stems from the different cooling rates, which varies with position of the coil after coiling. Tensile testing from room temperature to 700$^{\circ}C$ indicated that strength increases with test temperature showing peaks at around 600$^{\circ}C$. Creep-rupture properties have been being investigated at the temperature of 500$^{\circ}C$ with 27.5, 32kg/$\textrm{mm}^2$ loads and have showed no rupture for over 1000 hours.

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Effect of Intercritical Annealing on the Dynamic Strain Aging(DSA) and Toughness of SA106 Gr.C Piping Steel

  • Lee, Joo-Suk;Kim, In-Sup;Park, Chi-Yong;Kim, Jin-Weon
    • Nuclear Engineering and Technology
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    • 제32권1호
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    • pp.77-87
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    • 2000
  • It is reported that the toughness and safety margins of the SA106 Gr.C main steam line piping steel is reduced due to dynamic strain aging (DSA) at the reactor operating temperature for Leak-Before-Break (LBB) application. In this study, intercritical annealing in two-phase ($\alpha$+${\gamma}$)region was performed to investigate the possibility of improving the toughness and reducing DSA susceptibility. The manifestations of DSA were still observed in the tensile tests of the annealed specimens. However, the ductility loss caused by DSA was smaller than that in the as-received material. Furthermore, the intercritical annealing was able to increase the Charpy impact toughness by 1.5 times compared to as-received. With the heat treatment, we could obtain microstructural changes such as the cleaner retained ferrite, increased ferrite content and somewhat finer grain size. It is considered that the reduced DSA was induced by cleaner retained ferrite, which in turn resulted in higher impact toughness in addition to the general toughening due to finer grain sizes and increased ferrite content.

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Hexachlorocyclophosphazene과 Triethanolamine을 이용한 면섬유의 포름알데히드-프리 내구성 방염가공 (Formaldehyde-Free Durable Flame-Retardant Finish of Cotton Using Hexachlorocyclophosphazene and Triethanolamine)

  • 김정환;장진호
    • 한국염색가공학회지
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    • 제32권3호
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    • pp.150-157
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    • 2020
  • Hexachloro-cyclophosphazene(HCCP), a formaldehyde-free flame retardant (FR), was steam-cured with triethanol amine(TEA) to impart durable flame-retardancy to cotton fabrics. While the HCCP treatment alone showed very limited resistance to repeated laundering cycles, the addition of TEA substantially improved the laundering durability of the FR cotton up to twenty laundering cycles. The extended washing resistance was accomplished by the increased nucleophilic substitution of unreacted P-Cl groups in HCCP by the TEA resulting in the more densely crosslinked FR networks. With increasing molar ratio of TEA to the HCCP up to 2, the flame retarding effectivity and the synergistic effectiveness improved to 2.8 and 1.8 respectively. TGA and microscale combustion calorimetry verified the pyrolysis and combustion behaviors of the FR-cotton, which showed lower maximum pyrolysis and combustion temperatures together with substantially decreased peak pyrolysis and heat release rate, synergistically yielding larger amounts of carbonaceous chars. The formaldehyde-free HCCP and TEA can be a durable FR finishing agents for cotton fabrics acting through a solid-phase flame-retarding mechanism.

인코넬 합금의 미세조직과 기계적 특성에 미치는 냉각속도 영향 (Effect of Cooling Rates on Mechanical Properties and Microstructure of Inconel Alloys)

  • 박노경;이호성;채영석
    • 한국재료학회지
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    • 제17권10호
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    • pp.555-559
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    • 2007
  • The mechanical properties and microstructure of Inconel 690 and 600 alloys with various cooling rates were investigated. Optical microscopy and scanning electron microscopy observations indicated that in case of the cooling rate of $0.5^{\circ}C/min$, discontinuous carbides along the grain boundaries were formed and when the cooling rate was $10^{\circ}C/min$, continuous carbides were formed in Inconel 690 and 600 alloys. For the annealed Inconel 690 alloy with high Cr content, a lot of annealing twins, which led the preferential growth of (111) planes, were observed. However, the annealed Inconel 600 alloy with low Cr content showed a few annealing twins and the preferential growth of (200) planes. Inconel 600 alloy had a larger value of ultimate tensile strength (UTS) than Inconel 690 alloy.

Kideco 석탄의 스팀 가스화 반응에서 K2CO3 촉매의 비활성화 거동 (Deactivation Behavior of K2CO3 Catalyst in the Steam Gasification of Kideco Coal)

  • ;김수현;유지호;이시훈;임영준;임정환;김상도;전동혁;최호경;이영우
    • 한국수소및신에너지학회논문집
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    • 제27권5호
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    • pp.517-525
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    • 2016
  • The present work investigates the effect of $K_2CO_3$ catalyst on steam gasification of Kideco coal and the deactivation of the catalyst due to thermal exposure and interaction with coal ash. The gasification reactivity at $700^{\circ}C$ is highly enhanced by $K_2CO_3$, which is not deactivated by the heat treatment at $T{\leq}800^{\circ}C$. TGA and XRD results prove minor decomposition of $K_2CO_3$ after the calcination at $800^{\circ}C$. $K_2CO_3$ is, however, evaporated at the higher temperature. Assuming the conversion of $K_2CO_3$ into $K_2O$ by the decomposition and into $K_2O{\cdot}2.5SiO_2$ and $KAlO_2$ by the interaction with coal ash, the reactivity of the gasification is evaluated in the presence of $K_2O$, $K_2O{\cdot}2.5SiO_2$ and $KAlO_2$. Among them, $K_2O$ is the most active, but much lower in the activity than $K_2CO_3$. XRD results show that $K_2CO_3$ could react readily with the ash above $700^{\circ}C$.

황산 환경에서 Fe-Si, Ni-Ti계 및 Ni 합금의 내부식성 특성 (Corrosion Characteristics of Fe-Si, Ni-Ti and Ni Alloy in Sulfuric Acid Environments)

  • 권혁철;김동진;김홍표;박지연;홍성덕
    • 한국재료학회지
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    • 제21권1호
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    • pp.1-7
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    • 2011
  • Methods of producing hydrogen include steam reforming, electrochemical decomposition of water, and the SI process. Among these methods, the Sulfur iodine process is one of the most promising processes for hydrogen production. The thermochemical sulfur-iodine (SI) process uses heat from a high-temperature-gas nuclear reactor to produce $H_2$ gas; this process is known for its production of clean energy as it does not emit $CO_2$ from water. But the SI-process takes place in an extremely corrosive environment for the materials. To endure SI environments, the materials for the SI environment will have to have strong corrosion resistance. This work studies the corrosion resistances of the Fe-Si, Ni-Ti and Ni Alloys, which are tested in SI-process environments. Among the SI-process environments, the conditions of boiling sulfuric acid and decomposed sulfuric acid are selected in this study. Before testing in boiling sulfuric acid environments, the specimens of Fe-4.5Si, Fe-6Si, Ni-4.5Si, Ni-Ti-Si-Nb and Ni-Ti-Si-Nb-B are previously given heat treatment at $1000^{\circ}C$ for 48 hrs. The reason for this heat treatment is that those specimens have a passive film on the surface. The specimens are immersed for 3~14 days in 98wt% boiling sulfuric acid. Corrosion rates are measured by using the weight change after immersion. The corrosion rates of the Fe-6Si and Ni-Ti-Si-Nb-B are found to decrease as the time passes. The corrosion rates of Fe-6si and Ni-Ti-Si-Nb-B are measured at 0.056 mm/yr and 0.16 mm/yr, respectively. Hastelloy-X, Alloy 617, Alloy 800H and Haynes 230 are tested in the decomposed sulfuric acid for one day. Alloy 800H was found to show the best corrosion resistance among the materials. The corrosion rate of Alloy 800H is measured at -0.35 mm/yr. In these results, the corrosion resistance of materials depends on the stability of the oxide film formed on the surface. After testing in boiling sulfuric acid and in decomposed sulfuric acid environments, the surfaces and compositions of specimens are analyzed by SEM and EDX.

율무 flake 제조시 가열정도에 따른 특성 (Functional Characteristics of Job's-tears Flakes Subjected to Varying Degree of Heating)

  • 이영택;석호문;김성수;홍희도;김경탁
    • 한국식품과학회지
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    • 제27권5호
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    • pp.640-645
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    • 1995
  • 율무쌀을 이용하여 간편식인 flaked cereal을 제조하기 위하여 율무를 수침, 가열처리, 중간수분$(25{\sim}30%)$건조, flaking, 건조 및 cooking하였다. 율무는 가열처리시 가열시간이 $5{\sim}30$분으로 증가함에 따라 호화도가 증가하였으며 가열정도에 따른 호화도는 율무의 flaking roll 통과 적성에 변수로 작용하여 최종 flake 제품의 특성에 영향을 미쳤다. 율무는 flaking하기에 적합한 물성을 제공한 가열조건($5{\sim}10$분 증자처리)에서 호화도가 증가함에 따라 율무 flake의 specific volume이 증가하고 절단 강도는 감소하였다. 그러나 가열시간이 20분 이상으로 길어 호화도가 높아진 경우 flake 성형에 부정적 영향을 미쳐 specific volume이 감소하고 절단강도는 증가하는 경향을 보였다. 율무는 가열시간이 길어짐에 따라 율무 flake의 수분흡수지수와 수분용해도지수가 증가하였다. 율무 flake를 분쇄한 분말의 점도를 측정한 결과 전분의 호화도가 높아짐에 따라 점도는 현저히 증가하였고 amylograph에 의한 초기점도는 높은 반면 온도상승에 따라 최고점도는 낮아지는 경향을 나타냈다.

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